Simultaneous determination of four coccidiostats in eggs and broiler meat: Validation of an LC-MS/MS method

Food Additives and Contaminants

Volumn 23, Issue 5, 2006, Pages 470-478

  Rokka, Mervi ^a   Peltonen, Kimmo ^a  

^a NATL VET AND FOOD RES INSTITUTE   (Finland)

Author keywords

Coccidiostats; Eggs; LC MS MS; Poultry meat; Validation; Veterinary drug residues

Indexed keywords

ACETONITRILE; COCCIDIOSTATIC AGENT; LASALOCID; MONENSIN; NARASIN; SALINOMYCIN; SILICON DIOXIDE;

ACCURACY; ARTICLE; CONTROLLED STUDY; DRUG DETERMINATION; DRUG SELECTIVITY; DRUG SPECIFICITY; EGG; FOOD ANALYSIS; FOOD CONTAMINATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; MEAT; NONHUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; SAMPLING; SOLID PHASE EXTRACTION; VALIDATION PROCESS;

ANIMALS; CHICKENS; CHROMATOGRAPHY, LIQUID; COCCIDIOSTATS; EGGS; FOOD CONTAMINATION; LASALOCID; MASS SPECTROMETRY; MEAT; MONENSIN; PYRANS; REPRODUCIBILITY OF RESULTS;

EID: 33646401124     PISSN: 0265203X     EISSN: 14645122     Source Type: Journal    
DOI: 10.1080/02652030600573251     Document Type: Article

References (22)

1. Akhtar, MH and El-Soouds, KA and Shehata, MAA. (1996) Concentrations of salinomycin in eggs and tissues of laying chickens fed medicated feed 14 days followed by withdrawal for 3 days Food Additives and Contaminants, 13, pp. 897-907.
2. Antignac, J-P and Le, B and Monteau, F and Andre, F. (2003) Validation of analytical methods based on mass spectrometric detection according to the "20027/657/EC" European decision: Guidelines and application Analytica Chimica Acta, 483, pp. 325-334.
3. Anonymous.(2004) Results of residue examinations of products of animal origin in Finland 2003. In National Food Agency (NFA), National Veterinary and Food Research Institute (EELA) and Ministry of Agriculture and Forestry (MAF). (pp. 1-69). Helsinki: Finland.
4. Blanchflower, WJ and Kennedy, DG. (1995) Determination of lasalocid in eggs using liquid chromatography-electrospray mass spectrometry The Analyst, 120, pp. 1129-1132.
5. Blanchflower, WJ and Kennedy, DG. (1996) Determination of monensin, salinomycin and narasin in muscle, liver and eggs from domestic fowl using liquid chromatography-electrospray mass spectrometry Journal of Chromatography B, 675, pp. 225-233.
6. Coleman, MR and Moran, JW and Mowrey, DH. (1997) Liquid chromatographic determination of monensin in premix and animal feeds: Collaborative study Journal of AOAC International, 80, pp. 693-702.
7. (2002) Commission Decision 2002/657/EC of 12 August 2002 Official Journal of the European Communities, L221, pp. 8.
8. Gerhardt, GC and Salisbury, CDC and Campbell, HM. (1995) Determination of ionophores in the tissues of food animals by liquid chromatography Food Additives and Contamination, 12, pp. 731-737.
9. Harris, JA and Russell, CAL and Wilkins, JPG. (1998) The characterisation of polyether ionophore veterinary drugs by HPLC-electrospray MS The Analyst, 123, pp. 2625-2628.
10. Kennedy, DG and Blanchflower, WJ and Hughes, PJ and McMaughey, WJ. (1996) The incidence and cause of lasalocid residues in eggs in Northern Ireland Food Additives and Contaminants, 13, pp. 787-794.
11. Kennedy, DG and Hughes, PJ and Blanchflower, WJ. (1998) Ionophore residues in eggs in Northern Ireland: Incidence and cause Food Additives and Contaminants, 15, pp. 535-541.
12. Matabudul, DK and Conway, B and Lumley, ID. (2000) A rapid method for the determination of lasalocid in animal tissues and eggs by high performance liquid chromatography with fluorescence detection and confirmation by LC-MS-MS The Analyst, 125, pp. 2196-2200.
13. Matabudul, DK and Conway, B and Lumley, ID and Sumar, S. (2001) The simultaneous determination of the ionophore antibiotics in animal tissues and eggs by tandem electrospray LC-MS-MS Food Chemistry, 75, pp. 345-354.
14. Matabudul, DK and Lumley, ID and Points, JS. (2002) The determination of 5 anticoccidial drugs (nicarbazin, lasalocid, monensin, salinomycin and narasin) in animal livers and eggs by liquid chromatography linked with tandem mass spectrometry (LC-MS-MS) The Analyst, 127, pp. 760-768.
15. Moran, JW and Rodewald, JM and Donoho, AL and Coleman, MR. (1994) Determination of monensin in chicken tissues by liquid chromatography with postcolumn derivatization Journal of AOAC International, 77, pp. 885-890.
16. Pecorelli, I and Bibi, R and Fioroni, L and Galarini, R. (2004) Validation of a confirmatory method for the determination of sulphonamides in muscle according to the European Union regulation 2002/ 657/EC Journal of Chromatography A., 1032, pp. 23-29.
17. Rosén, J. (2001) Efficient and sensitive screening and conformation of residues of selected polyether ionophore antibiotics in liver and eggs by liquid chromatography-electrospray tandem mass spectrometry The Analyst, 126, pp. 1990-1995.
18. Tarbin, JA and Rawlings, E and Tyler, D and Sharman, M. (2002) Improved clean-up for the determination of lasalocid in "difficult" food matrices Food Additives and Contamination, 19, pp. 28-32.
19. Tarbin, JA and Shearer, G. (1992) Improved high-performance liquid chromatographic procedure for the determination of lasalocid in chicken tissues and egg using polymeric and porous graphitic carbon columns Journal of Chromatography Biomedical Applications, 579, pp. 177-183.
20. Turnipseed, SB and Roybal, JE and Pfenning, AP and Gonzales, SA and Hurlbut, JA and Madson, MR. (2001) LC/MS confirmation of ionophores in animal feeds Journal of AOAC International, 84, pp. 640-647.
21. van Trijp, JMP and Roos, AH.(1991) Model for the calculation of calibration curves. In RIKILT Report 91.02 1991.
22. Yakkundi, S and Cannacan, A and Elliott, CT and Lövgren, T and Kennedy, DG. (2003) Development and validation of a method for the confirmation of halofuginone in chicken liver and eggs using electrospray tandem mass spectrometry Journal of Chromatography B, 788, pp. 29-36.