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The discrete rectangle structurally resembles double-strand porphyrin ladders: (a) Screen, T. E. O.; Thorne, J. R. G.; Denning, R. G.; Bucknall, D. G.; Anderson, H. L. J. Am. Chem. Soc. 2002, 124, 9712-9713. (b) Taylor, P. N.; Anderson, H. L. J. Am. Chem. Soc. 1999, 121, 11538-11545. (c) Anderson, H. L. Inorg. Chem. 1994, 33, 972-981.
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note
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Significant UV/vis spectral changes of 3b were also observed upon addition of 4,4′-bipyridine ligand (see the Supporting Information).
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36
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note
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In the evaluation of binding constants, an excellent fit was obtained for all data points with a simple model which assumes an equal K for all aza ligand-zinc porphyrin interactions, i.e., independent, and not cooperative binding.
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