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32
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note
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4, then filtered, and concentrated under reduced pressure. The resultant crude mixture was purified by column chromatography (silica gel), using an 1:4 EtOAc/hexane mixture as eluent, to give pure 2-decanone (0.13 g, 85%).
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2, followed by stirring under identical reaction conditions.
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31444449566
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note
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The oxidation of cyclohexene did not proceed efficiently, and trace amounts of cyclohexanone were obtained.
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