The first isolation and characterization of a palladium-copper heterometallic complex bearing μ4-oxo atom derived from molecular oxygen

Journal of the American Chemical Society

Volumn 118, Issue 16, 1996, Pages 3990-3991

  Hosokawa, Takahiro ^a   Takano, Minora ^a   Murahashi, Shun Ichi ^a  

^a OSAKA UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

COPPER COMPLEX; PALLADIUM COMPLEX;

ARTICLE; DRUG STRUCTURE; DRUG SYNTHESIS; REACTION ANALYSIS; STEREOCHEMISTRY;

EID: 0029989836     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja953514k     Document Type: Article

References (23)

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13. X-ray crystallographic data were collected using the ω/2θ technique on a RIGAKU AFC7R diffractometer with graphite-monochromated Mo Ka radiation (λ = 0.71069 Å) to maximum 2θ = 55° at room temperature. The structures were solved by direct methods using SAPI 91 for complex 1 and SHELXS-86 for complex 2 and refined by full-matrix least squares for observed unique reflections with 1 > 3σ(1).
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