Comparison of dynamic headspace methods used for the analysis of the volatile composition of Spanish PDO ewe's raw milk cheeses

Lait

Volumn 85, Issue 6, 2005, Pages 491-513

  Barron, Luis Javier R ^a   Redondo, Yolanda ^a   Ortigosa, María ^c   Carbonell, María ^b   García, Susana ^c   Torre, Paloma ^c   De Renobales, Mertxe ^a   Fernández García, Estrella ^b  

^a UNIVERSITY OF THE BASQUE COUNTRY UPV EHU   (Spain)

^b INIA   (Spain)

^c PUBLIC UNIVERSITY OF NAVARRE   (Spain)

Author keywords

Cheese; Dynamic headspace analysis; Inter laboratory study; Volatile compound

Indexed keywords

EID: 28844452969     PISSN: 00237302     EISSN: None     Source Type: Journal    
DOI: 10.1051/lait:2005036     Document Type: Article

References (52)

1. Almarcha M., Rovira J., Análisis de compuestos orgánicos volátiles (VOC) mediante atrapamiento en adsorbentes carbonáceos y desorción térmica mediante microondas guiadas, Técn. Lab. 164 (1991) 322-327.
2. Ayad E.H.E., Awad S., El Attar A., de Jong C., El-Soda M., Characterisation of Egyptian Ras cheese. 2. Flavour formation, Food Chem. 86 (2004) 553-561.
3. Barroso M., Barron L.J.R., Optimization of the analytical conditions dealing with the volatile fraction of cheese using dynamic headspace and trap desorption by means of microwave energy, in: Sontag G., Pfannhauser W. (Eds.), Current Status and Future Trends, vol. 1, Proceedings of EURO FOOD CHEM VIII, Wageningen Press, Wageningen, Germany, 1995, pp. 18-25.
4. Boscaini E., van Ruth S., Biasioli F., Gasperi F., Maerk T.D., Gas chromatography-olfactometry (GC-O) and proton transfer reaction-mass spectrometry (PTR-MS) analysis of the flavour profile of Grana Padano, Parmiggiano Reggiano, and Grana Trentino cheeses, J. Agric. Food Chem. 51 (2003) 1782-1790.
5. Bosset J.O., Gauch R., Mariaca R., Klein B., Comparison of various sample treatments for the analysis of volatile compounds by GC-MS: Application to the Swiss Emmental cheese, Mitt. Gebiete Lebensm. Hyg. 86 (1995) 672-698.
6. Carbonell M., Núñez M., Fernández-García E., Evolution of the volatile components of ewe raw milk La Serena cheese during ripening. Correlation with flavour characteristics, Lait 82 (2002) 683-698.
7. Carbonell M., Núñez M., Fernández-García E., Seasonal variation of volatile compounds in ewe raw milk La Serena cheese, Lait 82 (2002) 699-711.
8. Careri M., Manini P., Spagnoli S., Barbieri G., Bolozoni L., Simultaneous-distillation-extraction and dynamic headspace methods in the gas chromatographic analysis of Parmesan cheese volatiles, Chromatographia 38 (1994) 386-394.
9. Chávarri F., Bustamante M.A., Santisteban A., Virto M., Barron L.J.R., de Renobales M., Changes in free fatty acids during ripening of Idiazabal cheese manufactured at different times of the year, J. Dairy Sci. 82 (1999) 885-890.
10. Chávarri F., Bustamante M.A., Santisteban A., Virto M., Albisu M., Barron L.J.R., de Renobales M., Effect of milk pasteurization on lipolysis during ripening of Idiazabal cheese manufactured at different times of the year, Lait 80 (2000) 433-444.
11. Curioni P.M.G., Bosset J.O., Key odorants in various cheese types as determined by gas chromatography-olfactometry, Int. Dairy J. 12 (2002) 959-984.
12. Di Cagno R., Banks J., Sheehan L., Fox P.F., Brechany E.Y., Corsetti A., Gobbetti M., Comparison of the microbiological, compositional, biochemical, volatile profile and sensory characteristics of three Italian PDO ewes' milk cheeses, Int. Dairy J. 13 (2003) 961-972.
13. Dirink P., De Winne A., Flavour characterisation and classification of cheeses by gas chromatographic-mass spectrometric profiling, J. Chromatogr. A 847 (1999) 203-208.
14. Fernández-García E., Use of headspace sampling in the quantitative analysis of artisanal Spanish cheese aroma, J. Agric. Food Chem. 44 (1996) 1833-1839.
15. Fernández-García E., Carbonell M., Núñez M., Volatile fraction and sensory characteristics of Manchego cheese. 1. Comparison of raw and pasteurized milk cheese, J. Dairy Res. 69 (2002) 579-593.
16. Fernández-García E., Carbonell M., Gaya P., Núñez M., Evolution of the volatile components of ewes raw milk Zamorano cheese. Seasonal variation, Int. Dairy J. 14 (2004) 701-711.
17. Fernández-García E., Gaya P., Medina M., Núñez M., Evolution of the volatile components of raw ewes' milk Castellano cheese: seasonal variation, Int. Dairy J. 14 (2004) 39-46.
18. Ferraza R.E., Fresno J.M., Riberiro J.I., Tornadejo M.E., Mansur Furtado M., Changes in the microbial flora of Zamorano cheese (P.D.O.) by accelerated ripening process, Food Res. Int. 37 (2004) 149-155.
19. Freitas A.C., Macedo A.C., Malcata F.X., Review: technological and organoleptic issues pertaining to cheeses with denomination of origin manufactured in the Iberian Peninsula from ovine and caprine milks, Food Sci. Technol. Int. 6 (2000) 351-370.
20. Gallois A., Langlois F., New results in the volatile odorous compounds of French cheeses, Lait 70 (1990) 89-106.
21. Gómez-Ruiz J.A., Ballesteros C., Gonzalez Viñas M.A., Cabezas L., Martínez-Castro I., Relationships between volatile compounds and odour in Manchego cheese: comparison between artisanal and industrial cheeses at different ripening times, Lait 82 (2002) 613-628.
22. Hair J.F., Anderson R.E., Tatham R.L., Black W.C., Multivariate data analysis, 5th edn., Prentice-Hall, London, UK, 1998.
23. Imhof R., Bosset J.O., Comparison of two systems for sample preparation and injection by dynamic headspace GC analysis, J. High Resol. Chromatogr. Comm. 14 (1991) 621-625.
24. Irigoyen A., Izco J.M., Ibáñez F.C., Tone P., Influence of rennet milk-clotting activity on the proteolytic and sensory characteristics of an ovine cheese, Food Chem. 72 (2001) 137-144.
25. Izco J.M., Torre P., Characterisation of volatile flavour compounds in Roncal cheese extracted by the "purge and trap" method and analysed by GC-MS, Food Chem. 70 (2000) 409-417.
26. Larráyoz P., Carbonell M., Ibáñez F.C., Torre P., Barcina Y., Optimization of indirect parameters which affect the extractability of volatile aroma compounds from Idiazabal cheese using analytical supercritical fluid extraction (SFE), Food Chem. 64 (1999) 123-127.
27. Larráyoz P., Addis M., Gauch R., Bosset J.O., Comparison of dynamic headspace and simultaneous distillation extraction techniques used for the analysis of the volatile components in three European PDO ewe's milk cheeses, Int. Dairy J. 11 (2001) 911-926.
28. Lawlor J.B., Delahunty C.M., Wilkinson M.G., Sheehan J., Relationships between the gross, non-volatile and volatile compositions and the sensory attributes of eight hard-type cheeses, Int. Dairy J. 12 (2002) 493-509.
29. Lawlor J.B., Delahunty C.M., Sheehan J., Wilkinson M.G., Relationships between sensory attributes and the volatile compounds, non-volatile and gross compositional constituents of six blue-type cheeses, Int. Dairy J. 13 (2003) 481-494.
30. Lecanu L., Ducruet V., Jouquand C., Gratadoux J.J., Feigenbaum A., Optimization of head-space soli-phase microextraction (SPME) for the odor analysis of surface-ripened cheese, J. Agric. Food Chem. 50 (2002) 3810-3817.
31. Lee J.H., Diono R., Kim G.Y., Min D., Optimization of solid phase microextraction analysis for the headspace volatile compounds of Parmesan cheese, J. Agric. Food Chem. 51 (2003) 1136-1140.
32. Mariaca R., Bosset J.O., Instrumental analysis of volatile (flavour) compounds in milk and dairy products, Lait 77 (1997) 13-40.
33. Ministerio de Agricultura, Pesca y Alimentacion, Reglamento de la Denominación de Origen Roncal y de su Consejo Regulador, Bol. O. Estado 63 (1991) 8489.
34. Ministerio de Agricultura, Pesca y Alimentación, Reglamento de la Denominación de Origen Idiazabal y de su Consejo Regulador, Bol. O. Estado 289 (1993) 34591.
35. Ministerio de Agricultura, Pesca y Alimentación, Reglamento de la Denominación de Origen Queso Zamorano y su Consejo Regulador, Bol. O. Estado 120 (1993) 115311.
36. Ministerio de Agricultura, Pesca y Alimentación, Reglamento de la Denominación de Origen Queso de La Serena y su Consejo Regulador, Bol. O. Estado 100 (1993) 12501.
37. Ministerio de Agricultura, Pesca y Alimentación, Reglamento de la Denominación de Origen Queso Manchego y de su Consejo Regulador, Bol. O. Estado 295 (1995) 35548.
38. Moio L., Piombino P., Addeo F., Odourimpact compounds of Gorgonzola cheese, J. Dairy Res. 67 (2000) 273-285.
39. Muñoz N., Ortigosa M., Torre P., Izco J.M., Free amino acids and volatile compounds in an ewe's milk cheese as affected by seasonal and cheese-making plant variations, Food Chem. 83 (2003) 329-338.
40. Núñez A.J., Gonzalez L.F., Janák J., Preconcentration of headspace volatiles for trace organic analysis by gas chromatography, J. Chromatogr. 300 (1984) 127-162.
41. O'Riordan P.J., Delahunty C.M., Characterisation of commercial Cheddar cheese flavour. 2: study of Cheddar cheese discrimination by composition, volatile compounds and descriptive flavour assessment, Int. Dairy J. 13 (2003) 371-389.
42. Ortigosa M., Torre P., Izco J.M., Effect of pasteurization of ewe's milk and use of a native starter culture on the volatile components and sensory characteristics of Roncal cheese, J. Dairy Sci. 84 (2001) 1320-1330.
43. Pérez-Elortondo F.J., Aldámiz-Echebarria P., Albisu M., Barcina Y., Indigenous lactic acid and bacteria in Idiazabal ewe's milk cheese, Int. Dairy J. 8 (1998) 725-732.
44. Póveda J., Pérez-Coello M.S., Cabezas L., Evolution of the free fatty acid fraction in Manchego cheese during ripening, Milchwissenschaft 54 (1999) 685-687.
45. Rektorik J., Head-space and desorption by microwaves, Riv. Ital. EPPOS 4 (1993) 165-173.
46. Roa L, López M.B., Mendiola F.J., Residual clotting activity and ripening properties of vegetable rennet from Cynara cardunculus in La Serena cheese, Food Res. Int. 32 (1999) 413-419.
47. Stefanon B., Procida G., Effects of including silage in the diet on voaltile compound profiles in Montasio cheese and their modification during ripening, J. Dairy Res. 71 (2004) 58-65.
48. Thierry A., Maillard M.B., Hervé C., Richoux R., Lortal S., Varied volatile compounds are produced by Propionibacterium freudenreichii in Emmental cheese, Food Chem. 87 (2004) 439-446.
49. Valero E., Villaseñor M.J., Sanz J., Martínez-Castro I., Comparison of two methods based on dynamic headspace for GC-MS analysis of volatile components of cheeses, Chromatographia 52 (2000) 340-344.
50. Valero E., Sanz J., Martínez-Castro I., Direct thermal desorption in the analysis of cheese volatiles by gas chromatography and gas chromatography-mass spectrometry: comparison with simultaneous distillationextraction and dynamic headspace, J. Chromatogr. Sci. 39 (2001) 222-228.
51. Villaseñor M.J., Valero E., Sanz J., Martínez-Castro I., Analysis of volatile compounds of Manchego cheese by dynamic headspace followed by automatic thermal desorption-GC-MS, Milchwissenschaft 55 (2000) 378-382.
52. Wilkes J.G., Conte E.D., Kim Y., Holcomb M., Sutherland J.B., Miller D.W., Sample preparation for the analysis of flavours and off-flavours in foods, J. Chromatogr. A 880 (2000) 3-33.