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Experimental conditions, a: Cd/Se = 1/1 in molar ratio, ODE (octadecene) 1 mL, TOPO 4 g, 180°C for 10 min; b: Cd/Se = 1/1.2, ODE 1 mL, TOPO 4 g, 200°C for 10 min; c: Cd/Se = 1/1.2, TOPO 4.5 g, ODA (octadecylamine) or HDA (hexadecylamine) 0.5 g, 240°C for 20 min; d: Cd/Se = 1/1.5, TOPO 4.5 g, ODA or HDA 0.5 g, 260°C for 30 min; e: Cd/Se = 1/2, TOPO 5 g, 300°C for 30 min; f: Cd/Se = 1/5, TOPO 5 g, 360°C for 60 min.
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