HS-SPME gas chromatographic characterization of volatile compounds in milk tainted with off-flavour

International Dairy Journal

Volumn 15, Issue 12, 2005, Pages 1203-1215

  Mounchili, A ^a   Wichtel, J J ^a   Bosset, J O ^b   Dohoo, I R ^a   Imhof, M ^b   Altieri, D ^b   Mallia, S ^b   Stryhn, H ^a  

^a UNIVERSITY OF PRINCE EDWARD ISLAND   (Canada)

^b AGROSCOPE LIEBEFELD POSIEUX RESEARCH STATION ALP   (Switzerland)

Author keywords

Feeding; Flame ionization detector; Gas chromatography; Mass spectrometry; Milk; Off flavour; Olfactometry; Sensory analysis; Silage; Solid phase micro extraction; Volatile (flavour impact) compound

Indexed keywords

BUTANE; IONIZATION; MASS SPECTROMETRY;

FLAME IONIZATION; SENSORY PANELS;

GAS CHROMATOGRAPHY;

EID: 24044499977     PISSN: 09586946     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.idairyj.2004.11.018     Document Type: Article

References (38)

1. AOAC International. (2000). Official methods of analysis of AOAC International (17th ed.) Gaithersburg, MD, USA: AOAC International.
2. J. Bendall Aroma compounds of fresh milk from New Zealand cows fed different diets Journal of Agricultural Food Chemistry 49 2001 4825 4832
3. Bosset, J. O., Ebenhard, P., Gallmann, P., Gauch, R., Rattray, W., & Sieber, R. (1995). Occurrence and behaviour of volatile sulfur-containing compounds in milk by heat treatment. Heat treatments & alternative methods. Proceeding of the IDF symposium, Vienna, Austria, September 6-8, 1995 (pp. 409-421).
4. D.V. Cicchetti, and A.R. Feinstein High agreement but low kappa: II. Resolving the paradoxes Journal of Clinical Epidemiology 43 1990 551 558
5. J. Cohen A coefficient of agreement for nominal scales Educational and Psychological Measurement 20 1960 37 46
6. L.J. Cronbach Coefficient alpha and the internal structure of tests Psychometrika 16 1951 297 334
7. E.H. Farrington Silage odor in milk Hoard's Dairyman 36 1905 32
8. E. Fernández-García Use of the headspace sampling in the quantitative analysis of the artisanal Spanish cheese aroma Journal of Agricultural and Food Chemistry 44 1996 1833 1839
9. E. Fernández-Garcia, C. Serrano, and M. Nuňez Volatile fraction and sensory characteristics of Manchego cheese, 2. Seasonal variation Journal of Dairy Research 69 2002 595 604
10. Gamble, J. A., & Kelly, E. (1922). The effect of silage on the flavor and odor of milk. US Department of Agriculture Bulletin no. 1097 (p. 24).
11. D.T. Gordon, and M.E. Morgan Principal volatile compounds in feed flavored milk Journal of Dairy Science 55 1972 905 912
12. A.M. Graham, and V. Walker Headspace solid-phase microextraction procedures for gas chromatographic analysis of biological fluids and materials Journal of Chromatography A 902 2000 267 287
13. K. Gwet Kappa statistic is not satisfactory for assessing the extent of agreement between raters Statistical Methods for Inter-rater Reliability Assessment 1 2002 1 6
14. R. Imhof, and J.O. Bosset Quantitative GC-MS analysis of volatile flavour compounds in pasteurized milk and fermented milk products applying a standard addition method Lebensmittel Wissenschaft und Technologie 27 1994 265 269
15. W.J. Keller Jr., and D.H. Kleyn Headspace gas chromatography for objectively determining intensity of flavor in raw milk Journal of Dairy Science 55 1972 574 576
16. E. Kovats Gas chromatography characterization of organic substances in the retention index system Advances in Chromatography 1 1965 229 247
17. J.R. Landis, and G.G. Koch The measurement of observer agreement for categorical data Biometrics 33 1977 159 174
18. B.E. Loney, R. Bassette, and G.M. Ward Some volatile components in milk, blood, and urine from cows fed silage, bromegrass, and hay and grain Journal of Dairy Science 46 1963 922 926
19. R.T. Marsili Gas chromatography-olfactometry in food aroma analysis R.T. Marsili Flavor, fragrance, and odor analysis 1997 Marcel Dekker Inc New York 203 227
20. M.E. Morgan, and R.L. Pereira Volatiles constituents of grass and corn silage. I. Steam distillates Journal of Dairy Science 45 1962 467 471
21. M.E. Morgan, and R.L. Pereira Volatile constituents of grass and corn silage. II. Gas-entrained aroma Journal of Dairy Science 45 1962 457 466
22. A. Mounchili, J.J. Wichtel, I.R. Dohoo, G.P. Keefe, and L.J. Halliday Risk factors for milk off-flavours in dairy herds from Prince Edward Island, Canada Preventive Veterinary Medicine 64 2004 133 145
23. S. Patton, D.A. Forss, and E.A. Day Methylsulfide and the flavor of milk Journal of Dairy Science 39 1956 1469 1470
24. W.E. Petersen, and J.G. Brereton Effect of inhaled substances on milk flavors Journal of Dairy Science 25 1942 381 387
25. P. Pollien, L. Fay, M. Baumgartner, and A. Chaitreau First attempt of odorant quantification using gas chromatography-olfactometry Analytical Chemistry 71 1999 5391 5397
26. L.M. Poste, D.A. Mackie, G. Butler, and E. Larmond J. Buckly Laboratory methods for sensory analysis of food 1991 Canada Communication Group-Publishing Center Ottawa
27. R.B. Potts, and E.M. Kessler Milk flavor and blood and acetone bodies Journal of Dairy Science 40 1957 1466 1470
28. A.T. Randby, I. Selmer-Olsen, and L. Bævre Effect of ethanol in feed on milk flavor and chemical composition Journal of Dairy Science 82 1998 420 428
29. M.C. Reddy, R. Bassette, G. Ward, and J.R. Dunham Relationship of methyl sulfide and flavor score of milk Journal of Dairy Science 50 1967 147 150
30. F.J. Señorans, J. Tabera, M. Herraiz, and C. Reglero A method for direct isolation and gas chromatography analysis of milk flavor components using a programmed temperature vaporizer Journal of Dairy Science 79 1996 1706 1712
31. W.F. Shipe, R.A. Ledford, R.D. Peterson, R.A. Scanlon, H.F. Geerken, R.W. Dougherty, and M.E. Morgan Physiological mechanism involved in transmitting flavors and odors to milk. II. Transmission of some flavor components of silage Journal of Dairy Science 45 1962 477 480
32. ® statistical software: release 8.0. College Station, Texas, USA.
33. B. Toso, G. Procida, and B. Stefanon Determination of volatile compounds in cows'milk using headspace GC-MS Journal of Dairy Research 69 2002 569 577
34. G. Urbach Headspace volatiles from cold-stored raw milk Australian Journal of Dairy Technology 45 1990 80 85
35. P.J. Van Soest, J.B. Robertson, and B.A. Lewis Methods for dietary fiber, neutral detergent fiber, and nonstarch polysaccharides in relation to animal nutrition Journal of Dairy Science 74 1991 3583 3597
36. I. Verdier, J.B. Coulon, P. Pradel, and J.L. Berdagué Effect of forage type and cow breed on the characteristics of matured Saint-Nectaire cheese Lait 75 1995 523 533
37. Woll, F. W., & Humphrey, G. C. (1904). Soybean silage as a food for dairy cows. Wisconsin Agricultural Experimental Station, 21st Annual Report (pp. 67-74).
38. J.D. Wynn, J.R. Brunner, and G.M. Trout Gas chromatography as a means of detecting odors in milk Food Technology 14 1960 248 250