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(a) At least two runs were performed for each experiment, and average yields are given in Table 1.
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20444464628
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Side-product formation was increased in proportion to an excess amount of the Grignard reagent. Each regioisomer is predominantly (8:1) the (E)-isomer by comparison of the chemical shift to that of related compounds: Tarasova, O. A.; Schmidt, E. Y.; Albanov, A. I.; Mikhaleva, A. I.; Brandsma, L.; Trofimov, B. A. Zh. Org. Khim. 1999, 35, 1530.
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