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0038710934
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A double focusing SAXS camera with μm focal spot based on a circular Bragg-Fresnel lens
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A. Snigirev, I. Snigireva, C. Riekel, A. Miller, L. Wess, and T. Wess A double focusing SAXS camera with μm focal spot based on a circular Bragg-Fresnel lens J. Phys. 3 1994 443 446 Important step in the development of μ-SAXS as first order of collagen (65 nm) could be resolved with 1-2 μm spot. The unusual geometry of the camera (back reflection) and the difficulty in obtaining optical elements did, however, result in an abandon of this approach.
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Submicrometer beamsize observed at the exit of an X-ray waveguide
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W. Jark, S. DiFonzo, S. Lagomarsino, A. Cedola, E.D. Fabrizio, A. Bram, and C. Riekel Submicrometer beamsize observed at the exit of an X-ray waveguide J. Appl. Phys. 80 1996 4831 4836 First evaluation of performance of 1D X-ray waveguide at 3rd generation SR-source. The groups from Trieste (Jark, DiFonzo) and Rome (Lagomarsini, Cedola) pioneered the use of 1D X-ray waveguides at ESRF.
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0034509852
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M. Müller, M. Burghammer, D. Flot, C. Riekel, C. Morawe, B. Murphy, and A. Cedola Microcrystallography with an X-ray waveguide J. Appl. Crystallogr. 33 2000 1231 1240 This paper explores various applications of 1D X-ray waveguides for μ-XRD ranging from hard to soft condensed matter.
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Cedola, A.7
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0031079236
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Micro-diffraction experiments on single polymeric fibres by synchrotron radiation
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C. Riekel, A. Cedola, F. Heidelbach, and K. Wagner Micro-diffraction experiments on single polymeric fibres by synchrotron radiation Macromolecules 30 1997 1033 1037 First demonstration of single fiber m-XRD experiments with a glass capillary microbeam at a 3rd generation SR-source. Introduces new ways to display information contained in composite diffraction images.
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Macromolecules
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Riekel, C.1
Cedola, A.2
Heidelbach, F.3
Wagner, K.4
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0029952099
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A compound refractive lens for focusing high-energy X-rays
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Nature
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Snigirev, A.1
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B. Lengeler, C.G. Schroer, B. Benner, T.F. Guenzler, M. Kuhlmann, J. Tuemmler, A.S. Simionovici, M. Drakopoulos, A. Snigirev, and I. Snigireva Parabolic refractive X-ray lenses: a breakthrough in X-ray optics NIM A 467-468 2001 944 950 Discussion of 2D focusing refractive lenses developed by the group of Lengeler et al. For micron-sized spots, several hundred lenses have to be stacked. The absorption of the first generation Al-lenses implied that large stacks could only be used at shorter wavelength. The recent introduction of refractive Be-lenses by the same group is of particular interest for microfocusing at about 13 keV.
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20444369058
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http://nano.anl.gov/research/nanoprobe.html. • This web site provides information on the scope of the Center for Nanoscale Materials at the APS, which will make use of a dedicated nanofocus beamline for X-ray imaging, μ-XRD and X-ray micro-fluorescence applications.
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15
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0037067599
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Two-dimensional X-ray waveguides and point sources
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F. Pfeiffer, C. David, M. Burghammer, C. Riekel, and T. Salditt Two-dimensional X-ray waveguides and point sources Science 297 2002 230 234 Detailed simulation and first experimental demonstration of 2D X-ray waveguide structures.
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Science
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Pfeiffer, F.1
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0000326319
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High gain beam compression in new-generation thin-film x-ray waveguides
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W. Jark, A. Cedola, S.D. Fonzo, M. Fiordelisi, S. Lagomarsino, N.V. Kovalenko, and V.A. Chernov High gain beam compression in new-generation thin-film x-ray waveguides Appl. Phys. Lett. 78 2001 1192 1194 The performance of the latest generation of 1D waveguides used at ESRF is discussed. The waveguide has been produced at Budger institute in Russia.
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Jark, W.1
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Chernov, V.A.7
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17
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0034505692
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Microbeam small-angle scattering experiments and their combination with microdiffraction
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C. Riekel, M. Burghammer, and M. Müller Microbeam small-angle scattering experiments and their combination with microdiffraction J. Appl. Crystallogr. 33 2000 421 423 Discussion on the layout of μ-SAXS cameras with pinhole geometry. The resolution is shown to depend on the beam divergence at the sample position and on the angular detector acceptance.
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J. Appl. Crystallogr.
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Riekel, C.1
Burghammer, M.2
Müller, M.3
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18
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0035061067
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Microstructural homogeneity of support silk spun by Eriophora fuliginea (C.L. Koch) determined by scanning X-ray microdiffraction
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C. Riekel, C.L. Craig, M. Burghammer, and M. Müller Microstructural homogeneity of support silk spun by Eriophora fuliginea (C.L. Koch) determined by scanning X-ray microdiffraction Naturwissenschaften 88 2001 67 72 Composite image of spider silk fibers showing the presence of two types of fibers.
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Naturwissenschaften
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Riekel, C.1
Craig, C.L.2
Burghammer, M.3
Müller, M.4
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19
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0345593647
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Aspects of X-ray diffraction on single spider fibers
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C. Riekel, C. Bränden, C. Craig, C. Ferrero, F. Heidelbach, and M. Müller Aspects of X-ray diffraction on single spider fibers Int. J. Biol. Macromol. 24 1999 187 195
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Int. J. Biol. Macromol.
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Riekel, C.1
Bränden, C.2
Craig, C.3
Ferrero, C.4
Heidelbach, F.5
Müller, M.6
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20
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0035997060
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Direct X-ray observation of a single hexagonal myofilament lattice in native myofibrils of striated muscle
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H. Iwamoto, Y. Nishikawa, K. Wakayama, and T. Fujisawa Direct X-ray observation of a single hexagonal myofilament lattice in native myofibrils of striated muscle Biophys. J. 2002 1074 1081 The best geometry for m-SAXS on very small fibrous biopolymers is systematically explored.
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Biophys. J.
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Iwamoto, H.1
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Fujisawa, T.4
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21
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0035877950
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Structural investigation of poly(3-hydroxybutyrate) spherulites by microfocus X-ray diffraction
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M. Gazzano, M.L. Focarete, C. Riekel, A. Ripamonti, and M. Scandola Structural investigation of poly(3-hydroxybutyrate) spherulites by microfocus X-ray diffraction Macromol. Chem. Phys. 202 2001 1405 1409
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Macromol. Chem. Phys.
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22
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0034575299
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Bacterial poly(3-hydroxybutyrate): An optical microscopy and microfocus X-ray diffraction study
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M. Gazzano, M.L. Focarete, C. Riekel, and M. Scandola Bacterial poly(3-hydroxybutyrate): an optical microscopy and microfocus X-ray diffraction study Biomacromolecules 1 2000 604 608
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Biomacromolecules
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Gazzano, M.1
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Scandola, M.4
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24
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0000705985
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Imaging of the helical arrangement of cellulose fibrils in wood by synchrotron radiation X-ray microdiffraction
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H. Lichtenegger, M. Müller, O. Paris, C. Riekel, and P. Fratzl Imaging of the helical arrangement of cellulose fibrils in wood by synchrotron radiation X-ray microdiffraction J. Appl. Crystallogr. 32 1999 1127 1133 Paper showing for the first time that the orientation of cellulose nanofibrils in single wood cells can be directly derived from a scanning μ-WAXS experiment. The data served to generate a vector diagram showing the across-cell variation of helical orientation.
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J. Appl. Crystallogr.
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Lichtenegger, H.1
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Relationship between structure and mechanical properties for aramide fibres
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R.J. Young, D. Lu, R.J. Day, W.F. Knoff, and H.A. Harris Relationship between structure and mechanical properties for aramide fibres J. Mater. Sci. 27 1992 5431 5440 Systematic investigation of varieties of PPTA fibers using tensile testing with Raman spectroscopy. Difference in Raman band shift rates for PPTA fibers with large 'skin-core' variations noted and differences in tensile properties observed.
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Young, R.J.1
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Single fibre deformation studies of poly(p-phenylene benzobisoxazole) fibres
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R.J. Davies, M.A. Montes-Moran, C. Riekel, and R.J. Young Single fibre deformation studies of poly(p-phenylene benzobisoxazole) fibres J. Mater. Sci. 36 2001 3079 3087
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An X-ray microdiffraction study of chain-orientation in poly(p-phenylene terephthalamide)
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C. Riekel, T. Dieing, P. Engström, L. Vincze, C. Martin, and A. Mahendrasingam An X-ray microdiffraction study of chain-orientation in poly(p-phenylene terephthalamide) Macromolecules 32 1999 7859 7865 First paper combining 2D scanning mXRD with tensile strain. It could be shown that the 'skin-core' structure was dependent on the strain.
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Macromolecules
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Rotational disorder in poly(p-phenylene terephthalamide) fibers by X-ray diffraction with a 100 nm beam
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S. Roth, M. Burghammer, A. Janotta, and C. Riekel Rotational disorder in poly(p-phenylene terephthalamide) fibers by X-ray diffraction with a 100 nm beam Macromolecules 36 2003 1585 1593 This paper introduces a rotational domain disorder model for PPTA with a layering structure. A variation of layering with processing is suggested. A more detailed study of the onset of layering during fiber formation would be a logical step.
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Macromolecules
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C. Riekel, M.C. García-Gutiérrez, A. Gourrier, and S. Roth Recent synchrotron radiation microdiffraction experiments on polymer and biopolymer fibers Anal. Bioanal. Chem. 376 2003 594 601
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Supramolecular structure of a high-modulus polyaromatic fiber (Kevlar 49)
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The use of synchrotron radiation X-ray scattering coupled with in-situ mechanical testing for studying deformation and structural change in isotactic polypropylene
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R.J. Davies, N.E. Zafeiropoulos, K. Schneider, S.V. Roth, M. Burghammer, C. Riekel, J.C. Kotek, and M. Stamm The use of synchrotron radiation X-ray scattering coupled with in-situ mechanical testing for studying deformation and structural change in isotactic polypropylene Colloid Polym. Sci. 282 2004 854 866 Shows how laboratory equipment (optical, tensile) can be integrated into a μ-XRD environment.
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Y.T. Shyng, R.J. Young, and R.J. Davies Analysis of interfacial micromechanics of single-fibre model composites using synchrotron microfocus X-ray diffraction ECCM11 2004 Rhodes Greece (Paper B124) Demonstration of composite interface assessment with μ-XRD-techniques
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ASM International
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ASM Metals Handbook vol 8 2000 ASM International
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P.J.M. Bartos J.J. Hughes P. Trtik W. Zhu Royal Society of Chemistry
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D. Loidl, O. Paris, M. Müller, M. Burghammer, C. Riekel, K. Kromp, and H. Peterlik Nanostructure of single carbon fibres investigated with synchrotron radiation P.J.M. Bartos J.J. Hughes P. Trtik W. Zhu Nanotechnology in Construction 2004 Royal Society of Chemistry 205 214 This paper uses for the first time a 1D X-ray waveguide beam to scan a deformed fiber.
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Numerical-experimental method for the identification of plastic properties of polymers from microhardness tests
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Investigation of structural processes during indentation of polymers by synchrotron radiation microdiffraction
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A. Gourrier, M.C. García-Gutiérrez, and C. Riekel Combined microindentation and synchrotron radiation microdiffraction applied to polymers Macromolecules 35 2002 8072 8077 First paper showing the combination of microindentation and μ-XRD. It shows notably that in-situ studies during indentation are possible.
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0043199384
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Fast intra-crystalline hydration of β-chitin revealed by a combined microdrop generation and on-line synchrotron radiation microdiffraction
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M. Rössle, D. Flot, J. Engel, C. Riekel, and H. Chanzy Fast intra-crystalline hydration of β-chitin revealed by a combined microdrop generation and on-line synchrotron radiation microdiffraction Biomacromolecules 4 2003 981 986 A microdrop generator is used to hydrate locally a Pogonophora tube made out of β-chitin. A single water drop has a volume of 65 pL! The experiments suggest a transient, highly disordered, hydrated β-chitin phase.
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(2003)
Biomacromolecules
, vol.4
, pp. 981-986
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Rössle, M.1
Flot, D.2
Engel, J.3
Riekel, C.4
Chanzy, H.5
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47
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4143090569
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Structural processes during starch granule hydration by synchrotron radiation microdiffraction
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H. Lemke, M. Burghammer, D. Flot, M. Roessle, and C. Riekel Structural processes during starch granule hydration by synchrotron radiation microdiffraction Biomacromolecules 5 2004 1316 1324 A microdrop generator is used to locally hydrate single starch granules. A fast hydration process with a half-time of about 7 sec is observed by time-resolved μ-XRD.
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(2004)
Biomacromolecules
, vol.5
, pp. 1316-1324
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Lemke, H.1
Burghammer, M.2
Flot, D.3
Roessle, M.4
Riekel, C.5
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48
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20444425185
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Combined microdrop generation and microdiffraction for biopolymer hydration experiments
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C. Riekel, M. Burghammer, D. Flot, and M. Rössle Combined microdrop generation and microdiffraction for biopolymer hydration experiments Fibre Diffr. Rev. 12 2004 36 40 Review of several microdrop experiments and discussion of instrumental features of a droplet-mixing set-up for turbulent mixing.
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(2004)
Fibre Diffr. Rev.
, vol.12
, pp. 36-40
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Riekel, C.1
Burghammer, M.2
Flot, D.3
Rössle, M.4
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49
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0346101649
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Trends in microfluidics with complex fluids
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T. Pfohl, F. Mugele, R. Seemann, and S. Herminghaus Trends in microfluidics with complex fluids Chem. Phys. Chem. 4 2003 1273 1274 Contains much useful information on microfluidic devices and applications. This group has studied the alignment of fibrous biopolymers in microfluidic channels by μ-SAXS.
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(2003)
Chem. Phys. Chem.
, vol.4
, pp. 1273-1274
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Pfohl, T.1
Mugele, F.2
Seemann, R.3
Herminghaus, S.4
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50
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0037150212
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Evaluation of a photon-counting hybrid pixel detector array with a synchrotron X-ray source
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C. Ponchut, J.L. Visschers, A. Fornaini, H. Graafsma, M. Maiorino, G. Mettivier, and D. Calvet Evaluation of a photon-counting hybrid pixel detector array with a synchrotron X-ray source NIM A 484 2002 396 406 Evaluation of a small pixel detector at ESRF. Large frame pixel detectors are developed notably at PSI (Switzerland) and Chess (USA).
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(2002)
NIM a
, vol.484
, pp. 396-406
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Ponchut, C.1
Visschers, J.L.2
Fornaini, A.3
Graafsma, H.4
Maiorino, M.5
Mettivier, G.6
Calvet, D.7
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51
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0011741685
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Time-resolved small-angle X-ray scattering combined with wide-angle X-ray scattering
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W. Bras, and T. Ryan Time-resolved small-angle X-ray scattering combined with wide-angle X-ray scattering J. Appl. Crystallogr. 30 1997 816 821
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(1997)
J. Appl. Crystallogr.
, vol.30
, pp. 816-821
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Bras, W.1
Ryan, T.2
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52
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13244289637
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Current limits of X-ray microdiffraction in soft condensed matter experiments
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C. Riekel Current limits of X-ray microdiffraction in soft condensed matter experiments Fibre Diffr. Rev. 2002 11 18 Discussion of resolution obtained in practice with pinhole μ-SAXS camera.
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(2002)
Fibre Diffr. Rev.
, pp. 11-18
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Riekel, C.1
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