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note
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Attempts to prepare F6T2 polyfluorene (2e, Table 1) under these conditions were unsuccessful due to the insoluble nature of this polymer.
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23
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12844269063
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note
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Details relating to the synthesis of the dibromoalkylter- and pentathiophene species described in this paper will be presented at a later date.
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24
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12844268370
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note
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The unusually high levels of residual bromine in polymers 6-8 may be a result of incomplete polymer endcapping reactions of the bromine end groups with phenylboronic acid.
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25
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0021093572
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12844264557
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note
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Analysis of residual inorganic species as determined by neutron activation analysis (NAA): Cl - 61 ppm, Na - 31 ppm, Br - 6.6 ppm, K - ND@ 1 ppm, Pd - 1.2 ppm.
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27
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12844285929
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note
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Dissolution of polymer 9 in these solvents required a short initial heating at 50-60°C.
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28
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The use of thermally removable solublizing groups in oligothiophenes has recently been described. See A. R. Murphy; J. M. J. Fréchet, P. Chang, J. Lee, and V. Subramanian, J. Am. Chem. Soc. 126, 1596, (2004).
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