Crystal engineering of acentric diamondoid metal-organic coordination networks

Angewandte Chemie - International Edition

Volumn 38, Issue 4, 1999, Pages 536-538

  Evans, Owen R ^a   Xiong, Ren Gen ^a   Wang, Zhiyong ^a   Wong, George K ^b   Lin, Wenbin ^a  

^a BRANDEIS UNIVERSITY   (United States)

^b HONG KONG UNIVERSITY OF SCIENCE AND TECHNOLOGY   (Hong Kong)

Author keywords

Coordination polymers; Crystal engineering; Network structures; Nonlinear optics; Solid state structures

Indexed keywords

CADMIUM DERIVATIVE; ZINC DERIVATIVE;

ARTICLE; CRYSTAL STRUCTURE; OPTICAL ROTATION; SOLID STATE; SYNTHESIS; THERMOSTABILITY;

EID: 0033558180     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1521-3773(19990215)38:4<536::AID-ANIE536>3.0.CO;2-3     Document Type: Article

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28. Kα radiation (λ = 0.71073 Å). Least-squares refinement based on 2034 reflections with I > 3σ(I) and 226 parameters led to convergence, with a final value of R = 0.039 and R, = 0.043. - Further details of the crystal structure investigation(s) can be obtained from the Fachinfor-mationszentrum Karlsruhe, D-76344 Eggenstein-Leopoldshafen, Germany (fax: (+49)7247-808-666; e-mail: crysdata@fiz-karlsruhe.de), on quoting the depository numbers CSD-391070 and CSD-391071.
29. 2(EtOH)][EtOH] adopts a centrosymmetric structure (space group Pbca, SHG-inactive) due to the twofold interpenetration: W. Lin, R. Xiong, O. Evans, Z. Wang, unpublished results.
30. Identical X-ray powder diffraction patterns were obtained for samples of 2 before and after the removal of water guest molecules.