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note
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2) = 1.027. CCDC-187412 and -187413 contains the supplementary crystallographic data for this paper. These data can be obtained free of charge via www.ccdc.cam.ac.uk/conts/retrieving.html (or from the Cambridge Crystallographic Data Centre, 12 Union Road, Cambridge CB21EZ, UK; fax: (+44) 1223-336-033; or deposit@ccdc.cam.ac.uk).
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25
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2242422112
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note
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max = 440 nm.
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26
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2242489420
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note
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1H NMR spectrum of the polymer is identified as arising from the end-group protons associated with the aromatic terminus. The integration of the peak at 7.47 ppm versus that at 7.32 ppm is 1:18. Assuming both ends of the polymer are capped by the iodo end group (as no acetylene proton resonance is observed in the NMR spectrum), this integration ratio gives the number of repeating units at 18.
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