Structural chemistry of halogenated monocarbaboranes: The extended structures of Cs[1-HCB9H4Br5], Cs[1-HCB 11H5Cl6] and Cs[1-HCB11H 5Br6]

New Journal of Chemistry

Volumn 28, Issue 12, 2004, Pages 1499-1505

  Franken, Andreas ^a   Bullen, Neil J ^a   Jelínek, Tomáš ^a   Thornton Pett, Mark ^a   Teat, Simon J ^b   Clegg, William ^b,c   Kennedy, John D ^a   Hardie, Michaele J ^a  

^a UNIVERSITY OF LEEDS   (United Kingdom)

^b DARESBURY LABORATORY   (United Kingdom)

^c NEWCASTLE UNIVERSITY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

ANION; BROMINE; CARBORANE DERIVATIVE; CESIUM; HALOCARBON;

ARTICLE; CHEMICAL STRUCTURE; CRYSTAL STRUCTURE; GEOMETRY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; PRIORITY JOURNAL; REACTION ANALYSIS; STRUCTURE ANALYSIS; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

EID: 11244267137     PISSN: 11440546     EISSN: None     Source Type: Journal    
DOI: 10.1039/b410929e     Document Type: Article

References (70)

1. For example: T. Onak, in Boron Hydride Chemistry, ed. E. L. Muetterties, Academic Press, New York, 1973, pp. 349-382.
2. For example: B. Štíbr, Chem. Rev., 1992, 92, 225.
3. (a) J. Plešek, T. Jelínek, B. Štíbr and S. Heřmánek, J. Chem. Soc., Chem. Commun., 1988, 348;
4. (b) J. Plešek, B. Štíbr, X. L. R. Fontaine, J. D. Kennedy, S. Heřmánek and T. Jelínek, Collect. Czech. Chem. Commun., 1991, 56, 1618;
5. (c) A. E. Wille, J. Plešek, J. Holub, B. Štíbr, P. J. Carrol and L. G. Sneddon, Inorg. Chem., 1996, 35, 5342.
6. W. H. Knoth, J. Am. Chem. Soc., 1967, 89, 1274.
7. (a) B. Brellochs, in Contemporary Boron Chemistry, ed. M. G. Davidson, A. K. Hughes, T. B. Marder and K. Wade, Royal Society of Chemistry, Cambridge, UK, 2000, pp. 212-214;
8. (b) B. Štíbr and B. Wrackmeyer, J. Organomet. Chem., 2002, 657, 3;
9. (c) A. Franken, C. A. Kilner, M. Thornton-Pett and J. D. Kennedy, Collect. Czech. Chem. Commun., 2002, 67, 869.
10. For example: (a) T. Jelínek, B. Štíbr, J. Plešek and S. Heřmánek, J. Organomet. Chem., 1986, 307, C13;
11. (b) J. A. Kautz, D. A. Kissounko, N. S. Kissounko and F. G. A. Stone, Organometallics, 2002, 21, 2547;
12. (c) D. Shaowu, A. Franken, P. A. Jelliss, J. A. Kautz, F. G. A. Stone and P.-Y. Yu, J. Chem. Soc., Dalton Trans., 2001, 1846;
13. (d) I. V. Pisareva, I. T. Chizhevsky, P. V. Petrovskii, V. I. Bregadze, F. M. Dolgushin and A. I. Yanovsky, Organometallics, 1997, 16, 5598.
14. A. S. Larsen, J. D. Holbrey, F. S. Tham and C. A. Reed, J. Am. Chem. Soc., 2000, 122, 7264.
15. P. Kaszynski, S. Pakhomov, K. F. Tesh and V. G. Young, Inorg. Chem., 2001, 40, 6622.
16. B. Grüner, Z. Janoušek, B. T. King, J. N. Woodford, C. H. Wang, V. Všetečka and J. Michl, J. Am. Chem. Soc., 1999, 121, 3122.
17. (a) A. Franken, B. T. King, J. Rudolph, P. Rao, P. C. Noll and J. Michl, Collect. Czech. Chem. Commun., 2001, 66, 1238;
18. (b) X. Yang, W. Jiang, C. B. Knobler and M. F. Hawthorne, J. Am. Chem. Soc., 1992, 114, 9719;
19. (c) J. Müller, K. Baše, T. F. Magnera and J. Michl, J. Am. Chem. Soc., 1992, 114, 9721;
20. (d) S. J. Cantrill, A. R. Pease and J. F. Stoddart, J. Chem. Soc., Dalton Trans., 2000, 3715.
21. (a) M. J. Hardie and C. L. Raston, Chem. Commun., 2001, 905;
22. (b) M. J. Hardie, N. Malic, B. Roberts and C. L. Raston, Chem. Commun., 2001, 865;
23. (c) A. Franken, C. A. Kilner, M. Thornton-Pett and J. D. Kennedy, Chem. Commun., 2002, 2048;
24. (d) S. I. Renard, A. Franken, C. A. Kilner, J. D. Kennedy and M. A. Halcrow, New J. Chem., 2002, 26, 1634.
25. (a) C. A. Reed, Acc. Chem. Res., 1998, 31, 133;
26. (b) S. H. Strauss, Chem. Rev., 1993, 93, 927.
27. For example: (a) B. T. King, Z. Janoušek, B. Grüner, M. Trammell, B. C. Noll and J. Michl, J. Am. Chem. Soc., 1996, 118, 3313;
28. (b) C. W. Tsang and Z. W. Xie, Chem. Commun., 2000, 1839;
29. (c) S. V. Ivanov, J. J. Rockwell, O. G. Polyakov, C. M. Gaudinski, O. P. Anderson, K. A. Solntsev and S. H. Strauss, J. Am. Chem. Soc., 1998, 120, 4224.
30. Z. W. Xie, C. W. Tsang, E. T. P. Sze, Q. C. Yang, D. T. W. Chan and T. C. W. Mak, Inorg. Chem., 1998, 37, 6444.
31. (a) H. W. Turner and G. G. Hlatky, Eur. Pat. Appl., 277003, 1988;
32. (b) H. W. Turner and G. G. Hlatky, US Pat., 5278119, 1994;
33. (c) H. W. Turner and G. G. Hlatky, US Pat., 5407884, 1995;
34. (d) H. W. Turner and G. G. Hlatky, US Pat., 5483014, 1996.
35. (a) Z. Xie, R. Bau and C. A. Reed, Angew. Chem., Int. Ed. Engl., 1994, 33, 2433;
36. (b) Z. Xie, J. Manning, R. W. Reed, R. Mathur, P. D. W. Boyd, A. Benesi and C. A. Reed, J. Am. Chem. Soc., 1996, 118, 2922;
37. (c) N. J. Patmore, M. F. Mahon, J. W. Steed and A. S. Weller, J. Chem. Soc., Dalton Trans., 2001, 277.
38. (a) C. A. Reed, N. L. P. Fackler, K.-C. Kim, D. Stasko, D. R. Evans, P. D. W. Boyd and C. E. F. Rickard, J. Am. Chem. Soc., 1999, 121, 6314;
39. (b) I. A. Koppel, P. Burk, I. Koppel, I. Leito, T. Sonoda and M. Mishima, J. Am. Chem. Soc., 2000, 122, 5114.
40. C.-W. Tsang, Q. Yang, E. Tung-Po Sze, T. C. W. Mak, D. T. W. Chan and Z. Xie, Inorg. Chem., 2000, 39, 5851.
41. N. J. Patmore, C. Hague, J. H. Cotgreave, M. F. Mahon, C. G. Frost and A. S. Weller, Chem. Eur. J., 2002, 8, 2088.
42. D. R. Evans and C. A. Reed, J. Am. Chem. Soc., 2000, 122, 4660.
43. N. J. Patmore, M. J. Ingleson, M. F. Mahon and A. S. Weller, Dalton Trans., 2003, 2894.
44. For example: (a) A. Wescott, N. Whitford and M. J. Hardie, Inorg. Chem., 2004, 43, 3663;
45. (b) N. J. Patmore, J. W. Steed and A. S. Weller, Chem. Commun., 2000, 1055;
46. (c) K. Shelly, D. C. Finster, Y. J. Lee, W. R. Scheidt and C. A. Reed, J. Am. Chem. Soc., 1985, 107, 5955.
47. J. Rais, J. Plesek, P. Selucky, M. Kyrs and L. Kadlecova, J. Radioanal. Nucl. Chem., 1991, 148, 349.
48. C.-W. Tsang, Q. Yang, E. Tung-Po Sze, T. C. W. Mak, D. T. W. Chan and Z. Xie, Inorg. Chem., 2000, 39, 3582.
49. T. Jelínek, P. Baldwin, W. R. Scheidt and C. A. Reed, Inorg. Chem., 1993, 32, 1982.
50. (a) R. Ahmad, A. Franken, J. D. Kennedy and M. J. Hardie, Chem. Eur. J., 2004, 10, 2190;
51. (b) R. Ahmad and M. J. Hardie, New J. Chem., 2004, 11, 1315.
52. For example: (a) M. A. Beckett, M. Bown, X. L. R. Fontaine, N. N. Greenwood, J. D. Kennedy and M. Thornton-Pett, J. Chem. Soc., Dalton Trans., 1988, 1969;
53. (b) G. Ferguson, J. D. Kennedy, X. L. R. Fontaine, Faridoon and T. R. Spalding, J. Chem. Soc., Dalton Trans., 1988, 2555;
54. (c) D. Reed, Chem. Soc. Rev., 1993, 22, 109;
55. (d) S. Heřmánek, Inorg. Chim. Acta, 1999, 289, 20.
56. J. D. Kennedy, Boron, in Multinuclear NMR, ed. J. Mason., Plenum, New York and London, 1987, ch. 8, pp. 221-254.
57. W. McFarlane, Proc. R. Soc. London, Ser. A, 1968, 306, 185.
58. T. Jelínek, J. Plešek, S. Heřmánek and B. Štíbr, Collect. Czech. Chem. Commun., 1986, 51, 819.
59. (a) Z. Xie, D. J. Liston, T. Jelínek, V. Mítro, R. Bau and C. A. Reed, J. Chem. Soc., Chem. Commun., 1993, 384;
60. (b) Z. Xie, T. Jelínek, R. Bau and C. A. Reed, J. Am. Chem. Soc., 1994, 116, 1907.
61. J. H. Morris and N. N. Greenwood, Proc. Chem. Soc., 1963, 388.
62. P. Cortona, Phys. Rev. B, 1992, 46, 2008.
63. + coordination-sphere geometry incorrectly reported as cuboctahedral in: M. Avdeev and V. Kharton, Mater. Res. Bull., 2002, 37, 735.
64. S. Uhrlandt, H. M. Artelt and G. Meyer, Z. Anorg. Allg. Chem., 1994, 620, 1532.
65. S. Loss and C. Roehr, Z. Naturforsch. B, 1998, 53, 75.
66. For example: (a) D. V. Domasevitch, J. A. Rusanova, O. Y. Vassilyeva, V. N. Kokozay, P. J. Squattrito, J. Sieler and P. R. Raithby, J. Chem. Soc., Dalton Trans., 1999, 3087;
67. (b) D. T. Rosa and D. Coucouvanis, Inorg. Chem., 1998, 37, 2328;
68. (c) T. G. Levitskaia, J. C. Bryan, R. A. Sachleben, J. D. Lamb and B. A. Moyer, J. Am. Chem. Soc., 2000, 122, 554;
69. (d) M. Cai, A. L. Marlow, J. C. Fettinger, D. Fabris, T. J. Haverlock, B. A. Moyer and J. T. Davis, Angew. Chem., Int. Ed., 2000, 39, 1283.
70. H. H. Schmidtke, Z. Naturforsch., 1964, 19a, 1502.