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Details are available in the Supporting Information
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Details are available in the Supporting Information.
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9
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note
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w = 0.0693 and GOF = 1.07. The methylene protons were observable in difference-electron density maps; positions were refined in the final model.
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13
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0344883061
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s symmetry (neglecting the methyl protons) consistent with the cyclohexadienyl structure: C(1)-C(2) 1.480, 1.473, 1.478 Å, C(2)-C(3) 1.358, 1.386, 1.377 Å, C(3)-C(4) 1.431, 1.428, 1.432 Å, respectively
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s symmetry (neglecting the methyl protons) consistent with the cyclohexadienyl structure: C(1)-C(2) 1.480, 1.473, 1.478 Å, C(2)-C(3) 1.358, 1.386, 1.377 Å, C(3)-C(4) 1.431, 1.428, 1.432 Å, respectively.
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