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3 = H, the unique proton shift ranged from 8.2 to 8.5 ppm and its corresponding carbon shift (C5) was close to 142 ppm. In the other cases, quaternary carbon shifts of triazole were observed between 150 and 156 ppm.
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4, and concentrated under reduced pressure. The resulting compound was purified by flash chromatography on silica gel to yield the expected 1,2,4-triazole derivative.
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