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note
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2O in a molar ratio of 1:5:3:2:555 under autogenous pressure at 160 °C for 4 days. After cooling to room temperature, the sapphire-colored tetra-prism crystals of 1 were isolated as a major phase (70% yield on Mo) from the pale-yellow slurry, then washed with distilled water, and dried at ambient temperature. The crystals were manually selected for structural determination and further characterization. Anal. Calcd for 1: C, 23.23; H, 1.60; N. 4.93; Cu, 11.18; Mo, 37.74 (%). Found: C, 22.07; H. 1.65; N, 4.91; Cu, 11.06; Mo, 37.82 (%). A summary of the crystallographic data and structural determination for compound 1 is provided in Table S1. Selected bond lengths and angles are listed in Table S2. CCDC-211193 contains the supplementary crystallographic data for this paper.
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