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Volumn 122, Issue 36, 2000, Pages 8789-8790

The first covalent organic-inorganic networks of hybrid chalcogenides: Structures that may lead to a new type of quantum wells [7]

Author keywords

[No Author keywords available]

Indexed keywords

CHALCOGEN; RESIN;

EID: 0034644434     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja002224n     Document Type: Letter
Times cited : (248)

References (44)
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    • note
    • 2O (0.595 g), Te (0.128 g) and pda (5 mL) in a mole ratio of 2:1:60 at 200 °C for 3 days (yield: 91.3%). A mixture of 0.0175 g I and II in 0.30 mL of pda sealed in an evacuated Pyrex tube was heated at 190 °C for 8 days and was converted completely to III; 0.0580 g of III in 5 mL of en solution reacted at 200 °C for 4 days resulted in a mixture of I and II, Thermogravimetric analyses of I-III were performed on a computer controlled TA Instrument 2050TGA analyzer, 23.498, 8.917, and 12.814 mg powder samples of I, II, and III, respectively, were loaded into alumina pans and heated with a ramp rate of 10 °C/min from room temperature to 410 °C. The residues were examined by powder X-ray diffraction immediately after the TGA experiment. The title compounds can also be obtained by heating ZnTe directly in en and pda at 200 °C for 3 days.
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    • max = 26.0 °) with I ≥ 2σ(I) yielding R1 = 0.0351, wR2 = 0.0716, GOF = 1.183.
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    • max = 26.0 °) with I ≥ 2σ(I) yielding R1 = 0.0495, wR2 = 0.0816, GOF = 1.345.
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    • max = 26.0 °) with I ≥ 2σ(I) yielding R1 = 0.0594, wR2 = 0.0750, GOF = 0.997.
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