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2O (0.595 g), Te (0.128 g) and pda (5 mL) in a mole ratio of 2:1:60 at 200 °C for 3 days (yield: 91.3%). A mixture of 0.0175 g I and II in 0.30 mL of pda sealed in an evacuated Pyrex tube was heated at 190 °C for 8 days and was converted completely to III; 0.0580 g of III in 5 mL of en solution reacted at 200 °C for 4 days resulted in a mixture of I and II, Thermogravimetric analyses of I-III were performed on a computer controlled TA Instrument 2050TGA analyzer, 23.498, 8.917, and 12.814 mg powder samples of I, II, and III, respectively, were loaded into alumina pans and heated with a ramp rate of 10 °C/min from room temperature to 410 °C. The residues were examined by powder X-ray diffraction immediately after the TGA experiment. The title compounds can also be obtained by heating ZnTe directly in en and pda at 200 °C for 3 days.
-
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26
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0342806290
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note
-
max = 26.0 °) with I ≥ 2σ(I) yielding R1 = 0.0351, wR2 = 0.0716, GOF = 1.183.
-
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-
-
29
-
-
0342806291
-
-
note
-
max = 26.0 °) with I ≥ 2σ(I) yielding R1 = 0.0495, wR2 = 0.0816, GOF = 1.345.
-
-
-
-
30
-
-
0342371363
-
-
note
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max = 26.0 °) with I ≥ 2σ(I) yielding R1 = 0.0594, wR2 = 0.0750, GOF = 0.997.
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31
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0343240876
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note
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