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note
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These estimates are lower limits, as small amounts of sodium in the spectra obscure and artificially inflate the starting material peak.
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note
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n. When n ≥ 2, the yield was less than 50%; when n = 6 or 10, coupled products were barely detectable. Therefore, the amide bonds were biased to form between amino and carboxyl groups on adjacent nucleotidyl residues.
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