Synthesis of 1,1′-diphospha[4]ferrocenophanes by molybdenum-catalyzed ring-closing metathesis

Organometallics

Volumn 22, Issue 6, 2003, Pages 1174-1176

  Ogasawara, Masamichi ^a   Nagano, Takashi ^a   Hayashi, Tamio ^a  

^a KYOTO UNIVERSITY   (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

DIPHOSPHAFERROCENOPHANES; LEWIS BASIC SUBSTRATES; RING CLOSING METATHESIS; SCHROCKS MOLYBDENUM CARBENE;

ALKALINITY; CATALYSIS; CATALYSTS; ISOMERS; MOLYBDENUM COMPOUNDS; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SUBSTRATES; SYNTHESIS (CHEMICAL);

PHOSPHORUS COMPOUNDS;

EID: 0037451210     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om021058k     Document Type: Article

References (24)

1. Locke, A. J.; Jones, C.; Richard, C. J. J. Organomet. Chem. 2001, 637-639, 669.
2. Schwab, P.; Grubbs, R. H.; Ziller, J. W. J. Am. Chem. Soc. 1996, 118, 100.
3. (b) Scholl, M.; Ding, S.; Lee, C. W.; Grubbs, R. H. Org. Lett. 1999, 1, 953.
4. Ogasawara, M.; Nagano, T.; Hayashi, T. J. Am. Chem. Soc. 2002, 124, 9068
5. Ogasawara, M.; Nagano, T.; Hayashi, T. J. Am. Chem. Soc. 2002, 124, 12626.
6. Hüerländer, D.; Kleigrewe, N.; Kehr, G.; Erker, G.; Fröhlich, R. Eur. J. Inorg. Chem. 2002, 2633.
7. Recently preparation of 1,1'-diphospha[2]ferrocenophane was reported, see: Deschamps, E.; Ricard, L.; Mathey, F. Organometallics 2001, 20, 1499.
8. Schrock, R. R.; Murdzek, J. S.; Bazan, G. C.; Robbins, J.; Di Mare, M.; O'Regan, M. J. Am. Chem. Soc. 1990, 112, 3875.
9. For RCM reactions of phosphorus-containing compounds, see: (a) Leconte, M.; Jourdan, I.; Pagano, S.; Lefebvre, F.; Basset, J.-M. J. Chem. Soc., Chem. Commun. 1995, 857.
10. (b) Leconte, M.; Pagano, S.; Mutch, A.; Lefebvre, F.; Basset, J.-M. Bull. Soc. Chim. Fr. 1995, 132, 1069.
11. (c) Hanson, P. R.; Stoianova, D. S. Tetrahedron Lett. 1998, 39, 3939.
12. (d) Bujard, M.; Gouverneur, V.; Mioskowski, C. J. Org. Chem. 1999, 64, 2119.
13. (e) Hanson, P. R.; Stoianova, D. S. Tetrahedron Lett. 1999, 40, 3297.
14. (f) Trevitt, M.; Gouverneur, V. Tetrahedron Lett. 1999, 40, 7333.
15. (g) Hetherington, L.; Greedy, B.; Gouveneur, V. Tetrahedron 2000, 56, 2053.
16. (h) Schuman, M.; Trevitt, M.; Redd, A.; Gouverneur, V. Angew. Chem., Int. Ed. 2000, 39, 2491.
17. Douglas, T.; Theopold, K. H. Angew. Chem., Int. Ed. Engl. 1989, 28, 8, 1367.
18. (b) Westerhausen, M.; Digeser, J. H.; Gückel, C.; Nöth, H.; Knizek, J.; Ponikwar, W. Organometallics 1999, 18, 2491.
19. (c) Sava, X.; Mézailles, N.; Maigrot, N.; Nief, F.; Ricard, L.; Mathey, F.; Le Floch, P. Organometallics 1999, 18, 4205.
20. (d) Sava, X.; Ricard, L.; Mathey, F.; Le Floch, P. Organometallics 2000, 19, 4899.
21. Fagan, P. J.; Nugent, W. A. J. Am. Chem. Soc. 1988, 110, 2310.
22. (b) Fagan, P. J.; Nugent, W. A.; Calabrese, J. C. J. Am. Chem. Soc. 1994, 116, 1880.
23. Dias, E. L.; Nguyen, S. T.; Grubbs, R. H. J. Am. Chem. Soc. 1997, 119, 3887.
24. 3. Data were collected on a Rigaku AFC7S diffractometer with graphite-monochromated Mo Kα radiation (λ = 0.71069 Å). Full details of the crystallographic analysis are described in the Supporting Information.