The titanocene complex of bis(trimethylsilyl)acetylene: Synthesis, structure, and chemistry

Organometallics

Volumn 22, Issue 5, 2003, Pages 884-900

  Rosenthal, Uwe ^a   Burlakov, Vladimir V ^a,b   Arndt, Perdita ^a   Baumann, Wolfgang ^a   Spannenberg, Anke ^a  

^a UNIVERSITY OF ROSTOCK   (Germany)

^b A N NESMEYANOV INSTITUTE OF ORGANOELEMENT COMPOUNDS   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

COMPLEXATION; CRYSTALS; MAGNESIUM PRINTING PLATES; NUCLEAR MAGNETIC RESONANCE; REDUCTION; SPECTROSCOPIC ANALYSIS; SUBLIMATION; X RAY CRYSTALLOGRAPHY;

ELECTRON DELOCALIZATION;

TITANIUM COMPOUNDS;

EID: 0037416345     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om0208570     Document Type: Review

References (161)

1. (a) Levitin, I.; Shur, V. B. Inorg. Chim. Acta 1997, 254, 203.
2. (b) Levitin, I. Inorg. Chim. Acta 1999, 285, 15.
3. (c) Leigh, G. Chem. Eur. J. 1997, 3, 332.
4. (d) Vol'pin, M. E.; Koreshkov, Yu. D.; Kursanov, D. N. Izv. Akad. Nauk SSSR, Ser. Khim. 1961, 1355.
5. (e) Vol'pin, M. E.; Koreshkov, Yu. D.; Dulova, V. G.; Kursanov, D. N. Tetrahedron 1962, 18, 107.
6. (a) Johnson, F.; Gohlke, R. S.; Nasutavicus, W. H. J. Organomet. Chem. 1965, 3, 233.
7. (b) West, R.; Bailey, R. E. J. Am. Chem. Soc. 1963, 85, 2871.
8. (c) Bokii, N. G.; Struchkov, Yu. T. J. Struct. Chem. USSR (Engl. Transl.) 1965, 6, 548.
9. (a) Conlin, R. T.; Gaspar, P. P. J. Am. Chem. Soc. 1976, 98, 3715.
10. (b) Seyferth, D.; Annarelli, D. C.; Vick, S. C. J. Am. Chem. Soc. 1976, 98, 6832.
11. (a) Vol'pin, M. E.; Dubovitsky, V. A.; Nogina, O. V.; Kursanov, D. N. Dokl. Akad. Nauk SSSR 1963, 151, 1100.
12. (b) Shur, V. B.; Bernadyuk, S. Z.; Burlakov, V. V.; Vol'pin, M. E. II-nd All-Union Conf. Organomet. Chem., Gorky, 1982, 178.
13. (c) Shur, V. B.; Burlakov, V. V.; Vol'pin, M. E. J. Organomet. Chem. 1988, 347, 77.
14. Cohen, S. A.; Bercaw, J. E. Organometallics 1985, 4, 1006.
15. (a) Rosenthal, U.; Schulz, W. J. Organomet. Chem. 1987, 321, 103.
16. (b) Rosenthal, U.; Görls, H. J. Organomet. Chem. 1988, 348, 135.
17. (c) Rosenthal, U.; Oehme, G.; Burlakov, V. V.; Petrovskii, P. V.; Shur, V. B.; Vol'pin, M. E. J. Organomet. Chem. 1990, 391, 119.
18. (d) Rosenthal, U.; Nauck, C.; Arndt, P.; Pulst, S.; Baumann, W.; Burlakov, V. V.; Görls, H. J. Organomet. Chem. 1994, 484, 81 and references therein.
19. Rosenthal, U.; Schulz, W. Z. Anorg. Allg. Chem. 1987, 550, 169.
20. (a) Burlakov, V. V.; Rosenthal, U.; Petrovskii, P. V.; Shur, V. B.; Vol'pin, M. E. Organomet. Chem. USSR 1988, 1, 526.
21. -3, 5851 reflections measured, 3192 reflections independent of symmetry, 2209 observed reflections (I > 2σ(I)), R1 = 0.050, wR2 (all data) = 0.114, 187 parameters.
22. Burlakov, V. V.; Rosenthal, U.; Beckhaus, R.; Struohkov, Yu. T.; Oehme, G.; Shur, V. B.; Vol'pin, M. E. Organomet. Chem. USSR 1990, 3, 237.
23. (a) Rosenthal, U.; Görls, H.; Burlakov, V. V.; Shur, V. B.; Vol'pin, M. E. J. Organomet. Chem. 1992, 426, C53.
24. (b) Burlakov, V. V.; Polyakov, A. V.; Yanovsky, A. I.; Struchkov, Y. T.; Shur, V. B.; Vol'pin, M. E.; Rosenthal, U.; Görls, H. J. Organomet. Chem. 1994, 476, 197.
25. Lefeber, C.; Ohff, A.; Tillack, A.; Baumann, W.; Kempe, R.; Burlakov, V. V.; Rosenthal, U.; Görls, H. J. Organomet. Chem. 1995, 501, 179.
26. (a) Bruckmann, J.; Krüger, C. Acta Crystallogr., Sect. C, 1997, 53, 1845.
27. (b) Zanin, I. E.; Antipin, M. Yu.; Struchkov, Yu. T. Kristallografiya 1991, 36, 411.
28. Allen, F. H.; Kennard, O.; Watson, D. G.; Brammer, L.; Orpen, A. G.; Taylor, R. J. Chem. Soc., Perkin Trans. 2 1987, S1.
29. Lefeber, C.; Baumann, W.; Tillack, A.; Görls, H.; Rosenthal, U. Organometallics 1996, 15, 3486.
30. (a) Rosenthal, U.; Ohff, A.; Michalik, M.; Görls, H.; Burlakov, V. V.; Shur, V. B. Angew. Chem., Int. Ed. Engl. 1993, 32, 1193.
31. (b) Rosenthal, U.; Ohff, A.; Baumann, W.; Tillack, A.; Görls, H.; Burlakov, V. V.; Shur, V. B. Z. Anorg. Allg. Chem. 1995, 621, 77.
32. (c) Nitschke, J. R.; Zürcher, S.; Tilley, T. D. J. Am. Chem. Soc. 2000, 122, 10345.
33. (d) Rosenthal, U.; Ohff, A.; Baumann, W.; Tillack, A.; Görls, H.; Burlakov, V. V.; Shur, V. B. J. Organomet. Chem. 1994, 484, 203.
34. (a) McDade, C.; Bercaw, J. E. J. Organomet. Chem. 1985, 279, 281.
35. (b) Lamaire, S. J. Ph.D. Thesis, Chemistry Department, Massachusetts Institute of Technology, 1989.
36. (c) Threlkel, R. S. Ph.D. Thesis, California Institute of Technology, 1980.
37. Hiller, J.; Thewalt, U.; Polasek, M.; Petrusova, L.; Varga, V.; Sedmera, P.; Mach, K. Organometallics 1996, 15, 3752.
38. (a) List, A. K.; Koo, K.; Rheingold, A. L.; Hillhouse, G. L. Inorg. Chim. Acta 1998, 270, 399.
39. (b) Pellny, P.-M.; Burlakov, V. V.; Baumann, W.; Spannenberg, A.; Rosenthal, U. Z. Anorg. Allg. Chem. 1999, 625, 910.
40. (a) Peulecke, N.; Lefeber, C.; Ohff, A.; Baumann, W.; Tillack, A.; Kempe, R.; Burlakov, V. V.; Rosenthal, U. Chem. Ber. 1996, 129, 959.
41. (b) Peulecke, N.; Baumann, W.; Kempe, R.; Burlakov, V. V.; Rosenthal, U. Eur. J. Inorg. Chem. 1998, 419.
42. (c) Kempe, R.; Spannenberg, A.; Peulecke, N.; Rosenthal, U. Z. Kristallogr. 1998, 213, 629.
43. (a) Kupfer, V.; Thewalt, U.; Tislerova, I.; Stepnicka, P.; Gyepes, R.; Kubista, J.; Horacek, M.; Mach, K. J. Organomet. Chem. 2001, 620, 39.
44. (b) Varga, V.; Hiller, J.; Gyepes, R.; Polasek, M.; Sedmera, P.; Thewalt, U.; Mach, K. J. Organomet. Chem. 1997, 538, 63.
45. (c) Schmid, G.; Thewalt, U.; Polasek, M.; Mach, K.; Sedmera, P. J. Organomet. Chem. 1994, 482, 231.
46. (d) Horacek, M.; Stepnicka, P.; Kubista, J.; Gyepes, R.; Cisarova, I.; Petrusova, L.; Mach, K. J. Organomet. Chem. 2002, 658, 235.
47. (e) Horacek, M.; Stepnicka, P.; Gentil, S.; Fejfarova, K.; Kubista, J.; Pirio, N.; Meunier, P.; Gallou, F.; Paquette, L. A.; Mach, K. J. Organomet. Chem. 2002, 656, 81.
48. (f) Varga, V.; Mach, K.; Hiller, J.; Thewalt, U.; Sedmera, P.; Polasek, M. Organometallics 1995, 14, 1410.
49. (a) Horacek, M.; Hiller, J.; Stepnicka, P.; Mach, K. J. Organomet. Chem. 1998, 571, 77.
50. (b) Varga, V.; Mach, K.; Schmid, G.; Thewalt, U. J. Organomet. Chem. 1993, 454, C1.
51. (c) Varga, V.; Mach, K.; Schmid, G.; Thewalt, U. J. Organomet. Chem. 1994, 475, 127.
52. (d) Hiller, J.; Thewalt, U.; Podlaha, J.; Hanus, V.; Mach, K. Collect. Czech. Chem. Commun. 1997, 62, 1551.
53. (a) Negishi, E.; Takahashi, T. Aldrichim. Acta 1985, 18, 31.
54. (b) Nugent, W. A.; Thorn, D. L.; Harlow, R. L. J. Am. Chem. Soc. 1987, 109, 2788.
55. (c) Negishi, E. Acc. Chem. Res. 1987, 20, 65.
56. (d) Buchwald, S. L.; Nielsen, R. B. Chem. Rev. 1988, 88, 1047.
57. (e) Negishi, E.; Takahashi, T. Synthesis 1988, 1.
58. (f) Buchwald, S. L.; Fisher, R. A. Chim. Scr. 1989, 29, 417.
59. (g) Negishi, E. Chim. Scr. 1989, 29, 457.
60. (h) Erker, G. Angew. Chem., Int. Ed. Engl. 1989, 28, 397.
61. (i) Buchwald, S. L.; Broene, R. D. Science 1993, 1696.
62. (j) Negishi, E.; Takahashi, T. Acc. Chem. Res. 1994, 27, 124.
63. (k) Hanzawa, Y.; Ito, H.; Taguchi, T. Synlett 1995, 299.
64. (l) Maier, E. L. Nachr. Chem. Technol. Lab. 1993, 41, 811.
65. (m) Negishi, E.; Takahashi, T. Bull. Chim. Soc. Jpn. 1998, 71, 755.
66. (n) Beckhaus, R. Nachr. Chem. Technol. Lab. 1998, 46, 611.
67. (o) Negishi, E.; Montchamp, J.-L.: Zirconocenes. In Metallocenes: Synthesis, Reactivity, Applications; Togni, A., Halterman, R. L., Eds.; Wiley-VCH: Weinheim, Germany, 1998; Vol. 1, p 241.
68. (p) Backhaus, R.: Titanocenes. In Metallocenes: Synthesis, Reactivity, Applications; Togni, A., Halterman, R. L., Eds.; Wiley-VCH: Weinheim, Germany, 1998; Vol. 1, p 153.
69. (q) Negishi, E.; Huo, S. Synthesis and Reactivity of Zirconocene Derivatives. In Titanium and Zirconium in Organic Synthesis; Marek, I., Ed.; Wiley-VCH: Weinheim, Germany, 2002; p 1.
70. (r) Takahashi, T.; Li, Y. Zirconacyclopentadienes in Organic Synthesis. In Titanium and Zirconium in Organic Synthesis; Marek, I., Ed.; Wiley-VCH: Weinheim, Germany, 2002; p 50.
71. Fagan, P. J.; Nugent, W. A. J. Am. Chem. Soc. 1988, 110, 2310.
72. Van Wagenen, B. C.; Livinghouse, T. Tetrahedron Lett. 1989, 30, 3495.
73. (a) Horacek, M.; Kupfer, V.; Thewalt, U.; Stepnicka, P.; Polasek, M.; Mach, K. Organometallics 1999, 18, 3572.
74. (b) Lukesova, L.; Horacek, M.; Stepnicka, P.; Fejfarova, K.; Gyepes, R.; Cisarova, I.; Kubista, J.; Mach, K. J. Organomet. Chem. 2002, 663, 134.
75. Hitchcock, P. B.; Kerton, F. M.; Lawless, G. A. J. Am. Chem. Soc. 1998, 120, 10264.
76. Horacek, M.; Hiller, J.; Polasek, M.; Mach, K. Organometallics 1997, 16, 4185.
77. Varga, V.; Mach, K.; Polasek, M.; Sedmera, P.; Hiller, J.; Thewalt, U.; Troyanov, S. I. J. Organomet. Chem. 1996, 506, 241.
78. (a) Ohff, A.; Pulst, S.; Peulecke, N.; Arndt, P.; Burlakov, V. V.; Rosenthal, U. Synlett 1996, 111.
79. (b) Rosenthal, U.; Pellny, P.-M.; Kirchbauer, F. G.; Burlakov, V. V. Acc. Chem. Res. 2000, 33, 119.
80. (c) Rosenthal, U.; Burlakov, V. V. Organometallic Chemistry of Titanocene and Zirconocene Complexes with Bis(trimethylsilyl)acetylene as the Basis for Applications in Organic Synthesis. In Titanium and Zirconium in Organic Synthesis; Marek, I., Ed.; Wiley-VCH: Weinheim, Germany, 2002; p 355.
81. (d) Rosenthal, U.; Burlakov, V. V.; Arndt, P.; Baumann, W.; Spannenberg, A. J. Organomet. Chem., in press.
82. Rosenthal, U.; Lefeber, C.; Arndt, P.; Tillack, A.; Baumann, W.; Kempe, R.; Burlakov, V. V. J. Organomet. Chem. 1995, 503, 221.
83. Tillack, A.; Baumann, W.; Ohff, A.; Lefeber, C.; Spannenberg, A.; Rosenthal, U. J. Organomet. Chem. 1996, 520, 187.
84. Thomas, D.; Peulecke, N.; Burlakov, V. V.; Heller, B.; Baumann, W.; Spannenberg, A.; Kempe, R.; Rosenthal, U.; Backhaus, R. Z. Anorg. Allg. Chem. 1998, 624, 919.
85. (a) Ohff, A.; Kosse, P.; Baumann, W.; Tillack, A.; Kempe, R.; Görls, H.; Burlakov, V. V.; Rosenthal, U. J. Am. Chem. Soc. 1995, 117, 10399.
86. (b) Peulecke, N.; Ohff, A.; Kosse, P.; Tillack, A.; Kempe, R.; Spannenberg, A.; Baumann, W.; Burlakov, V. V.; Rosenthal, U. Chem. Eur. J. 1998, 4, 1852.
87. (a) Low, P. J.; Bruce, M. I. Adv. Organomet. Chem. 2002, 48, 71.
88. (b) Lotz, S.; Van Rooyen, H.; Meyer, R. Adv. Organomet. Chem. 1995, 37, 219.
89. (c) Manna, J.; John, K. D.; Hopkins, M. D. Adv. Organomet. Chem. 1995, 38, 79.
90. (d) Choukroun, R.; Cassoux, P. Acc. Chem. Res. 1999, 32, 494.
91. (e) Lang, H.; Weinmann, M. Synlett 1996, 1.
92. (f) Lang, H.; Rheinwald, G. J. Prakt. Chem. 1999, 341, 1.
93. (g) Lang, H.; George, D. S. A.; Rheinwald, G. Coord. Chem. Rev. 2000, 206-207, 102.
94. (a) Rosenthal, U.; Ohff, A.; Tillack, A.; Baumann, W.; Görls, H. J. Organomet. Chem. 1994, 468, C4.
95. (b) Rosenthal, U.; Pulst, S.; Arndt, P.; Ohff, A.; Tillack, A.; Baumann, W.; Kempe, R.; Burlakov, V. V. Organometallics 1994, 14, 2961.
96. (a) Burlakov, V. V.; Ohff, A.; Lefeber, C.; Tillack, A.; Baumann, W.; Kempe, R.; Rosenthal, U. Chem. Ber. 1998, 128, 967.
97. (b) Burlakov, V. V.; Peulecke, N.; Baumann, W.; Spannenberg, A.; Kempe, R.; Rosenthal, U. J. Organomet. Chem. 1997, 536-537, 293.
98. Wittig, G. Angew, Chem., Int. Ed. Engl. 1962, 1, 415.
99. (a) Pavankumar, P. N. V.; Jemmis, E. D. J. Am. Chem. Soc. 1988, 110, 125.
100. (b) Jemmis, E. D.; Giju, K. T. J. Am. Chem. Soc. 1998, 120, 6952.
101. (a) Pellny, P.-M.; Burlakov, V. V.; Peulecke, N.; Baumann, W.; Spannenberg, A.; Kempe, R.; Francke, V.; Rosenthal, U. J. Organomet. Chem. 1999, 578, 125.
102. (b) Jemmis, E. D.; Phukan, A. K.; Rosenthal, U. J. Organomet. Chem. 2001, 635, 204.
103. (c) Jemmis, E. D.; Phukan, A. K.; Giju, A. T. Organometallics 2002, 21, 2254.
104. Rosenthal, U.; Görls, H. J. Organomet. Chem. 1992, 439, C 36.
105. Jemmis, E. D.; Giju, K. T. Angew. Chem., Int. Ed. Engl. 1997, 36, 606.
106. Pellny, P.-M.; Peulecke, N.; Burlakov, V. V.; Tillack, A.; Baumann, W.; Spannenberg, A.; Kempe, R.; Rosenthal, U. Angew. Chem., Int. Ed. 1997, 36, 2615.
107. (a) Pellny, P.-M.; Peulecke, N.; Burlakov, V. V.; Baumann, W.; Spannenberg, A.; Rosenthal, U. Organometallics 2000, 19, 1198.
108. (b) Horacek, M.; Bazyakina, N.; Stepnicka, P.; Gyepes, R.; Cisarova, I.; Bredeua, S.; Meunier, P.; Kubista, J.; Mach, K. J. Organomet. Chem. 2001, 628, 30.
109. (c) Takahashi, T.; Xi, Z.; Obora, Y.; Suzuki, N. J. Am. Chem. Soc. 1995, 117, 2665.
110. (d) Xi, Z.; Fischer, R.; Hara, R.; Sun, W.-H.; Obora, Y.; Suzuki, N.; Takahashi, T. J. Am. Chem. Soc. 1997, 119, 12842.
111. Pellny, P.-M.; Burlakov, V. V.; Baumann, W.; Spannenberg, A.; Kempe, R.; Rosenthal, U. Organometallics 1999, 18, 2906.
112. Kempe, R.; Spannenberg, A.; Peulecke, N.; Rosenthal, U. Z. Kristallogr, 1998, 213, 425.
113. Lefeber, C.; Arndt, P.; Tillack, A.; Baumann, W.; Kempe, R.; Burlakov, V. V.; Rosenthal, U. Organometallics 1995, 14, 3090.
114. (a) Ohff, A.; Zippel, T.; Arndt, P.; Spannenberg, A.; Kempe, R.; Rosenthal, U. Organometallics 1998, 17, 1649.
115. (b) Zippel, T.; Arndt, P.; Ohff, A.; Kempe, R.; Rosenthal, U. Organometallics 1998, 17, 4429.
116. Tillack, A.; Arndt, P.; Spannenberg, A.; Kempe, R.; Rosenthal, U. Z. Anorg. Allg. Chem. 1998, 624, 737.
117. Tillack, A.; Arndt, P.; Spannenberg, A.; Kempe, R.; Zippel, T.; Rosenthal, U. Z. Anorg. Allg. Chem. 1998, 624, 2038.
118. (a) Burlakov, V. V.; Rosenthal, U.; Yanovsky, A. I.; Struchkov, Yu. T.; Ellert, O. G.; Shur, V. B.; Vol'pin, M. E. Organomet. Chem. USSR 1989, 2, 1193.
119. (b) Burlakov, V. V.; Yanovsky, A. I.; Struchkov, Yu. T.; Shur, V. B.; Ellert, O. G.; Rosenthal, U. J. Organomet. Chem. 1997, 542, 105 and references therein.
120. (c) Demerseman, B.; Mahe, R.; Dixneuf, P. H. J. Chem. Soc., Chem. Commun. 1984, 1394.
121. Arndt, P.; Lefeber, C.; Tillack, A.; Rosenthal, U. Chem. Ber. 1996, 129, 1281.
122. (a) Witte, P.; Klein, R.; Kooijman, H.; Spek, A. L.; Polasek, M.; Varga, V.; Mach, K. J. Organomet. Chem. 1996, 519, 195.
123. (b) Gyepes, R.; Horacek, M.; Cisarova, I.; Mach, K. J. Organomet. Chem. 1998, 551, 207.
124. Arndt, P.; Spannenberg, A.; Baumann, W.; Becke, S.; Rosenthal, U. Eur. J. Inorg. Chem. 2001, 2885.
125. (a) Ohff, A.; Kempe, R.; Baumann, W.; Rosenthal, U. J. Organomet. Chem. 1996, 520, 241.
126. (b) Ohff, A.; Kempe, R.; Baumann, W.; Rosenthal, U. J. Organomet. Chem. 1997, 532, 281.
127. (a) Burlakov, V. V.; Troyanov, S. I.; Letov, A. V.; Mysov, E. I.; Furin, G. G.; Shur, V. B. Izv. Akad. Nauk, Ser. Khim. 1999, 1022; Russ. Chem. Bull. (Engl. Transl.) 1999, 48, 1012.
128. (a) Burlakov, V. V.; Troyanov, S. I.; Letov, A. V.; Mysov, E. I.; Furin, G. G.; Shur, V. B. Izv. Akad. Nauk, Ser. Khim. 1999, 1022; Russ. Chem. Bull. (Engl. Transl.) 1999, 48, 1012.
129. (b) Burlakov, V. V.; Troyanov, S. I.; Letov, A. V.; Strunkina, L. I.; Minacheva, M. Kh.; Furin, G. G.; Rosenthal, U.; Shur, V. B. J. Organomet. Chem. 2000, 598, 243.
130. Burlakov, V. V.; Arndt, P.; Baumann, W.; Spannenberg, A.; Rosenthal, U.; Letov, A. V.; Lyssenko, K. A.; Korlyukov, A. A.; Strunkina, L. I.; Minacheva, M. Kh.; Shur, V. B. Organometallics 2001, 19, 4072.
131. Burlakov, V. V.; Usatov, A. V.; Lyssenko, K. A.; Antipin, M. Yu.; Novikov, Yu. N.; Shur, V. B. Eur. J. Inorg. Chem. 1999, 1855.
132. Ohff, A.; Burlakov, V. V.; Rosenthal, U. J. Mol. Catal. 1996, 108, 119.
133. (a) Varga, V.; Petrusova, L.; Cejka, J.; Hanus, V.; Mach, K. J. Organomet. Chem. 1996, 509, 235.
134. (b) Stepnicka, P.; Gyepes, R.; Cisarova, I.; Horacek, M.; Kubista, J.; Mach, K. Organometallics 1999, 18, 4869 and references therein.
135. Ohff, A.; Burlakov, V. V.; Rosenthal, U. J. Mol. Catal. 1996, 105, 103.
136. (a) Kirchbauer, F. G.; Pulst, S.; Heller, B.; Baumann, W.; Rosenthal, U. Angew. Chem., Int. Ed. 1998, 37, 1925.
137. (b) Pulst, S.; Arndt, P.; Heller, B.; Baumann, W.; Kempe, R.; Rosenthal, U. Angew. Chem., Int. Ed. Engl. 1996, 35, 1112.
138. Tillack, A.; Lefeber, C.; Peulecke, N.; Thomas, D.; Rosenthal, U. Tetrahedron Lett. 1997, 35, 1533.
139. (a) Aitken, C.; Harrod, J. F.; Samuel, E. J. Organomet. Chem. 1985, 279, C11-C13.
140. (b) Aitken, C.; Barry, J. P.; Gauvin, F.; Harrod, J. F.; Malek, A.; Rousseau, D. Organometallics 1989, 8, 1732 and references therein.
141. (a) Peulecke, N.; Thomas, D.; Baumann, W.; Fischer, C.; Rosenthal, U. Tetrahedron Lett. 1997, 38, 6655.
142. (b) Lunzer, F.; Marschner, C.; Winkler, B.; Peulecke, N.; Baumann, W.; Rosenthal, U. Monatsh. Chem. 1999, 130, 215.
143. (a) Arndt, P.; Thomas, D.; Rosenthal, U. Tetrahedron Lett. 1997, 38, 5467.
144. (b) Thomas, D.; Arndt, P.; Peulecke, N.; Spannenberg, A.; Kempe, R.; Rosenthal, U. Eur. J. Inorg. Chem. 1998, 1351.
145. Peulecke, N. Ph.D. Thesis, University of Rostock, 1997.
146. Tillack, A.; Castro, I. G.; Hartung, C. G.; Beller, M. Angew. Chem., Int. Ed. 2002, 114, 2646.
147. (a) Rao, M. N. S.; Roesky, H. W.; Anantharaman, G. J. Organomet. Chem. 2002, 646, 2.
148. (b) Cui, C.; Köpke, S.; Herbst-Irmer, E.; Roesky, H. W.; Noltemeyer, M.; Schmidt, H.-G.; Wrackmeyer, B. J. Am. Chem. Soc. 2001, 123, 9091.
149. (a) Gordon, M. S.; Boudjouk, Anwari, F. J. Am. Chem. Soc. 1983, 105, 4972.
150. (b) Göller, A.; Heydt, H.; Clark, T. J. Org. Chem. 1996, 61, 5840.
151. (c) Göller, A.; Clark, T. J. Mol. Model. 2000, 6, 133.
152. (a) Seyferth, D.; Duncan, D. P.; Vick, S. C. J. Organomet. Chem. 1977, 125, C5.
153. (b) Seyferth, D.; Vick, S. C.; Shannon, M. L.; Lim, T. F. O.; Duncan, D. P. J. Organomet. Chem. 1977, 135, C37.
154. (c) Seyferth, D.; Vick, S. C.; Shannon, M. L. Organometallics 1994, 3, 1897.
155. (a) Gasper, P. P.; Beatty, A. M.; Chen, T.; Haile, T.; Lei, D.; Winchester, W. R.; Braddock-Wilking, J.; Rath, N. P.; Klooster, W. T.; Koetzle, T. F.; Mason, S. A.; Albinati, A. Organometallics 1999, 18, 3921.
156. (b) Ishikawa, M.; Fuchikami, T.; Kumada, M. J. Am. Chem. Soc. 1977, 99, 245.
157. Kunai, A.; Mihara, T.; Matsuo, Y.; Oshita, J.; Naka, A.; Ishikawa, M. J. Organomet. Chem. 1997, 545-546, 611.
158. (a) Weidenbruch, M. J. Organomet. Chem. 2002, 646, 39.
159. (b) Kirmaier, L.; Weidenbruch, M.; Marsmann, H.; Peters, K.; von Schnering, H. G. Organometallics 1998, 17, 1237.
160. (c) Ostendorf, D.; Kirmeier, L.; Saak, W.; Marsmann, H.; Weidenbruch, M. Eur. J. Inorg. Chem. 1999, 2301.
161. (d) Ostendorf, D.; Saak, W.; Weidenbruch, M.; Marsmann, H. Organometallics 2000, 19, 4938.