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a) F. Palacios, A. M. Ochoa de Retana, J. I. Gil, and R. López de Munain, Org. Lett., 2002, 4, 2405.
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d) F. Palacios, A. M. Ochoa de Retana, and J. Oyarzabal, Heterocycles, 1998, 47, 517.
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0032546064
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0037136171
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a) F. Palacios, A. M. Ochoa de Retana, S. Pascual, and R. López de Munain. Tetrahedron, 2002, 58, 5917.
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0033525796
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b) F. Palacios, A. M. Ochoa de Retana, and J. Oyarzabal, Tetrahedron, 1999, 55, 3091.
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0030575347
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F. Palacios, D. Aparicio, and J. García, Tetrahedron, 1996, 52, 9609.
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Palacios, F.1
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34
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0012407093
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note
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26NOP: C. 80.52, H. 5.86, N. 3.13. Found: C. 80.45, H. 5.80, N. 3.16.
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35
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0012406758
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note
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General Procedure for the preparation of quinoline (4a)from N-arylimine (1a). A solution of a mixture of diphenyl 3-p-tolyl-2-(p-tolylimino)propyldiphenylphosphine oxide (85%) and 2-(p-tolylamino)-3-p-tolyl-1-propenylphosphine oxide (15%) (2.19 g, 5 mmol) and 1.03 mL of DMF-DEA (6 mmol) in toluene (15 mL) was stirred under reflux until TLC indicated the disappearance of imine/enamine (48 h). The mixture was then concentrated under vacuum and the crude residue was purified by flash column chromatography eluting with AcOEt/hexanes (3: 1).
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36
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0030972057
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F. Palacios, C. Alonso, and G. Rubiales, J. Org. Chem., 1997, 62, 1146.
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J. Org. Chem.
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Palacios, F.1
Alonso, C.2
Rubiales, G.3
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37
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0012469191
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note
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3 (15 mL) was stirred under reflux overnight. Solvent was evaporated under vacuum and diluted in toluene. DMF-DEA (1.03 mL, 6 mmol) was then added and the mixture was stirred under reflux until the completation of the reaction (2-3 d.). The mixture was then concentrated under vacuum and the crude residue was purified by flash column chromatography eluting with AcOEt/hexanes (3:1).
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38
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0034697180
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V. Aucagne, D. Gueyrard, A. Tatibouët, A. Quinsac, and P. Rollin, Tetrahedron, 2000, 56, 2647.
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Tetrahedron
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Aucagne, V.1
Gueyrard, D.2
Tatibouët, A.3
Quinsac, A.4
Rollin, P.5
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39
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0012406759
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note
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General Procedure for the preparation of quinolines (4) from N-arylamines (2) and 2-oxoalkyl phosphonates (6). A solution of diethyl 2-oxo-3-phenylpropylphosphonate (6) (1.35 g, 5 mmol) and N-arylamine (2) (5 mmol) in toluene (15 mL) was stirred under reflux with a Dean-Stark. After 3 h. the reaction was cooled to rt and DMF-DEA (1.03 mL, 6 mmol) was then added. The mixture was stirred under reflux until the completation of the reaction (2-3 d). The mixture was then concentrated under vacuum and the crude residue was purified by flash column chromatography eluting with AcOEt/hexanes (2:1).
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41
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0035477535
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b) J. Xiang, S. Toyoshima, and A. Orita, J. Otera, Angew. Chem., Int. Ed., 2001, 40, 3670.
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Angew. Chem., Int. Ed.
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Xiang, J.1
Toyoshima, S.2
Orita, A.3
Otera, J.4
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42
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0000298098
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a) F. Palacios, A. M. Ochoa de Retana, J. Oyarzabal, and S. Pascual, Org. Lett., 2002, 4, 769.
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43
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0037155508
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b) F. Palacios, C. Alonso, P. Amezua, and G. Rubiales, J. Org. Chem., 2002, 67, 1941.
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Palacios, F.1
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Amezua, P.3
Rubiales, G.4
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44
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0035831985
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c) F. Palacios, D. Aparicio, J. García, E. Rodríguez, and A. Fernández-Acebes, Tetrahedron, 2001, 57, 3131.
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(2001)
Tetrahedron
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Palacios, F.1
Aparicio, D.2
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Rodríguez, E.4
Fernández-Acebes, A.5
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45
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0035439209
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d) F. Palacios, M. Legido, I. Perez de Heredia, J. M. Ezpeleta, and G. Rubiales, Heterocycles, 2001, 55, 1641.
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Heterocycles
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Palacios, F.1
Legido, M.2
Perez de Heredia, I.3
Ezpeleta, J.M.4
Rubiales, G.5
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46
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0012445157
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note
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20NCl: C. 81.18, H. 5.45, N. 3.79. Found: C. 81.24, H. 5.41, N. 3.82.
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