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0442263465
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note
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Standard reaction conditions: 1 mmol of aryl chloride, 1.5 mmol of olefin, 1.2 mmol of sodium acetate, catalyst (0.5 mol %), and 2 g of tetrabutylammonium bromide were stirred under argon at 140°C for 24 h in a Schlenk tube. After the mixture was cooled, the internal standard (diethyleneglycol di-n-butyl ether) was added, and the mixture was diluted with 5 mL of water and extracted with 3 × 5 mL of ether. The combined organic layers were dried over sodium sulfate. The conversion and the yield were determined by gas chromatography.
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