N-(2-mercaptoethyl)picolylamine as a diaminomonothiolate ligand for the "fac-[Re(Co)3]+" core

Inorganic Chemistry

Volumn 41, Issue 24, 2002, Pages 6181-6183

  Kramer, Daniel J ^a   Davison, Alan ^a   Davis, William M ^a   Jones, Alun G ^b  

^a MASSACHUSETTS INSTITUTE OF TECHNOLOGY   (United States)

^b HARVARD MEDICAL SCHOOL   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

CYSTEAMINE DERIVATIVE; DIAMINE DERIVATIVE; LIGAND; N (2 MERCAPTOETHYL)PICOLYLAMINE; N-(2-MERCAPTOETHYL)PICOLYLAMINE; RADIOPHARMACEUTICAL AGENT; RHENIUM; SULFUR DERIVATIVE; TECHNETIUM 99M; TECHNETIUM COMPLEX; UNCLASSIFIED DRUG;

ARTICLE; BINDING SITE; CATALYSIS; CHEMICAL ANALYSIS; CHEMICAL REACTION; CHEMICAL STRUCTURE; CHEMISTRY; CONFORMATION; CRYSTAL STRUCTURE; DERIVATIZATION; LIGAND BINDING; REACTION ANALYSIS; SYNTHESIS; X RAY CRYSTALLOGRAPHY;

BINDING SITES; CATALYSIS; CRYSTALLOGRAPHY, X-RAY; LIGANDS; MERCAPTOETHYLAMINES; MOLECULAR CONFORMATION; MOLECULAR STRUCTURE; ORGANOTECHNETIUM COMPOUNDS; RADIOPHARMACEUTICALS; SULFUR COMPOUNDS;

EID: 0037010962     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic025887+     Document Type: Article

References (22)

1. Johannsen, B.; Spies, H. Top. Curr. Chem. 1996, 176, 77.
2. Abrams, M. J.; Davison, A.; Jones, A. G.; Costello, C. E.; Pang, H. Inorg. Chem. 1983, 22, 2798.
3. Alberto, R.; Schibli, R.; Egli, A.; Schubiger, P. A.; Herrmann, W. A.; Artus, G.; Abram, U.; Kaden, T. A. J. Organomet. Chem. 1995, 493, 119.
4. Alberto, R.; Schibli, R.; Egli, A.; Schubiger, A. P.; Abram, U.; Kaden, T. A. J. Am. Chem. Soc. 1998, 120, 7987.
5. Alberto, R.; Schibli, R.; Schubiger, P. A.; Abram, U.; Pietzsch, H.-J.; Johannsen, B. J. Am. Chem. Soc. 1999, 121, 6076.
6. Schibli, R.; Bella, R. L.; Alberto, R.; Garcia-Garayoa, E.; Ortner, K.; Abram, U.; Schubiger, P. A. Bioconjugate Chem. 2000, 11, 345.
7. Pietzsch, H.-J.; Gupta, A.; Reisgys, M.; Drews, A.; Seifert, S.; Syhre, R.; Spies, H.; Alberto, R.; Abram, U.; Schubiger, P. A.; Johannsen, B. Bioconjugate Chem. 2000, 11, 414.
8. Schibli, R.; Alberto, R.; Abram, U.; Abram, S.; Egli, A.; Schubiger, P. A.; Kaden, T. A. Inorg. Chem. 1998, 37, 3509.
9. Kramer, D. J.: Davison, A.; Jones, A. G. Inorg. Chim. Acta 2001, 312, 215.
10. Brand, U.; Vahrenkamp, H. Inorg. Chem. 1995, 34, 3285.
11. Alberto, R.; Schibli, R.; Waibel, R.; Abram, U.; Schubiger, P. A. Coord. Chem. Rev. 1999, 190-192, 901.
12. Alberto, R.; Schibli, R.; Abram, U.; Egli, A.; Knapp, F. F.; Schubiger, P. A. Radiochim. Acta 1997, 79, 99.
13. Meltzer, P. C.; Blundell, P.; Jones, A. G.; Mahmood, A.; Garada, B.; Zimmerman, R. E.; Davison, A.; Holman, B. L.; Madras, B. K. J. Med. Chem. 1997, 40. 1835.
14. Friebe, M.; Mahmood, A.; Bolzati. C.; Drews, A.; Johannsen. B.; Eisenhut, M.; Kramer, D.; Davison, A.; Jones, A. G. J. Med. Chem. 2001, 44, 3132.
15. Brenner, D.; Davison, A.; Lister-James, J.; Jones, A. G. Inorg. Chem. 1984, 23, 3793.
16. Egli, A.; Hegetschweiler, K.; Alberto, R.; Abram, U.; Schibli, R.; Hedinger, R.; Gramlich, V.; Kissner, R.; Schubiger, P. A. Organometallics 1997, 16, 1833.
17. Alberto, R.; Egli, A.; Abram. U.; Hegetschweiler, K.; Gramlich, V.; Schubiger, P. A. J. Chem. Soc., Dalton Trans. 1994, 2815.
18. 2, and the final refinement gave R1 = 0.0516 and wR2 = 0.0990 (1 > 2σ), and R1 = 0.0621 and wR2 = 0.1024 (all data), by using 3891 data per 326 parameters.
19. Alberto, R.; Schibli, R.; Angst, D.; Schubiger, P. A.; Abram, U.; Abram, S.; Kaden, T. A. Transition Met. Chem. 1997, 22, 597.
20. Leung, W.-H.; Hun, T. S. M.: Fung, S.; Williams, I. D.; Wong, K.-Y. Polyhedron 1997, 16, 3641.
21. Wong, Y.-L.: Dilworth, J. R. J. Chem. Soc., Dalton Trans. 2002, 2366.
22. 2, and the final refinement gave R1 = 0.0428 and wR2 = 0.1060 (1 > 2σ), and R1 = 0.0438 and wR2 = 0.1070 (all data), by using 1921 data per 183 parameters.