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31P NMR analysis was used to monitor reaction progress.
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67
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This is consistent with the RCM studies reported by Lee and co-workers, who report that the Grubbs benzylidene catalyst 3 is relatively ineffective for catalyzing RCM in the presence of the sulfide functionality, see: Shon, Y.-S.; Lee, T. R. Tetrahedron Lett. 1997, 38, 1283-1286.
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note
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Additional supporting information is available for all compounds upon request.
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