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23
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0034658143
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We have recently learned that Professor Nicolaou's group has determined the absolute configuration of 1 which is consistent with our own conclusion. Nicolaou, K. C.; Jung, J.-K.; Yoon, W. H.; He, Y.; Zhong, Y.-L.; Baran, P. S. Angew. Chem., Int. Ed. 2000, 39, 1829.
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0343625589
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note
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A detailed procedure for the preparation of this compound is described in Supporting Information.
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0001080242
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0343625588
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note
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In preliminary studies we found that the aldehyde 7b, which was derived from L-malic acid (S-configuration), formed a matched pair with 6.
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32
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0342755361
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note
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In the absence of pyridine, an acid-catalyzed double bond isomerization occurred to give a small amount of the unreactive 1,3-diene isomer.
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33
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0343190008
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note
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NOEs between H-9 and H-12, H-12 and H-16, H-17 and H-26, respectively, were observed.
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34
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0030813175
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Shaughnessy, E.A.4
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