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Volumn 65, Issue 1, 2000, Pages 176-185

Asymmetric synthesis of α-amino acids based on carbon radical addition to glyoxylic oxime ether

Author keywords

[No Author keywords available]

Indexed keywords

ALPHA AMINO ACID; ETHER DERIVATIVE; GLYOXYLIC ACID DERIVATIVE;

EID: 0033966817     PISSN: 00223263     EISSN: None     Source Type: Journal    
DOI: 10.1021/jo991353n     Document Type: Article
Times cited : (158)

References (126)
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    • For selected examples, see: (a) Murakata, M.; Jono, T.; Mizuno, Y.; Hoshino, O. J. Am. Chem. Soc. 1997, 119, 11713-11714. (b) Mase, N.; Watanabe, Y.; Ueno, Y.; Toru, T. J. Org. Chem. 1997, 62, 7794- 7800. (c) Braslau, R.; Burrill, L. C., II; Mahal, L. K.; Wedeking, T. Angew. Chem., Int. Ed. Engl. 1997, 36, 237-238. (d) Hanessian, S.; Yang, H.; Schaum, R. J. Am. Chem. Soc. 1996, 118, 2507-2508. (e) Badone, D.; Bernassau, J.-M.; Cardamone, R.; Guzzi, U. Angew. Chem., Int. Ed. Engl. 1996, 35, 535-537. (f) Nagano, H.; Azuma, Y. Chem. Lett. 1996, 845-846. (g) Urabe, H.; Yamashita, K.; Suzuki, K.; Kobayashi, K.; Sato, F. J. Org. Chem. 1995, 60, 3576-3577. (h) Kündig, E. P.; Xu, L.-H.; Romanens, P. Tetrahedron Lett. 1995, 36, 4047-4050. (i) Yamamoto, Y.; Onuki, S.; Yumoto, M.; Asao, N. J. Am. Chem. Soc. 1994, 116, 421-422. (j) Hamon, D. P. G.; Massy-Westropp, R. A.; Razzino, P. Tetrahedron 1993, 49, 6419-6428. (k) Morikawa, T.; Washio, Y.; Shiro, M.; Taguchi, T. Chem. Lett. 1993, 249-250. Hart, D. J.; Krishnamurthy, R. J. Org. Chem. 1992, 57, 4457-4470. (m) Beckwith, A. L. J.; Hersperger, R.; White, J. M. J. Chem. Soc., Chem. Commun. 1991, 1151-1152.
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    • For a related example, high 1,3-stereoinduction in radical additions to cyclic imines has recently been reported. See: (a) Bertrand, M. P.; Feray, L.; Nouguier, R.; Stella, L. Synlett 1998, 780-782. (b) Bertrand, M. P.; Feray, L.; Nouguier, R.; Perfetti, P. Synlett 1999, 1148-1150.
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    • For a related example, high 1,3-stereoinduction in radical additions to cyclic imines has recently been reported. See: (a) Bertrand, M. P.; Feray, L.; Nouguier, R.; Stella, L. Synlett 1998, 780-782. (b) Bertrand, M. P.; Feray, L.; Nouguier, R.; Perfetti, P. Synlett 1999, 1148-1150.
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    • note
    • Glyoxylic oxime ether 1 was prepared by the treatment of commercially available methyl 2-hydroxy-2-methoxyacetate with benzyloxyamine hydrochloride in the presence of sodium acetate in methanol. Oxime ether 1 was obtained as a single E isomer with respect to the geometry of the oxime ether group. See: ref 15b.
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    • note
    • 3B, reacted with i-PrI to generate an isopropyl radical. (2) The isopropyl radical then intermolecularly attacked glyoxylic oxime ether 1 to afford the intermediate benzyloxyaminyl radical as shown in Figure 1.
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    • (1992) J. Am. Chem. Soc. , vol.114 , pp. 5900-5902
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    • Oppolzer, W.1    Bienaymé, H.2    Genevois-Borella, A.3
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    • (1997) J. Am. Chem. Soc. , vol.119 , pp. 8379-8380
    • Mish, M.R.1    Guerra, F.M.2    Carreira, E.M.3
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    • (1997) Tetrahedron Lett. , vol.38 , pp. 2825-2828
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    • (1995) J. Org. Chem. , vol.60 , pp. 2271-2273
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    • For selected examples, see: (a) Jezewski, A.; Chajewska, K.; Wielogórski, Z.; Jurczak, J. Tetrahedron: Asymmetry 1997, 8, 1741-1749. (b) Bauer, T. Tetrahedron: Asymmetry 1996, 7, 981-984. (c) Bauer, T.; Chapuis, C.; Jezewski, A.; Kozak, J.; Jurczak, J. Tetrahedron: Asymmetry 1996, 7, 1391-1404.
    • (1997) Tetrahedron: Asymmetry , vol.8 , pp. 1741-1749
    • Jezewski, A.1    Chajewska, K.2    Wielogórski, Z.3    Jurczak, J.4
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    • For selected examples, see: (a) Jezewski, A.; Chajewska, K.; Wielogórski, Z.; Jurczak, J. Tetrahedron: Asymmetry 1997, 8, 1741- 1749. (b) Bauer, T. Tetrahedron: Asymmetry 1996, 7, 981-984. (c) Bauer, T.; Chapuis, C.; Jezewski, A.; Kozak, J.; Jurczak, J. Tetrahedron: Asymmetry 1996, 7, 1391-1404.
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    • (1996) Tetrahedron: Asymmetry , vol.7 , pp. 1391-1404
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    • note
    • 3B is required. See: ref 17b.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.