Electroactive 3'-(N-phenylpyrazolyl)isoxazoline [4',5': 1,2] [60] fullerene dyads

Tetrahedron Letters

Volumn 40, Issue 26, 1999, Pages 4889-4892

  De La Cruz, Pilar ^a   Espildora, Eva ^a   García, José J ^a   De La Hoz, Antonio ^a   Langa, Fernando ^a   Martín, Nazario ^b   Sánchez, Luis ^b  

^a UNIVERSITY OF CASTILLA LA MANCHA   (Spain)

^b UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

Author keywords

Cyclic Voltammetry; Cycloadditions; Fullerenes; Isuxazole; Microwave Healing; Pyrazole

Indexed keywords

BENZENE DERIVATIVE; FULLERENE DERIVATIVE; ISOXAZOLINE DERIVATIVE; PYRAZOLE DERIVATIVE;

ARTICLE; CALCULATION; CHEMICAL REACTION; MICROWAVE RADIATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POTENTIOMETRY; SYNTHESIS; THERMAL ANALYSIS;

EID: 0033603303     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(99)00904-1     Document Type: Article

References (25)

1. Martín, N.; Sánchez, L.; Illescas, B.; Pérez, I. Chem. Rev. 1998, 98, 2527-2548.
2. Echegoyen, L.E.; Echegoyen, L. Ace. Chem. Res. 1998, 31, 593-601.
3. 60-based electron acceptor organofullerenes in "Recent Advances in the Chemistry and Physics of Fullerenes Ond Related Materials"; Kadish, K. M.; Ruoff, R. S. Eds.; Vol. 6 (August 1998) pp. 1127-1145.
4. Hummelen, J.C.; Knight, B.; Pavlovich, J.; González, R.; Wudl, F. Science, 1995, 269, 1554-1556.
5. Knight, B.; Martín, N.; Ohno, T.; Ortí, E.; Rovira, C.; Veciana, J.; Vidal-Gancedo, J.; Viruela, P.M.; Viruela, R.; Wudl, F. J. Am. Chem. Soc. 1997, 119, 9871-9882 and references cited therein.
6. da Ros, T.; Prato, M.; Carano, M.; Ceroni, F.; Paolucci, F.; Roffia, F. J. Am. Chem. Soc. 1998, 120, 11645-11648.
7. de la Cruz, F.; Díaz-Ortiz, A.; García, J.J.; Gómez-Escalonilla, M.J.; de la Hoz, A.; Langa, F. Tetrahedron Lett. 1998, 40, 1587-1590.
8. Talukdar, S.; Pradhan, P.; Banerji, A. Full. Sci. & Techn. 1997, 5, 547.
9. Matsubara, Y.; Tada, H.; Nagase, S.; Yoshida, Z. J. Org. Chem. 1995, 60, 5372-5373.
10. 60 (50 mg, 0.07 mmol) were added. The mixture was irradiated in a focused microwave reactor (Maxidigest MX350, from Prolabo) at 210 W for 10 min.
11. de la Cruz, P.; de la Hoz, A.; Langa, F.; Illescas, B.; Martín, N. Tetrahedron 1997, 53, 2599-2608.
12. Langa, F.; de la Cruz, P.; de la Hoz, A.; Diez-Barra, E.; Diaz-Ortiz, A. Contemporary Org. Synth. 1997, 373-386.
13. max (log ε) 317 (6.56), 426 (5.29), 458 (5.18), 675 (4.25), 685 (4.34) nm
14. The polarizability of a solvent is connected with the index of refraction (n) according to the equation of Lorenz-Lorentz. Reichardt Ch, "Solvents and Solvents Effects in Organic Chemistry", VCH, Weinheim, 1990.
15. Bondi, A. J. Phys. Chem. 1964, 64, 441-451.
16. a) Meier, M.S.; Poplawska, M. J. Org. Chem. 1993, 58, 4524-525;
17. b) Irngartinger, H.; Köhler, C-M.; Huber-Patz, U.; Krästchmer, W. Chem. Ber. 1994, 127, 581-584;
18. c) Irngartinger, H.; Weber, A. Tetrahedron Lett. 1996, 37, 4137-4140;
19. d) Ohno, M.; Yashiro, A.; Eguchi, S. Synlett 1996, 815-816;
20. e) Irngartinger, H.; Weber, A.; Escher, T. Liebigs Ann. 1996, 1845-1850;
21. f) Irngartinger, H.; Weber, A. Tetrahedron Lett. 1997, 38, 2075-2076;
22. g) Da Ros, T.; Prato, M.; Novello, F.; Maggini, M.; de Amici, M.; de Micheli, C. Chem. Commun. 1997, 59-60.
23. Meier, M.S.; Poplawska, M. Tetrahedron 1996, 52, 5043-5052.
24. Williams, RM.; Zwier, J.M.; Verhoeven, J.W. J. Am. Chem. Soc. 1995, 117, 4093-4097.
25. Seshadri, R; D'souza, F.; Krishnan, V.; Rao, C.N.R. Chem. Lett. 1993, 217-218.