Synthesis of new C60-donor dyads by reaction of pyrazolylhydrazones with [60]fullerene under microwave irradiation

Tetrahedron Letters

Volumn 40, Issue 8, 1999, Pages 1587-1590

  De La Cruz, Pilar ^a   Díaz Ortiz, Angel ^a   García, José J ^a   Gómez Escalonilla, María J ^a   De La Hoz, Antonio ^a   Langa, Fernando ^a  

^a UNIVERSITY OF CASTILLA LA MANCHA   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

FULLERENE DERIVATIVE; HYDRAZONE DERIVATIVE; PYRAZOLONE DERIVATIVE;

ARTICLE; ELECTRON TRANSPORT; MICROWAVE IRRADIATION; SYNTHESIS;

EID: 0033582725     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(98)02651-3     Document Type: Article

References (20)

1. Martin, N.; Seoane, C. Handbook of Organic Conductive Molecules and Polymers; Vol.1 Ed. H.S. Nalwa. John Wiley & Sons 1997. Pg 1-86.
2. a) Williams, R.M.; Koeberg, M.; Lawson, J.M.; An, Y.; Rubin, Y.; Paddon-Row, M.N.; Verhoeven, J.W. J. Am. Chem. Soc. 1996, 118, 5055.
3. b) Liddell, P.A.; Kuciauskas. D.; Sumida, J. P.; Nash, B.; Nguyen, D.; Moore, A.L.; Moore, A.; Devens, G. J. Am. Chem. Soc. 1997, 119, 1400.
4. c) Diekers, M.; Hirch, A.; Pyo, S.; Rivera, J.; Echegoyen, L. Eur. J. Org. Chem. 1998, 1111 and references therein.
5. a) Crane, J.D.; Hitchcock, P.B.; Kroto, H.W.; Taylor, R.; Walton D. R. J. Chem. Soc., Chem. Commun. 1992, 1764.
6. b) Izuoka, A.; Tachikawa, T.; Sugawara, T.; Suzuki, Y.; Konno, M.; Saito, Y.; Shinohara, M. J. Chem. Soc., Chem. Commun. 1992, 1472.
7. c) Alam, M.M.; Watanabe, A.; Ito, O. J. Photochem. Photobiol. A. 1997, 104, 59.
8. d) Alam, M.M.; Watanabe, A.; Ito, O. Bull. Chem. Soc. Japan 1997, 70, 1833. Diekers, M.; Hirch, A.; Pyo, Soomi.; Rivera, J.; Echegoyen, L. Eur. J. Org. Chem. 1998, 1111 and references therein.
9. d) Alam, M.M.; Watanabe, A.; Ito, O. Bull. Chem. Soc. Japan 1997, 70, 1833. Diekers, M.; Hirch, A.; Pyo, Soomi.; Rivera, J.; Echegoyen, L. Eur. J. Org. Chem. 1998, 1111 and references therein.
10. Matsubara, Y.; Tada, H.; Nagase, S.; Yoshida, Z. J. Org. Chem. 1995, 60, 5372.
11. Arrieta, A.; Carrillo, J. R.; Cossio, F. P.; Diaz-Ortiz, A.; Gomez-Escalonilla, M.J.; de la Hoz, A.; Langa, F.; Moreno, A. Tetrahedron 1998, 54, 13167.
12. Trichlorobenzene, 210 W, 120 min.
13. a) Muthu, S.; Maruthamuthu, P.; Ragunathan, R.; Vasudeva, P.R.; Mathews, C.K. Tetrahedron Lett. 1994, 35, 1763.
14. b) Matsubara, Y.; Muraoka, H.; Tada, H.; Yoshida, Z. Chem. Lett. 1996, 373.
15. 3) δ (ppm): 8.22 (s, 1H), 8.20 (d, J=9.1 Hz, 2H), 8.03 (s, 1H), 7.94 (s, 1H), 7.83 (s, 1H), 7.74 (d, J=8.1 Hz, 2H), 7.50 (dd, J=8.1 Hz, J=7.7 Hz, 2H), 7.37 (t, J=7.7 Hz, 1H), 7.10 (d, J=9.1 Hz, 2H).
16. Finar, I.L.; Lord, G.H. J. Org. Chem. 1957, 3314.
17. Maxidigest MX-350 from Prolabo.
18. 12): 257, 328, 424, 488.
19. Talukdar, S.; Pradhan, P.; Banerji, A. Fullerene Sci. & Techno. 1997, 5, 547.
20. Langa, F. Unpublished results.