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The resonance at g = 9.3 is detected only at 4.0 K.
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As explained by R. Aasa, T. Vännegard, J. Magn. Reson. 1975, 9, 308-315, the intensity of the spectrum was multiplied by the temperature. The new spectrum so obtained presents also a peak at g = 7.5. The area under this peak decreased with the temperature. Care was taken to avoid saturation conditions.
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2en: N,N′-dimethyl-N,N′-bis(2-pyridylmethyl)ethane-1,2-diamine.
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