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Compound 1 has been previously reported: P. R. Ashton, A. N. Collins, M. C. T. Fyfe, P. T. Glink, S. Menzer, J. F. Stoddart, D. J. Williams, Angew. Chem. 1997, 109, 59-62;
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22
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33646111020
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note
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[10] The lower association constant for 1:1 complex 4(5) may be attributed to the reduced accessibility and flexibility of the macrocyclic moiety of 4 due to the bulky dendritic substituent.
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23
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37049088218
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a) Z. Xu, M. Kahr, K. L. Walker, C. L. Wilkins, J. S. Moore, J. Am. Chem. Soc. 1994, 116, 4537-4550;
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27
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33847502058
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-2 M) was mixed with 1/3 mol equiv of solid 1 for 3 d. The mixture was then filtered and the filtrate was concentrated to afford a white solid, which was submitted for MALDI-MS analysis
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-2 M) was mixed with 1/3 mol equiv of solid 1 for 3 d. The mixture was then filtered and the filtrate was concentrated to afford a white solid, which was submitted for MALDI-MS analysis.
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28
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0000656279
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e) to minimize fragmentation. For reviews on characterization of hydrogen-bonded assemblies by ESI-MS, see: a) K. C. Russell, E. Leize, A. Van Dorsselaer, J.-M. Lehn, Angew. Chem. 1995, 107, 244-248;
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