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The dimethyl acetals of acetaldehyde and acetone are commercially available. All others were prepared from the respective carbonyl compounds following standard procedures (methanol, trimethyl orthoformate, acid).
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The secondary amine in compound 3b should be more nucleophilic than benzylamine itself and hence might lead to the formation of the tertiary amine 4c. However, in the mass spectrum of 46 only traces of m/z = 400 could be detected. (formula presented)
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