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41
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85037498230
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note
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The amount of leaching was determined by AA and ICPMS.
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42
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85037495182
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note
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The effect of the polymer surface area on catalysis was examined by comparing the RCM results of the catalyst precursor 5 in fine powder and small segment (ca. 0.2(cm) × 0.2(cm) × 0.2(cm)) forms. When the fine powder form of 5 was used in the RCM of 7, the reaction was complete in 30 rain (Table 1, entry 5). The same reaction after 5 h yielded only 77% product when the small solid pieces of 5 were used.
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43
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85037506299
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note
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For references on use of CuCl as phosphine sponge, see ref 2c.
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