Effect of sample moisture content on XRD-estimated cellulose crystallinity index and crystallite size

Cellulose

Volumn 24, Issue 5, 2017, Pages 1971-1984

  Agarwal, Umesh P ^a   Ralph, Sally A ^a   Baez, Carlos ^a   Reiner, Richard S ^a   Verrill, Steve P ^a  

^a FOREST PRODUCTS LABORATORY   (United States)

Author keywords

Cellulose; Crystallinity; Crystallite size; Moisture; X ray diffraction

Indexed keywords

CELLULOSE; CHROMIUM COMPOUNDS; CRYSTALLITE SIZE; MOISTURE; MOISTURE DETERMINATION; OVENS; SODIUM HYDROXIDE; X RAY DIFFRACTION;

ABSOLUTE INTENSITY; CELLULOSE CRYSTALLINITY INDICES; CELLULOSE MATERIALS; CELLULOSE-CONTAINING MATERIALS; CRYSTALLINITIES; CRYSTALLINITY INDEX; LOBLOLLY PINE WOOD; NON-PARAMETRIC STATISTICAL TESTS;

WOOD;

CELLULOSE; CRYSTALLINITY; MOISTURE CONTENT; PINUS TAEDA;

EID: 85015707067     PISSN: 09690239     EISSN: 1572882X     Source Type: Journal    
DOI: 10.1007/s10570-017-1259-0     Document Type: Article

References (58)

1. Abe K, Yamamoto H (2005) Mechanical interaction between cellulose microfibril and matrix substance in wood cell wall determination by X-ray diffraction. J Wood Sci 51:334–338
2. Abe K, Yamamoto H (2006) Change in mechanical interaction between cellulose microfibril and matrix substance in wood cell wall induced by hygrothermal treatment. J Wood Sci 52:107–110
3. Agarwal UP (2016) Evolution of wood-cellulose native structure upon thermal and hydrothermal Treatments. CELL Division Abstract # 202, ACS, 251st meeting, San Diego
4. Agarwal UP, Reiner RS, Ralph SA (2010) Cellulose I crystallinity determination using FT–Raman spectroscopy: univariate and multivariate methods. Cellulose 17:721–733
5. Agarwal UP, Reiner RS, Ralph SA (2013) Estimation of cellulose crystallinity of lignocelluloses using near-IR FT–Raman spectroscopy and comparison of the Raman and Segal-WAXS methods. J Agric Food Chem 61:103–113
6. Agarwal UP, Ralph SA, Reiner RS, Moore RK, Baez C (2014) Impacts of fiber orientation and milling on observed crystallinity in jack pine. Wood Sci Technol 48:213–1227
7. Agarwal UP, Ralph SA, Reiner RS, Baez C (2016) Probing crystallinity of never-dried wood cellulose with Raman spectroscopy. Cellulose 23:125–144
8. Ahvenainen P, Kontro I, Svedstrom K (2016) Comparison of sample crystallinity determination methods by X-ray diffraction for challenging cellulose I materials. Cellulose 23:1073–1086
9. Armstrong RC, Wolfram C, de Jong KP, Gross R, Lewis NS, Boardman B, Ragauskas AJ, Ehrhardt-Martinez K, Crabtree G, Ramana MV (2016) The frontiers of energy. Nat Energy 1:15020
10. Astley OM, Chanliaud E, Donald AM, Gidley MJ (2001) Structure of acetobacter cellulose composites in the hydrated state. Int J Biol Macromol 29:193–202
11. Atalla RH, Whitmore RE (1978) The influence of elevated temperatures on structures in the isolation of native cellulose. J Poly Sci Poly Lett Ed 16:601405
12. Atalla RS, Crowley MF, Himmel ME, Atalla RH (2014) Irreversible transformations of native celluloses, upon exposure to elevated temperatures. Carbohydr Poly 100:2–8
13. Awa K, Shinzawa H, Ozaki Y (2014) An effect of cellulose crystallinity on the moisture absorbability of a pharmaceutical tablet studied by near-infrared spectroscopy. Appl Spectrosc 68:625–632
14. Barnette AL, Lee C, Bradley LC, Schreiner EP, Park YB, Shin H, Cosgrove DJ, Park S, Kim SH (2012) Quantification of crystalline cellulose in lignocellulosic biomass using sum frequency generation (SFG) vibration spectroscopy and comparison with other analytical methods. Carbohydr Poly 89:802–809
15. Bertran MS, Dale BE (1986) Determination of cellulose accessibility by differential scanning calorimetry. J Appl Poly Sci 32:4241–4253
16. Davis MW (1998) A rapid method for compositional carbohydrate analysis of lignocellulosics by high pH anion-exchange chromatography with pulse amperometric detection (HPAE/PAD). J Wood Chem Technol 18:235–252
17. Driemeier C, Bragatto J (2013) Crystallite width determines monolayer Hydration across a wide spectrum of celluloses isolated from plants. J Phys Chem B 117:415–421
18. Eichhorn SJ (2011) Cellulose nanowhiskers: promising materials for advanced applications. Soft Matter 7:303–315
19. Fang L, Catchmark JM (2014) Structure characterization of native cellulose during dehydration and rehydration. Cellulose 21:3951–3963
20. Favier V, Chanzy H, Cavaille JY (1995) Polymer nanocomposites reinforced by cellulose whiskers. Macromolecules 28:6365–6367
21. Fink HP, Purz HJ, Bohn A, Kunze J (1997) Investigation of the supramolecular structure of never dried bacterial cellulose. J Macromol Symp 120:207–217
22. French AD, Santiago Cintrón M (2013) Cellulose polymorphy, crystallite size, and the Segal crystallinity index. Cellulose 20:583–588
23. Hill SJ, Kirby NM, Mudie ST, Hawley AM, Ingham B, Franich RA, Newman RH (2010) Effect of drying and rewetting of wood on cellulose molecular packing. Holzforschung 64:421–427
24. Hollander M, Wolfe DA, Chicken E (2014) Nonparametric statistical methods, 3rd edn. Wiley, Hoboken
25. Hu X-P, Hsieh Y-L (2001) Effects of dehydration on the crystalline structure and strength of developing cotton fibers. Text Res J 71:231–239
26. Hulleman SHD, Van Hazendonk JM, Van Dam JEG (1994) Determination of crystallinity in native cellulose from higher plants with diffuse reflectance Fourier transform infrared spectroscopy. Carbohydr Res 261:163–172
27. Isogai A (2013) Wood nanocelluloses: fundamentals and applications as new bio-based nanomaterials. J Wood Sci 59:449–459
28. Klemm D, Kramer F, Moritz S, Lindstrom T, Ankerfors M, Gray D, Dorris A (2011) Nanocelluloses: a new family of nature-based materials. Angew Chem Int Ed 50:5438–5466
29. Langan P, Petridis L, O’Neill HM, Pingali SV, Foston M, Nishiyama Y, Schulz R, Lindner B, Hanson BL, Harton S, Heller WT, Urban W, Evans B, Gnanakaran S, Ragauskas AJ, Smith JC, Davison BH (2014) Common processes drive the thermochemical pretreatment of lignocellulosic biomass. Green Chem 16:63–67
30. Langford J, Wilson A (1978) Scherrer after sixty years: a survey and some new results in the determination of crystallite size. J Appl Crystallogr 11:102–113
31. 13C-NMR spectroscopy applied to structure and interaction studies on cellulose I. Solid State Nucl Magn Reson 15:31–40
32. Lee JM, Pawlak JJ, Heitmann JA (2012) Dimensional and hygroexpansive behaviors of cellulose microfibrils (MFs) from kraft pulp-based fibers as a function of relative humidity. Holzforschung 66:1001–1008
33. Lindner B, Petridis L, Langan P, Smith JC (2014) Determination of cellulose crystallinity from powder diffraction diagrams. Biopoly 103:67–73
34. Miller RG Jr (1981) Simultaneous statistical inference. Springer, New York
35. Moon RJ, Martini A, Nairn J, Simonsen J, Youngblood J (2011) Cellulose nanomaterials review: structure, properties and nanocomposites. Chem Soc Rev 40:3941–3994
36. Nelson ML, O’Connor RT (1964) Relation of certain infrared bands to cellulose crystallinity and crystal lattice type. Part I. Spectra of lattice types I, II, III and of amorphous cellulose. J Appl Poly Sci 8:1311–1324
37. 13C NMR signal strengths. Solid State Nucl Magn Reson 15:21–29
38. Nishimura H, Okano T, Asano I (1981) Fine structure of wood cell walls. I. Structural features of noncrystalline substances in wood cell walls. Mokuzai Gakkaishi 27:611–617
39. Nishiyama Y, Langan P, Chanzy H (2002) Crystal structure and hydrogen-bonding system in cellulose Iα from synchrotron X-ray and neutron fiber diffraction. J Am Chem Soc 124:9074–9082
40. Nishiyama Y, Langan P, O’Neill H, Pingali SV, Harton S (2014) Structural coarsening of aspen wood by hydrothermal pretreatment monitored by small- and wide-angle scattering of X-ray and neutrons on oriented specimens. Cellulose 21:1015–1024
41. Oh SY, Yoo DI, Shin Y, Kim HC, Kim HY, Chung YS, Park WH, Youk JH (2005) Crystalline structure analysis of cellulose treated with sodium hydroxide and carbon dioxide by means of X-ray diffraction and FT-IR spectroscopy. Carbohydr Res 340:2376–2391
42. Park S, Baker JO, Himmel ME, Parilla PA, Johnson DK (2010) Cellulose crystallinity index: measurement techniques and their impact on interpreting cellulase performance. Biotechnol Biofuels 3:10
43. Peciulyte A, Karlström K, Larsson PT, Olsson E (2015) Impact of the supramolecular structure of cellulose on the efficiency of enzymatic hydrolysis. Biotechnol Biofuels 8:56
44. Reiner RS, Rudie AW (2013) Process scale-up of cellulose nanocrystal production to 25 kg per batch at the Forest Products Laboratory. In: Postek MT, Moon RJ, Rudie AJ, Bilodeau MA (eds) Production and applications of cellulose materials. TAPPI Press, Atlanta, pp 21–24
45. Richter U, Krause T, Schempp W (1991) Untersuchungen zur Alkalibehandlung von Cellulosefasern. Teil 1. Infrarotspektroskopische und Ro¨ntgenographische Beurteilung der A¨ nderung des Ordnungszustandes. Angew Makromol Chem 185:155–167
46. R Core Team (2013) R: A language and environment for statistical computing. R Foundation for Statistical Computing, Vienna, Austria. http://www.R-project.org
47. Schenzel K, Fischer S, Brendler E (2005) New method for determining the degree of cellulose I crystallinity by means of FT Raman spectroscopy. Cellulose 12:223–231
48. Scherrer P (1918) Bestimmung der Grösse und der inneren Struktur von Kolloidteilchen mittels Röntgenstrahlen. Nachrichten von der Gesellschaft der Wissenschaften, Göttingen, pp 98–100
49. Segal L, Creely JJ, Martin AE, Conrad CM (1959) An empirical method for estimating the degree of crystallinity of native cellulose using the X-ray diffractometer. Text Res J 29:786–794
50. Sisson WA (1933) X-ray analysis of fibers, part I, literature survey. Text Res J 3:295–307
51. Sugino H, Sugimoto H, Miki T, Kanayama K (2007) Fine structure changes of wood during moisture adsorption and desorption process analyzed by X-ray diffraction measurement. Mokuzai Gakkaishi 53:82–89
52. TAPPI test method (1983) Acid insoluble lignin in wood and pulp; official test method T-222 (Om). TAPPI, Atlanta
53. Toba K, Yamamoto H, Yoshida M (2013) Crystallization of cellulose microfibrils in wood cell wall by repeated dry-and-wet treatments, using X-ray diffraction technique. Cellulose 20:633–643
54. Tokoh C, Takabe K, Fujita M, Saiki H (1998) Cellulose synthesized by Acetobacter xylinum in the presence of acetyl glucomannan. Cellulose 5:249–261
55. Vieira FS, Pasquini C (2014) Determination of cellulose crystallinity by terahertz-time domain spectroscopy. Anal Chem 86:3780–3786
56. Wormald P, Wickholm K, Larsson PT, Iversen T (1996) Conversions between ordered and disordered cellulose. Effects of mechanical treatment followed by cyclic wetting and drying. Cellulose 3:141–152
57. Zabler S, Paris O, Burgert I, Fratzl P (2010) Moisture changes in the plant cell wall force cellulose crystallites to deform. J Struct Biol 171:133–141
58. Zhu H, Luo W, Ciesielski PN, Fang Z, Zhu JY, Henriksson G, Himmel ME, Hu L (2016) Wood-derived materials for green electronics, biological devices, and energy applications. Chem Rev 116:9305–9374