Near-Infrared Spectroscopy Using a Supercontinuum Laser: Application to Long Wavelength Transmission Spectra of Barley Endosperm and Oil

Applied Spectroscopy

Volumn 70, Issue 7, 2016, Pages 1176-1185

  Ringsted, Tine ^a   Dupont, Sune ^b   Ramsay, Jacob ^b   Jespersen, Birthe Møller ^a   Sørensen, Klavs Martin ^a   Keiding, Søren Rud ^b   Engelsen, Søren Balling ^a  

^a UNIVERSITY OF COPENHAGEN   (Denmark)

^b AARHUS UNIVERSITY   (Denmark)

Author keywords

Barley seed; beta glucan; food; near infrared spectroscopy; near infrared transmission spectroscopy; NIR; NIT; single seed; supercontinuum laser

Indexed keywords

FATTY ACIDS; FOOD PRODUCTS; GAS OILS; LIGHT SOURCES; MASS SPECTROMETRY; NEAR INFRARED SPECTROSCOPY; OILS AND FATS; PRINCIPAL COMPONENT ANALYSIS; SPECTROMETERS; SPECTRUM ANALYSIS;

BARLEY SEEDS; BETA-GLUCANS; NEAR-INFRARED TRANSMISSION SPECTROSCOPY; SINGLE SEEDS; SUPERCONTINUUM LASER;

INFRARED DEVICES;

BETA GLUCAN; LIPID; PLANT PROTEIN; STARCH; VEGETABLE OIL;

CHEMISTRY; DEVICES; ENDOSPERM; EQUIPMENT DESIGN; HORDEUM; LASER; NEAR INFRARED SPECTROSCOPY; PLANT SEED; PRINCIPAL COMPONENT ANALYSIS; PROCEDURES;

BETA-GLUCANS; ENDOSPERM; EQUIPMENT DESIGN; HORDEUM; LASERS; LIPIDS; PLANT OILS; PLANT PROTEINS; PRINCIPAL COMPONENT ANALYSIS; SEEDS; SPECTROSCOPY, NEAR-INFRARED; STARCH;

EID: 84978289168     PISSN: 00037028     EISSN: 19433530     Source Type: Journal    
DOI: 10.1177/0003702816652361     Document Type: Article

References (41)

1. Agelet L.E., Hurburgh C.R., "A Tutorial on Near Infrared Spectroscopy and Its Calibration". Crit. Rev. Anal. Chem 2010; 40 (4): 246-260.
2. DeThomas F.A., Brimmer P.J., "Monochromators for Near-infrared Spectroscopy". In: Chalmers J.M., Griffiths P.R., (eds). Handbook of Vibrational Spectroscopy 2002; Vol. 1, Chichester, UK: John Wiley & Sons Ltd, pp. 383-392.
3. Alfano R.R., Shapiro S.L., "Emission in the Region 4000 to 7000 Å via 4-Photon Coupling in Glass". Phys. Rev. Lett 1970; 24 (11): 584-587.
4. Dudley J.M., Genty G., Coen S., "Supercontinuum Generation in Photonic Crystal Fiber". Rev. Mod. Phys 2006; 78 (4): 1135-1184.
5. Kaminski C.F., Watt R.S., Elder A.D., Frank J.H., Hult J., "Supercontinuum Radiation for Applications in Chemical Sensing and Microscopy". Appl. Phys. B-Lasers Opt 2008; 92 (3): 367-378.
6. Dupont S., Petersen C., Thøgersen J., Agger C., Bang O., Keiding S.R., "IR Microscopy Utilizing Intense Supercontinuum Light Source". Opt. Express 2012; 20 (5): 4887-4892.
7. Agelet L.E., Hurburgh C.R., "Limitations and Current Applications of Near Infrared Spectroscopy for Single Seed Analysis". Talanta 2014; 121: 288-299.
8. Pedersen D.K., Martens H., Nielsen J.P., Engelsen S.B., "Near-Infrared Absorption and Scattering Separated by Extended Inverted Signal Correction (EISC): Analysis of Near-Infrared Transmittance Spectra of Single Wheat Seeds". Appl. Spectrosc 2002; 56 (9): 1206-1214.
9. Mikkelsen M.S., Jespersen B.M., Larsen F.H., Blennow A., Engelsen S.B., "Molecular Structure of Large-Scale Extracted Beta-Glucan from Barley and Oat: Identification of a Significantly Changed Block Structure in a High Beta-Glucan Barley Mutant". Food Chem 2013; 136 (1): 130-138.
10. Wood P.J., "Cereal Beta-Glucans in Diet and Health". J. Cereal Sci 2007; 46 (3): 230-238.
11. Munck L., Nielsen J.P., Møller B., Jacobsen S., Søndergaard I., Engelsen S.B., Nørgaard L., Bro R., "Exploring the Phenotypic Expression of a Regulatory Proteome-Altering Gene by Spectroscopy and Chemometrics". Anal. Chim. Acta 2001; 446 (1-2): 171-186.
12. Seefeldt H.F., Blennow A., Jespersen B.M., Wollenweber B., Engelsen S.B., "Accumulation of Mixed Linkage (1 -> 3) (1 -> 4)-Beta-D-Glucan During Grain Filling in Barley: A Vibrational Spectroscopy Study". J. Cereal Sci 2009; 49 (1): 24-31.
13. Tønning E., Thybo A.K., Pedersen L., Munck L., Hansen Å., Tøgersen F.A., Engelsen S.B., Nørgaard L., "Bulk Functionality Diversification by Unsupervised Single-Kernel Near-Infrared (SKNIR) Sorting of Wheat". Cereal Chem 2009; 86 (6): 706-713.
14. Ramsay J., Dupont S., Keiding S.R., "Pulse-to-Pulse Noise Reduction in Infrared Supercontinuum Spectroscopy: Polarization and Amplitude Fluctuations". Laser Phys. Lett 2014; 11 (9): 4.
15. Munck L., Møller B., Jacobsen S., Søndergaard I., "Near Infrared Spectra Indicate Specific Mutant Endosperm Genes and Reveal a New Mechanism for Substituting Starch with (1 -> 3,1 -> 4)-Beta-Glucan in Barley". J. Cereal Sci 2004; 40 (3): 213-222.
16. Jacobsen S., Søndergaard I., Møller B., Desler T., Munck L., "A Chemometric Evaluation of the Underlying Physical and Chemical Patterns that Support Near Infrared Spectroscopy of Barley Seeds as a Tool for Explorative Classification of Endosperm, Genes and Gene Combinations". J. Cereal Sci 2005; 42 (3): 281-299.
17. AACC. "β-Glucan Content of Barley and Oats-Rapid Enzymatic Procedure". In: Approved Methods of Analysis. St. Paul, MN: AACC International, 1999, Method 32-23.01.
18. AOAC. "Protein (Crude) in Animal Feed, Forage (Plant Tissue), Grain and Oilseeds". In: Official Methods of Analysis of AOAC International. Gaithersburg, MD: AOAC International, 2005, Official Method 2001.11.
19. AOAC. "Starch (Total) in Cereal Products". In: Official Methods of Analysis of AOAC International. Gaithersburg, MD: AOAC International, 2005, Official Method 996.11.
20. AACC. "Moisture-Air-Oven Methods". In: Approved Methods of Analysis. St. Paul, MN: AACC International, 1999, Method 44-15.02.
21. AOAC. "Crude Fat in Feeds, Cereal Grains, and Forages". In: Official Methods of Analysis of AOAC International. Gaithersburg, MD: AOAC International, 2006, Official Method 2003.06.
22. Sørensen K.M., Petersen H., Engelsen S.B., "An On-Line Near-Infrared (NIR) Transmission Method for Determining Depth Profiles of Fatty Acid Composition and Iodine Value in Porcine Adipose Fat Tissue". Appl. Spectrosc 2012; 66 (2): 218-226.
23. Agilent. "Application note 5988-5871EN" Santa Clara, CA: Agilent Technologies, 2012.
24. AOCS. "Calculated Iodine Value". In: Official Methods and Recommended Practices of the AOCS. Champaign, IL: American Oil Chemists Society, 2009, Recommended Practice Cd 1c-85.
25. Rinnan Å., van den Berg F., Engelsen S.B., "Review of the Most Common Pre-Processing Techniques for Near-Infrared Spectra". Trends Anal. Chem 2009; 28 (10): 1201-1222.
26. Bro R., Smilde A.K., "Principal Component Analysis". Anal. Methods 2014; 6 (9): 2812-2831.
27. Skov T., Honoré A.H., Jensen H.M., Næs T., Engelsen S.B., "Chemometrics in Foodomics: Handling Data Structures from Multiple Analytical Platforms". Trends Anal. Chem 2014; 60: 71-79.
28. G.P. Fox. "Chemical Composition in Barley Grains and Malt Quality". In: G. Zhang, C. Li, editors. Genetics and Improvement of Barley Malt Quality. Berlin Heidelberg: Springer, 2010. Chap. 3, Pp. 63-98.
29. Chandra G.S., Proudlove M.O., Baxter E.D., "The Structure of Barley Endosperm-An Important Determinant of Malt Modification". J. Sci. Food Agric 1999; 79 (1): 37-46.
30. Neuberger T., Sreenivasulu N., Rokitta M., Rolletschek H., Göbel C., Rutten T., Radchuk V., Feussner I., Wobus U., Jakob P., Webb A., Borisjuk L., "Quantitative Imaging of Oil Storage in Developing Crop Seeds". Plant Biotechnol. J 2008; 6 (1): 31-45.
31. Munck L., Jespersen B.M., Rinnan Å., Seefeldt H.F., Engelsen M.M., Nørgaard L., Engelsen S.B., "A Physiochemical Theory on the Applicability of Soft Mathematical Models-Experimentally Interpreted". J. Chemom 2010; 24 (7-8): 481-495.
32. Tønning E., Nørgaard L., Engelsen S.B., Pedersen L., Esbensen K.H., "Protein Heterogeneity in Wheat Lots Using Single-Seed NIT-A Theory of Sampling (TOS) Breakdown of All Sampling and Analytical Errors". Chemom. Intell. Lab. Syst 2006; 84 (1-2): 142-152.
33. Osborne B.G., Fearn T., Hindle P.H., Practical NIR Spectroscopy, with Applications in Food and Beverage Analysis, 2nd ed. Harlow, UK: Longman Scientific and Technical, 1993.
34. Czuchajowska Z., Szczodrak J., Pomeranz Y., "Characterization and Estimation of Barley Polysaccharides by Near-Infrared Spectroscopy. I. Barley, Starches, and Beta-Deuterium-Glucans". Cereal Chem 1992; 69 (4): 413-418.
35. Williams P., "Implementation of Near-Infrared Technology". In: Williams P., Norris K., (eds). Near-Infrared Technology in the Agricultureal and Food Industries, 2nd ed. St. Paul, MN: American Association of Cereal Chemists, 2001, pp. 168.
36. Hódsági M., Gergely S., Gelencsér T., Salgó A., "Investigations of Native and Resistant Starches and Their Mixtures Using Near-Infrared Spectroscopy". Food Bioprocess Technol 2012; 5 (1): 401-407.
37. B.G. Osborne, T. Fearn. "Applications of Near Infrared Spectroscopy in Food Analysis". In: B.G. Osborne (ed) Near Infrared Spectroscopy in Food Analysis. Harlow, UK: Longman Scientific & Technical, 1986. Chap. 7, Pp. 133.
38. Horvath L., Norris K.H., Horvathmosonyi M., Rigo J., Hegedusvolgyesi E., "Study into Determining Dietary Fiber of Wheat Bran by NIR-Technique". Acta Aliment 1984; 13 (4): 355-382.
39. de Sá R.M., Palmer G.H., "Assessment of Enzymatic Endosperm Modification of Malting Barley Using Individual Grain Analyses". J. Inst. Brew 2004; 110 (1): 43-50.
40. Cozzolino D., Murray I., Chree A., Scaife J.R., "Multivariate Determination of Free Fatty Acids and Moisture in Fish Oils by Partial Least-Squares Regression and Near-Infrared Spectroscopy". LWT 2005; 38 (8): 821-828.
41. Petersen C.R., Møller U., Kubat I., Zhou B.B., Dupont S., Ramsay J., Benson T., Sujecki S., Abdel-Moneim N., Tang Z.Q., Furniss D., Seddon A., Bang O., "Mid-Infrared Supercontinuum Covering The 1.4-13.3 Mu M Molecular Fingerprint Region Using Ultra-High NA Chalcogenide Step-Index Fibre". Nat. Photonics 2014; 8 (11): 830-834.