Liquid chromatography Orbitrap mass spectrometry with simultaneous full scan and tandem MS/MS for highly selective pesticide residue analysis

Analytical and Bioanalytical Chemistry

Volumn 407, Issue 21, 2015, Pages 6317-6326

  Del Mar Gómez Ramos, María ^a   Rajski, Łukasz ^a   Heinzen, Horacio ^b   Fernández Alba, Amadeo R ^a  

^a UNIVERSITY OF ALMERÍA   (Spain)

^b UNIVERSIDAD DE LA REPÚBLICA   (Uruguay)

Author keywords

Mass spectrometry; Orbitrap; Pesticides; Q Orbitrap

Indexed keywords

GAIN CONTROL; IDENTIFICATION (CONTROL SYSTEMS); INSECTICIDES; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; SPECTROMETRY;

AUTOMATIC GAIN CONTROL; FRUIT AND VEGETABLES; HIGH RESOLUTION MASS SPECTROMETRY; OPERATIONAL PARAMETERS; ORBITRAP; ORBITRAP MASS SPECTROMETRIES; PESTICIDE RESIDUE ANALYSIS; RETROSPECTIVE ANALYSIS;

PESTICIDES;

PESTICIDE RESIDUE;

LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; PROCEDURES;

CHROMATOGRAPHY, LIQUID; MASS SPECTROMETRY; PESTICIDE RESIDUES;

EID: 84943349483     PISSN: 16182642     EISSN: 16182650     Source Type: Journal    
DOI: 10.1007/s00216-015-8709-z     Document Type: Article

References (19)

1. Kaufmann A et al (2012) Study of high-resolution mass spectrometry technology as a replacement for tandem mass spectrometry in the field of quantitative pesticide residue analysis. J AOAC Int 95(2):528-548
2. Alder L, Steinborn A, Bergelt S (2011) Suitability of an Orbitrap mass spectrometer for the screening of pesticide residues in extracts of fruits and vegetables. J AOAC Int 94(6):1661-1673
3. Kellmann M et al (2009) Full scan MS in comprehensive qualitative and quantitative residue analysis in food and feed matrices: how much resolving power is required? J Am Soc Mass Spectrom 20(8): 1464-1476
4. Mol HG, Zomer P, de Koning M (2012) Qualitative aspects and validation of a screening method for pesticides in vegetables and fruits based on liquid chromatography coupled to full scan high resolution (Orbitrap) mass spectrometry. Anal Bioanal Chem 403(10):2891-2908
5. Kaufmann A et al (2011) Development of an improved high resolution mass spectrometry based multi-residue method for veterinary drugs in various food matrices. Anal Chim Acta 700(1-2):86-94
6. Ates E et al (2014) Screening of plant and fungal metabolites in wheat, maize and animal feed using automated on-line clean-up coupled to high resolution mass spectrometry. Food Chem 142: 276-284
7. Mol HG et al (2011) Screening of plant toxins in food, feed and botanicals using full-scan high-resolution (Orbitrap) mass spectrometry. Food Addit Contam Part A Chem Anal Control Expo Risk Assess 28(10):1405-1423
8. Farre M, Pico Y, Barcelo D (2013) Direct peel monitoring of xenobiotics in fruit by direct analysis in real time coupled to a linear quadrupole ion trap-orbitrap mass spectrometer. Anal Chem 85(5): 2638-2644
9. Jia W et al (2014) Multi-mycotoxin analysis in dairy products by liquid chromatography coupled to quadrupole orbitrap mass spectrometry. J Chromatogr A 1345:107-114
10. Vaclavik L et al (2013) Determination of multiple mycotoxins in dietary supplements containing green coffee bean extracts using ultrahigh-performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS). J Agric Food Chem 61(20):4822-4830
11. Fedorova G et al (2013) Comparison of the quantitative performance of a Q-Exactive high-resolution mass spectrometer with that of a triple quadrupole tandem mass spectrometer for the analysis of illicit drugs in wastewater. Rapid Commun Mass Spectrom 27(15): 1751-1762
12. Shi F et al (2014) Application of a high resolution benchtop quadrupole-Orbitrap mass spectrometry for the rapid screening, confirmation and quantification of illegal adulterated phosphodiesterase-5 inhibitors in herbal medicines and dietary supplements. J Chromatogr A 1344:91-98
13. Kumar P et al (2013) Targeted analysis with benchtop quadrupole-orbitrap hybrid mass spectrometer: application to determination of synthetic hormones in animal urine. Anal Chim Acta 780:65-73
14. Wang J et al (2012) Application of ultrahigh-performance liquid chromatography and electrospray ionization quadrupole orbitrap high-resolution mass spectrometry for determination of 166 pesticides in fruits and vegetables. J Agric Food Chem 60(49):12088-12104
15. Jia W et al (2014) High-throughput screening of pesticide and veterinary drug residues in baby food by liquid chromatography coupled to quadrupole Orbitrap mass spectrometry. J Chromatogr A 1347:122-128
16. Malato O et al (2011) Benefits and pitfalls of the application of screening methods for the analysis of pesticide residues in fruits and vegetables. J Chromatogr A 1218(42):7615-7626
17. Lozano A et al (2014) Evaluation of zirconium dioxidebased sorbents to decrease the matrix effect in avocado and almond multiresidue pesticide analysis followed by gas chromatography tandem mass spectrometry. Talanta 118:68-83
18. Rajski Ł, Gomez-Ramos MM, Fernandez-Alba AR (2014) Large pesticide multiresidue screening method by liquid chromatography-Orbitrap mass spectrometry in full scan mode applied to fruit and vegetables. J Chromatogr A 1360:119-127
19. European Commission, Health & Consumer Protection Directorate-General (2013) Guidance document on analytical quality control and validation procedures for pesticide residues analysis in food and feed, SANCO/12571/2013. EC, Brussels