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Volumn 63, Issue 26, 2015, Pages 5985-5992

Efficient Separation and Analysis of Triacylglycerols: Quantitation of β-Palmitate (OPO) in Oils and Infant Formulas

Author keywords

ELSD; fatty acid; HPLC; infant formula; regiospecific analysis; triacylglycerol

Indexed keywords

FATTY ACIDS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; ISOMERS; LIGHT SCATTERING; SEPARATION;

EID: 84936818693     PISSN: 00218561     EISSN: 15205118     Source Type: Journal    
DOI: 10.1021/acs.jafc.5b01835     Document Type: Article
Times cited : (18)

References (44)
  • 1
    • 0025378227 scopus 로고
    • Lipids of bovine and human milks: A comparison
    • 10.3168/jds.S0022-0302(90)78666-3
    • Jensen, R. G.; Ferris, A. M.; Lammi-Keefe, C. J.; Henderson, R. A. Lipids of bovine and human milks: A comparison J. Dairy Sci. 1990, 73, 223-40 10.3168/jds.S0022-0302(90)78666-3
    • (1990) J. Dairy Sci. , vol.73 , pp. 223-40
    • Jensen, R.G.1    Ferris, A.M.2    Lammi-Keefe, C.J.3    Henderson, R.A.4
  • 2
    • 33645325393 scopus 로고    scopus 로고
    • The stereospecific triacylglycerol structures and fatty acid profiles of human milk and infant formulas
    • Straarup, E. M.; Lauritzen, L.; Faerk, J.; Høy, C.-E.; Michaelsen, K. F. The stereospecific triacylglycerol structures and fatty acid profiles of human milk and infant formulas J. Pediatr. Gastroenterol. Nutr. 2006, 42, 293-299 10.1097/01.mpg.0000214155.51036.4f
    • (2006) J. Pediatr. Gastroenterol. Nutr. , vol.42 , pp. 293-299
    • Straarup, E.M.1    Lauritzen, L.2    Faerk, J.3    Michaelsen, K.F.4
  • 3
    • 84865793731 scopus 로고    scopus 로고
    • Phospholipid fingerprints of milk from different mammalians determined by 31P NMR: Towards specific interest in human health
    • Garcia, C.; Lutz, N. W.; Confort-Gouny, S.; Cozzone, P. J.; Armand, M.; Bernard, M. Phospholipid fingerprints of milk from different mammalians determined by 31P NMR: Towards specific interest in human health Food Chem. 2012, 135, 1777-1783 10.1016/j.foodchem.2012.05.111
    • (2012) Food Chem. , vol.135 , pp. 1777-1783
    • Garcia, C.1    Lutz, N.W.2    Confort-Gouny, S.3    Cozzone, P.J.4    Armand, M.5    Bernard, M.6
  • 4
    • 52549098079 scopus 로고    scopus 로고
    • Gangliosides in human, cow and goat milk, and their abilities as to neutralization of cholera toxin and botulinum type A neurotoxin
    • Iwamori, M.; Takamizawa, K.; Momoeda, M.; Iwamori, Y.; Taketani, Y. Gangliosides in human, cow and goat milk, and their abilities as to neutralization of cholera toxin and botulinum type A neurotoxin Glycoconjugate J. 2008, 25, 675-683 10.1007/s10719-008-9128-6
    • (2008) Glycoconjugate J. , vol.25 , pp. 675-683
    • Iwamori, M.1    Takamizawa, K.2    Momoeda, M.3    Iwamori, Y.4    Taketani, Y.5
  • 6
    • 85078377286 scopus 로고    scopus 로고
    • EFSA panel on dietetic products, scientific opinion on the substantiation of a health claim related to beta-palmitate and increased calcium absorption pursuant to Article 14 of Regulation (EC) No. 1924/2006. and references cited therein.
    • EFSA panel on dietetic products, scientific opinion on the substantiation of a health claim related to beta-palmitate and increased calcium absorption pursuant to Article 14 of Regulation (EC) No. 1924/2006. EFSA J. 2011, 9, 2289, and references cited therein.
    • (2011) EFSA J. , vol.9 , pp. 2289
  • 7
    • 0028833318 scopus 로고
    • The relationship between stool hardness and stool composition in breast- and formula-fed infants
    • Quinlan, P. T.; Lockton, S.; Irwin, J.; Lucas, A. L. The relationship between stool hardness and stool composition in breast- and formula-fed infants J. Pediatr. Gastroenterol. Nutr. 1995, 20, 81-90 10.1097/00005176-199501000-00014
    • (1995) J. Pediatr. Gastroenterol. Nutr. , vol.20 , pp. 81-90
    • Quinlan, P.T.1    Lockton, S.2    Irwin, J.3    Lucas, A.L.4
  • 8
    • 84858648337 scopus 로고    scopus 로고
    • InFatTM premium fat for infant formula: Fat closer to human milk
    • Wennermark, M.; Raveh, P. InFatTM premium fat for infant formula: Fat closer to human milk Agro Food Ind. Hi-Tech 2012, 23, 16-17
    • (2012) Agro Food Ind. Hi-Tech , vol.23 , pp. 16-17
    • Wennermark, M.1    Raveh, P.2
  • 9
    • 80051596648 scopus 로고    scopus 로고
    • Infant nutrition - Review of lipid innovation in infant formula
    • Sidnell, A.; Greenstreet, E. Infant nutrition-review of lipid innovation in infant formula Nutr. Bull. 2011, 36, 373-380 10.1111/j.1467-3010.2011.01913.x
    • (2011) Nutr. Bull. , vol.36 , pp. 373-380
    • Sidnell, A.1    Greenstreet, E.2
  • 10
    • 0036195597 scopus 로고    scopus 로고
    • Molecular weight distribution and regioisomeric structure of triacylglycerols in some common human milk substitutes
    • Kurvinen, J.-P.; Sjövall, O.; Kallio, H. Molecular weight distribution and regioisomeric structure of triacylglycerols in some common human milk substitutes J. Am. Oil Chem. Soc. 2002, 79, 13-22 10.1007/s11746-002-0428-3
    • (2002) J. Am. Oil Chem. Soc. , vol.79 , pp. 13-22
    • Kurvinen, J.-P.1    Sjövall, O.2    Kallio, H.3
  • 13
    • 84885795316 scopus 로고    scopus 로고
    • Regiospecific analysis of triacylglycerols
    • Kalo, P. Regiospecific analysis of triacylglycerols Lipid Technol. 2013, 25, 230-234 10.1002/lite.201300305
    • (2013) Lipid Technol. , vol.25 , pp. 230-234
    • Kalo, P.1
  • 14
    • 0025913327 scopus 로고
    • Stereospecific analysis of triacyl- sn -glycerols by chiral high-performance liquid chromatography
    • Takagi, T.; Ando, Y. Stereospecific analysis of triacyl- sn -glycerols by chiral high-performance liquid chromatography Lipids 1991, 26, 542-547 10.1007/BF02536601
    • (1991) Lipids , vol.26 , pp. 542-547
    • Takagi, T.1    Ando, Y.2
  • 15
    • 0015632367 scopus 로고
    • Triglyceride structure of milk fats
    • Kuksis, A.; Marai, L.; Myher, J. J. Triglyceride structure of milk fats J. Am. Oil Chem. Soc. 1973, 50, 193-201 10.1007/BF02640489
    • (1973) J. Am. Oil Chem. Soc. , vol.50 , pp. 193-201
    • Kuksis, A.1    Marai, L.2    Myher, J.J.3
  • 16
    • 22544472164 scopus 로고    scopus 로고
    • Lipase-catalyzed acidolysis of tripalmitin with hazelnut oil fatty acids and stearic acid to produce human milk fat substitutes
    • Sahin, N.; Akoh, C. C.; Karaali, A. Lipase-catalyzed acidolysis of tripalmitin with hazelnut oil fatty acids and stearic acid to produce human milk fat substitutes J. Agric. Food Chem. 2005, 53, 5779-5783 10.1021/jf050465e
    • (2005) J. Agric. Food Chem. , vol.53 , pp. 5779-5783
    • Sahin, N.1    Akoh, C.C.2    Karaali, A.3
  • 17
    • 0027570828 scopus 로고
    • Release of volatile branched-chain and other fatty-acids from ruminant milk fats by various lipases
    • Ha, J. K.; Lindsay, R. C. Release of volatile branched-chain and other fatty-acids from ruminant milk fats by various lipases J. Dairy Sci. 1993, 76, 677-690 10.3168/jds.S0022-0302(93)77391-9
    • (1993) J. Dairy Sci. , vol.76 , pp. 677-690
    • Ha, J.K.1    Lindsay, R.C.2
  • 18
    • 0242624546 scopus 로고    scopus 로고
    • Acyl migration incidence on accuracy of a triacylglycerol regioanalysis - A theoretical evaluation
    • Turon, F.; Bonnot, F.; Caro, Y.; Pina, M.; Graille, J. Acyl migration incidence on accuracy of a triacylglycerol regioanalysis-a theoretical evaluation Chem. Phys. Lipids 2003, 125, 41-48 10.1016/S0009-3084(03)00069-0
    • (2003) Chem. Phys. Lipids , vol.125 , pp. 41-48
    • Turon, F.1    Bonnot, F.2    Caro, Y.3    Pina, M.4    Graille, J.5
  • 19
    • 19444379562 scopus 로고    scopus 로고
    • Regio- and stereospecific analysis of glycerolipids
    • Kuksis, A.; Itabashi, Y. Regio- and stereospecific analysis of glycerolipids Methods 2005, 36, 172-185 10.1016/j.ymeth.2004.11.001
    • (2005) Methods , vol.36 , pp. 172-185
    • Kuksis, A.1    Itabashi, Y.2
  • 20
    • 2942627447 scopus 로고    scopus 로고
    • Off-line coupling of non-aqueous reversed-phase and silver ion high-performance liquid chromatography-mass spectrometry for the characterization of rice oil triacylglycerol positional isomers
    • Dugo, P.; Favoino, O.; Tranchida, P. Q.; Dugo, G.; Mondello, L. Off-line coupling of non-aqueous reversed-phase and silver ion high-performance liquid chromatography-mass spectrometry for the characterization of rice oil triacylglycerol positional isomers J. Chromatogr. A 2004, 1041, 135-142 10.1016/j.chroma.2004.04.063
    • (2004) J. Chromatogr. A , vol.1041 , pp. 135-142
    • Dugo, P.1    Favoino, O.2    Tranchida, P.Q.3    Dugo, G.4    Mondello, L.5
  • 21
    • 84872687758 scopus 로고    scopus 로고
    • Characterization and quantification of triacylglycerols in peanut oil by off-line comprehensive two-dimensional liquid chromatography coupled with atmospheric pressure chemical ionization mass spectrometry
    • Hu, J.; Wei, F.; Dong, X.-Y.; Lv, X.; Jiang, M.-L.; Li, G.-M.; Chen, H. Characterization and quantification of triacylglycerols in peanut oil by off-line comprehensive two-dimensional liquid chromatography coupled with atmospheric pressure chemical ionization mass spectrometry J. Sep. Sci. 2013, 36, 288-300 10.1002/jssc.201200567
    • (2013) J. Sep. Sci. , vol.36 , pp. 288-300
    • Hu, J.1    Wei, F.2    Dong, X.-Y.3    Lv, X.4    Jiang, M.-L.5    Li, G.-M.6    Chen, H.7
  • 22
    • 66149146680 scopus 로고    scopus 로고
    • Regioisomeric characterization of triacylglycerols using silver-ion HPLC/MS and randomization synthesis of standards
    • Lísa, M.; Velínská, H.; Holčapek, M. Regioisomeric characterization of triacylglycerols using silver-ion HPLC/MS and randomization synthesis of standards Anal. Chem. 2009, 81, 3903-3910 10.1021/ac900150j
    • (2009) Anal. Chem. , vol.81 , pp. 3903-3910
    • Lísa, M.1    Velínská, H.2    Holčapek, M.3
  • 23
    • 78649810918 scopus 로고    scopus 로고
    • Regioisomeric analysis of triacylglycerols using silver-ion liquid chromatography-atmospheric pressure chemical ionization mass spectrometry: Comparison of five different mass analyzers
    • Holčapek, M.; Dvořáková, H.; Lísa, M.; Jimenéz Girón, A.; Sandra, P.; Cvačka, J. Regioisomeric analysis of triacylglycerols using silver-ion liquid chromatography-atmospheric pressure chemical ionization mass spectrometry: Comparison of five different mass analyzers J. Chromatogr. A 2010, 1217, 8186-8194 10.1016/j.chroma.2010.10.064
    • (2010) J. Chromatogr. A , vol.1217 , pp. 8186-8194
    • Holčapek, M.1    Dvořáková, H.2    Lísa, M.3    Jimenéz Girón, A.4    Sandra, P.5    Cvačka, J.6
  • 24
    • 84877270274 scopus 로고    scopus 로고
    • Applicability of non-linear versus linear fractional abundance calibration plots for the quantitative determination of triacylglycerol regioisomers by tandem mass spectrometry
    • Ramaley, L.; Herrera, L. C.; Melanson, J. E. Applicability of non-linear versus linear fractional abundance calibration plots for the quantitative determination of triacylglycerol regioisomers by tandem mass spectrometry Rapid Commun. Mass Spectrom. 2013, 27, 1251-1259 10.1002/rcm.6569
    • (2013) Rapid Commun. Mass Spectrom. , vol.27 , pp. 1251-1259
    • Ramaley, L.1    Herrera, L.C.2    Melanson, J.E.3
  • 25
    • 84883144407 scopus 로고    scopus 로고
    • Development of an offline bidimensional high-performance liquid chromatography method for analysis of stereospecific triacylglycerols in cocoa butter equivalents
    • Kadivar, S.; De Clercq, N.; Nusantoro, B. P.; Le, T. T.; Dewettinck, K. Development of an offline bidimensional high-performance liquid chromatography method for analysis of stereospecific triacylglycerols in cocoa butter equivalents J. Agric. Food Chem. 2013, 61, 7896-7903 10.1021/jf401566c
    • (2013) J. Agric. Food Chem. , vol.61 , pp. 7896-7903
    • Kadivar, S.1    De Clercq, N.2    Nusantoro, B.P.3    Le, T.T.4    Dewettinck, K.5
  • 27
    • 84861175163 scopus 로고    scopus 로고
    • Rapid and direct quantitative analysis of positional fatty acids in triacylglycerols using 13C NMR
    • Gouk, S. W.; Cheng, S. F.; Ong, A. S. H.; Chuah, C. H. Rapid and direct quantitative analysis of positional fatty acids in triacylglycerols using 13C NMR Eur. J. Lipid Sci. Technol. 2012, 114, 510-519 10.1002/ejlt.201100074
    • (2012) Eur. J. Lipid Sci. Technol. , vol.114 , pp. 510-519
    • Gouk, S.W.1    Cheng, S.F.2    Ong, A.S.H.3    Chuah, C.H.4
  • 28
    • 0018890975 scopus 로고
    • A procedure for the quantitative isolation of brain gangliosides
    • Svennerholm, L.; Fredman, P. A procedure for the quantitative isolation of brain gangliosides Biochim. Biophys. Acta, Lipids Lipid Metab. 1980, 617, 97-109 10.1016/0005-2760(80)90227-1
    • (1980) Biochim. Biophys. Acta, Lipids Lipid Metab. , vol.617 , pp. 97-109
    • Svennerholm, L.1    Fredman, P.2
  • 29
    • 0017841053 scopus 로고
    • Adaptation of a macro-scale method to the micro-scale for fatty acid methyl transesterification of biological lipid extracts
    • Carreau, J. P.; Dubacq, J. P. Adaptation of a macro-scale method to the micro-scale for fatty acid methyl transesterification of biological lipid extracts J. Chromatogr. 1978, 151, 384-390 10.1016/S0021-9673(00)88356-9
    • (1978) J. Chromatogr. , vol.151 , pp. 384-390
    • Carreau, J.P.1    Dubacq, J.P.2
  • 30
    • 84985217481 scopus 로고
    • An improved method of characterizing fatty acids by equivalent chain length values
    • Stránský, K.; Jursĺk, T.; Vĺtek, A.; Skořepa, J. An improved method of characterizing fatty acids by equivalent chain length values J. High Resolut. Chromatogr. 1992, 15, 730-740 10.1002/jhrc.1240151107
    • (1992) J. High Resolut. Chromatogr. , vol.15 , pp. 730-740
    • Stránský, K.1    Jursĺk, T.2    Vĺtek, A.3    Skořepa, J.4
  • 31
    • 84988090443 scopus 로고
    • Analysis of triacylglycerol positional isomers by silver ion high performance liquid chromatography
    • Adlof, R. O. Analysis of triacylglycerol positional isomers by silver ion high performance liquid chromatography J. High Resolut. Chromatogr. 1995, 18, 105-107 10.1002/jhrc.1240180207
    • (1995) J. High Resolut. Chromatogr. , vol.18 , pp. 105-107
    • Adlof, R.O.1
  • 32
    • 0037467421 scopus 로고    scopus 로고
    • Synthesis and analysis of symmetrical and nonsymmetrical disaturated/monounsaturated triacylglycerols
    • Adlof, R. O.; List, G. R. Synthesis and analysis of symmetrical and nonsymmetrical disaturated/monounsaturated triacylglycerols J. Agric. Food Chem. 2003, 51, 2096-2099 10.1021/jf021085l
    • (2003) J. Agric. Food Chem. , vol.51 , pp. 2096-2099
    • Adlof, R.O.1    List, G.R.2
  • 34
    • 84864338772 scopus 로고    scopus 로고
    • Trends in fatty acids positional distribution in human colostrum, transitional, and mature milk
    • Haddad, I.; Mozzon, M.; Frega, N. G. Trends in fatty acids positional distribution in human colostrum, transitional, and mature milk Eur. Food Res. Technol. 2012, 235, 325-332 10.1007/s00217-012-1759-y
    • (2012) Eur. Food Res. Technol. , vol.235 , pp. 325-332
    • Haddad, I.1    Mozzon, M.2    Frega, N.G.3
  • 35
    • 84879520996 scopus 로고    scopus 로고
    • Critical considerations for fast and accurate regiospecific analysis of triacylglycerols using quantitative 13C NMR
    • Gouk, S. W.; Cheng, S. F.; Malon, M.; Hock Ong, A. S.; Chuah, C. H. Critical considerations for fast and accurate regiospecific analysis of triacylglycerols using quantitative 13C NMR Anal. Methods 2013, 5, 2064-2073 10.1039/c3ay26106a
    • (2013) Anal. Methods , vol.5 , pp. 2064-2073
    • Gouk, S.W.1    Cheng, S.F.2    Malon, M.3    Hock Ong, A.S.4    Chuah, C.H.5
  • 36
    • 0036473985 scopus 로고    scopus 로고
    • 13C NMR spectra of TAG: An easy way to distinguish milks from different animal species
    • Andreotti, G.; Lamanna, R.; Trivellone, E.; Motta, A. 13C NMR spectra of TAG: An easy way to distinguish milks from different animal species J. Am. Oil Chem. Soc. 2002, 79, 123-127 10.1007/s11746-002-0445-2
    • (2002) J. Am. Oil Chem. Soc. , vol.79 , pp. 123-127
    • Andreotti, G.1    Lamanna, R.2    Trivellone, E.3    Motta, A.4
  • 37
    • 0242498768 scopus 로고    scopus 로고
    • Alternative NMR method for quantitative determination of acyl positional distribution in triacylglycerols and related compounds
    • Simova, S.; Ivanova, G.; Spassov, S. L. Alternative NMR method for quantitative determination of acyl positional distribution in triacylglycerols and related compounds Chem. Phys. Lipids 2003, 126, 167-176 10.1016/j.chemphyslip.2003.08.003
    • (2003) Chem. Phys. Lipids , vol.126 , pp. 167-176
    • Simova, S.1    Ivanova, G.2    Spassov, S.L.3
  • 38
    • 0022110461 scopus 로고
    • Capillary GC of triglycerides in fats and oils using a high temperature phenylmethylsilicone stationary phase, part 1
    • Geeraert, E.; Sandra, P. Capillary GC of triglycerides in fats and oils using a high temperature phenylmethylsilicone stationary phase, part 1 J. High Resolut. Chromatogr. 1985, 8, 415-422 10.1002/jhrc.1240080812
    • (1985) J. High Resolut. Chromatogr. , vol.8 , pp. 415-422
    • Geeraert, E.1    Sandra, P.2
  • 39
    • 84936801560 scopus 로고    scopus 로고
    • Higherature gas chromatography of triacylglycerols - a cautionary note? (accessed June).
    • Christie, W. W. Higherature gas chromatography of triacylglycerols-a cautionary note? http://lipidlibrary.aocs.org/topics/gcoftg/index.htm (accessed June 3, 2015).
    • (2015)
    • Christie, W.W.1
  • 40
    • 0031567118 scopus 로고    scopus 로고
    • Normal-phase separation effects with lipids on a silver ion high-performance liquid chromatography column
    • Adlof, R. O. Normal-phase separation effects with lipids on a silver ion high-performance liquid chromatography column J. Chromatogr. A 1997, 764, 337-340 10.1016/S0021-9673(96)00886-2
    • (1997) J. Chromatogr. A , vol.764 , pp. 337-340
    • Adlof, R.O.1
  • 41
    • 0036483660 scopus 로고    scopus 로고
    • The composition of bovine milk lipids: January 1996 to December 2000
    • Jensen, R. G. The composition of bovine milk lipids: January 1996 to December 2000 J. Dairy Sci. 2002, 85, 295-350 10.3168/jds.S0022-0302(02)74079-4
    • (2002) J. Dairy Sci. , vol.85 , pp. 295-350
    • Jensen, R.G.1
  • 42
    • 0242367847 scopus 로고    scopus 로고
    • 3 rd ed. Oily Press: Bridgwater, UK
    • Christie, W. W. Lipid Analysis, 3 rd ed.; Oily Press: Bridgwater, UK, 2003; pp 260-261.
    • (2003) Lipid Analysis , pp. 260-261
    • Christie, W.W.1
  • 43
    • 37549023071 scopus 로고    scopus 로고
    • Comprehensive two-dimensional liquid chromatography with ultraviolet, evaporative light scattering and mass spectrometric detection of triacylglycerols in corn oil
    • van der Klift, E. J. C.; Vivó-Truyols, G.; Claassen, F. W.; van Holthoon, F. L.; van Beek, T. A. Comprehensive two-dimensional liquid chromatography with ultraviolet, evaporative light scattering and mass spectrometric detection of triacylglycerols in corn oil J. Chromatogr. A 2008, 1178, 43-55 10.1016/j.chroma.2007.11.039
    • (2008) J. Chromatogr. A , vol.1178 , pp. 43-55
    • Van Der Klift, E.J.C.1    Vivó-Truyols, G.2    Claassen, F.W.3    Van Holthoon, F.L.4    Van Beek, T.A.5
  • 44
    • 84869087490 scopus 로고    scopus 로고
    • HPLC/ELSD analysis of amidated bile acids: An effective and rapid way to assist continuous flow chemistry processes
    • Sardella, R.; Gioiello, A.; Ianni, F.; Venturoni, F.; Natalini, B. HPLC/ELSD analysis of amidated bile acids: An effective and rapid way to assist continuous flow chemistry processes Talanta 2012, 100, 364-371 10.1016/j.talanta.2012.07.092
    • (2012) Talanta , vol.100 , pp. 364-371
    • Sardella, R.1    Gioiello, A.2    Ianni, F.3    Venturoni, F.4    Natalini, B.5


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