Formation and Structure of Copper(II) Oxalate Layers on Carboxy-Terminated Self-Assembled Monolayers

Langmuir

Volumn 30, Issue 40, 2014, Pages 11945-11954

  Schrader, I ^a   Wittig, L ^b   Richter, K ^b   Vieker, H ^c   Beyer, A ^c   Golzhauser A ^c   Hartwig, A ^b   Swiderek, P ^a  

^a UNIVERSITY OF BREMEN   (Germany)

^b FRAUNHOFER INSTITUTE FOR MANUFACTURING TECHNOLOGY AND ADVANCED MATERIALS IFAM   (Germany)

^c BIELEFELD UNIVERSITY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

COPPER; CRYSTAL STRUCTURE; DEPOSITION; INFRARED SPECTROSCOPY; IONS; MONOLAYERS; ORGANIC ACIDS; OXALIC ACID; QUARTZ; QUARTZ CRYSTAL MICROBALANCES; SCANNING ELECTRON MICROSCOPY; VISCOELASTICITY; VOLATILE FATTY ACIDS;

DISSIPATION MEASUREMENTS; ETHANOLIC SOLUTION; HELIUM ION MICROSCOPIES; QUARTZ MICROBALANCE; REFLECTION ABSORPTION INFRARED SPECTROSCOPY; STEP-BY-STEP APPROACH; VISCO-ELASTIC BEHAVIORS; VISCOELASTIC LAYERS;

SELF ASSEMBLED MONOLAYERS;

EID: 84927511220     PISSN: 07437463     EISSN: 15205827     Source Type: Journal    
DOI: 10.1021/la5026312     Document Type: Article

References (34)

1. Love, J. C.; Estroff, L. A.; Kriebel, J. K.; Nuzzo, R. G.; Whitesides, G. M. Self-assembled monolayers of thiolates on metals as a form of nanotechnology Chem. Rev. 2005, 105, 1103 - 1169
2. Xia, Y.; Rogers, J. A.; Paul, K. E.; Whitesides, G. M. Unconventional methods for fabricating and patterning nanostructures Chem. Rev. 1999, 99, 1823 - 1848
3. Bumm, L. A.; Arnold, J. J.; Cygan, M. T.; Dunbar, T. D.; Burgin, T. P.; Jones, L.; Allara, D. L.; Tour, J. M.; Weiss, P. S. Are single molecular wires conducting? Science 1996, 271, 1705 - 1707
4. de Boer, B.; Hadipour, A.; Mandoc, M. M.; van Woudenbergh, T.; Blom, P. W. M. Tuning of metal work functions with self-assembled monolayers Adv. Mater. 2005, 17, 621 - 625
5. Kind, M.; Wöll, C. Organic surfaces exposed by self-assembled organothiol monolayers: Preparation, characterization, and application Prog. Surf. Sci. 2009, 84, 230 - 278
6. Plain, J.; Pallandre, A.; Nysten, B.; Jonas, A. M. Nanotemplated crystallization of organic molecules Small 2006, 2, 892 - 897
7. Zacher, D.; Shekhah, O.; Wöll, C.; Fischer, R. A. Thin films of metal-organic frameworks Chem. Soc. Rev. 2009, 38, 1418 - 1429
8. Shekhah, O.; Liu, J.; Fischer, R. A.; Wöll, C. MOF thin films: existing and future applications Chem. Soc. Rev. 2011, 40, 1081 - 1106
9. Biemmi, E.; Scherb, C.; Bein, T. Oriented growth of the metal organic framework Cu3(BTC)2(H2O)3·xH2O tunable with functionalized self-assembled monolayers J. Am. Chem. Soc. 2007, 129, 8054 - 8055
10. Shekhah, O.; Wang, H.; Zacher, D.; Fischer, R. A.; Wöll, C. Growth mechanism of metal-organic frameworks: Insights into the nucleation by employing a step-by-step route Angew. Chem., Int. Ed. 2009, 48, 5038 - 5041
11. Janiak, C.; Vieth, J. K. MOFs, MILs and more: concepts, properties and applications for porous coordination networks (PCNs) New J. Chem. 2010, 34, 2366 - 2388
12. Birzescu, M.; Niculescu, M.; Dimitru, R.; Budrugeac, P.; Segal, E. Copper(II) oxalate obtained through the reaction of 1,2-ethanediol with Cu(NO3)2·3H2O-Structural investigations and thermal analysis J. Therm. Anal. Calorim. 2008, 94, 297 - 303
13. Jongen, N.; Bowen, P.; Lemaiître, J.; Valmalette, J.-C.; Hofmann, H. Precipitation of self-organized copper oxalate polycrystalline particles in the presence of hydroxypropylmethylcellulose (HPMC): Control of morphology J. Colloid Interface Sci. 2000, 226, 189 - 198
14. Kitagawa, S.; Okubo, T.; Kawata, S.; Kondo, M.; Katada, M.; Kobayashi, H. An oxalate-linked copper(II) coordination polymer, [Cu2(oxalate)2(pyrazine)3]n constructed with two different copper units: X-ray crystallographic and electronic structures Inorg. Chem. 1995, 34, 4790 - 4796
15. Wu, W.-Y.; Zhai, L. X. Poly[diaqua- l -oxalato-copper(II) monohydrate] Acta Crystallogr., Sect. E 2007, 63, m429 - m430
16. Scott, K. L.; Wieghardt, K.; Sykes, A. G. μ-Oxalato-cobalt(III) complexes Inorg. Chem. 1973, 12, 655 - 663
17. Tolstoy, V. P.; Chernyshova, I. V.; Skryshevsky, V. A. Handbook of Infrared Spectroscopy of Ultrathin Films; Wiley: Hoboken, NJ, 2003.
18. Bradshaw, A. M.; Schweizer, E. In Spectroscopy of Surfaces; Clark, R. J. H.; Hester, R. E., Eds.; Wiley: New York, 1988; p 413.
19. Paul, J.; Williams, G. P.; Hoffmann, F. M. Carbon dioxide activation and alkali compound formation. I. Vibrational characterization of oxalate intermediates Surf. Sci. 2003, 531, 244 - 264
20. D'Antonio, M. C.; Palacios, D.; Coggiola, L.; Baran, E. J. Vibrational and electronic spectra of synthetic moolooite Spectrochim. Acta, Part A 2007, 68, 424 - 426
21. Edwards, H. G. M.; Farwell, D. W.; Rose, S. J.; Smith, D. N. Vibrational spectra of copper(II)oxalate dihydrate, CuC2O4·2H2O, and dipotassium bis-oxalato copper(II) tetrahydrate, K2Cu(C2O4)2·2H2O J. Mol. Struct. 1991, 249, 233 - 243
22. Clark, R. J. S.; Firth, S. Raman, infrared and force field studies of K212C2O4·H2O and K213C2O4·H2O in the solid state and in aqueous solution, and of (NH4)212C2O4·H2O and (NH4)213C2O4·H2O in the solid state Spectrochim. Acta, Part A 2002, 58, 1731 - 1746
23. Fujita, J.; Martell, A.; Nakamoto, K. Infrared spectra of metal chelate compounds. VI. A normal coordinate treatment of Oxalato Metal Complexes J. Chem. Phys. 1962, 36, 324 - 331
24. Rahimi-Nasrabadi, M.; Pourmortazavi, S. M.; Davoudi-Dehaghani, A. A.; Hajimirsadeghi, S. S.; Zahedi, M. M. Synthesis and characterization of copper oxalate and copper oxide nanoparticles by statistically optimized controlled precipitation and calcination of precursor CrystEngComm 2013, 15, 4077 - 4086
25. Lamprecht, E.; Watkins, G. M.; Brown, M. E. The thermal decomposition of copper(II) oxalate revisited Thermochim. Acta 2006, 446, 91 - 100
26. Heyns, A. M. The low-temperature infrared spectra of the copper(II)acetates J. Mol. Struct. 1972, 11, 93 - 103
27. Arnold, R.; Azzam, W.; Terfort, A.; Wöll, C. Preparation, modification, and crystallinity of aliphatic and aromatic carboxylic acid terminated self-assembled monolayers Langmuir 2002, 18, 3980 - 3992
28. Stavila, V.; Volponi, J.; Katzenmeyer, A. M.; Dixon, M. C.; Allendorf, M. D. Kinetics and mechanism of metal-organic framework thin film growth: systematic investigation of HKUST-1 deposition on QCM electrodes Chem. Sci. 2012, 3, 1531 - 1540
29. Höök, F.; Kasemo, B.; Nylander, T.; Fant, C.; Sott, K.; Elwing, H. Variations in coupled water, viscoelastic properties, and film thickness of a Mefp-1 protein film during adsorption and cross-linking: a quartz crystal microbalance with dissipation monitoring, ellipsometry, and surface plasmon resonance study Anal. Chem. 2001, 73, 5796 - 5804
30. Johannsmann, D. Viscoelastic, mechanical, and dielectric measurements on complex samples with the quartz crystal microbalance Phys. Chem. Chem. Phys. 2008, 10, 4516 - 4534
31. Zacher, D.; Yusenko, K.; Bétard, A.; Henke, S.; Molon, M.; Ladnorg, T.; Shekhah, O.; Schnüpbach, B.; de los Arcos, T.; Krasnopolski, M.; Meilikhov, M.; Winter, J.; Terfort, A.; Wöll, C.; Fischer, R. A. Liquid-phase epitaxy of multicomponent layer-based porous coordination polymer thin films of [M(L)(P)0.5] type: Importance of deposition sequence on the oriented growth Chem.-Eur. J. 2011, 17, 1448 - 1455
32. Frost, R.; Grandfils, C.; Cerda, B.; Kasemo, B.; Svedhem, S. Structural rearrangements of polymeric insulin-loaded nanoparticles interacting with surface-supported model lipid membranes J. Biomater. Nanobiotechnol. 2011, 2, 181 - 193
33. Richter, K.; Diaconu, G.; Rischka, K.; Amkreutz, M.; Müller, F. A.; Hartwig, A. Adsorption studies of mussel-inspired peptides Bioinspired, Biomimetic Nanobiomater. 2012, 2, 45 - 53
34. Ward, B. W.; Notte, J. A.; Economou, N. P. Helium ion microscopy: A new tool for nanoscale microscopy and metrology J. Vac. Sci. Technol. B: Microeletron. Nanometer Struct. 2006, 24, 2871 - 2874