Practical aspects in gas chromatography-mass spectrometry for the analysis of pesticide residues in exotic fruits

Food Chemistry

Volumn 182, Issue , 2015, Pages 14-22

  España Amórtegui, Julio César ^a   Guerrero Dallos, Jairo Arturo ^a  

^a UNIVERSIDAD NACIONAL DE COLOMBIA   (Colombia)

Author keywords

Analyte protectants (AP); Concurrent backflushing; Gas chromatography mass spectrometry (GC MS); Large volume injection (LVI); QuEChERS; Tropical fruits

Indexed keywords

CHROMATOGRAPHY; FRUITS; MASS SPECTROMETRY; MIXTURES; PESTICIDES; SPECTROMETRY;

ANALYTE PROTECTANTS; BACK-FLUSHING; GAS CHROMATOGRAPHY-MASS SPECTROMETRIES (GC-MS); LARGE VOLUME INJECTION; QUECHERS; TROPICAL FRUITS;

GAS CHROMATOGRAPHY;

PESTICIDE RESIDUE;

ARTICLE; FRUIT; HIGH TEMPERATURE; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; MOLECULAR WEIGHT; PHYSALIS; RESIDUE ANALYSIS; STANDARD; CHEMISTRY; PROCEDURES;

PHYSALIS;

FRUIT; GAS CHROMATOGRAPHY-MASS SPECTROMETRY; PESTICIDE RESIDUES;

EID: 84924033905     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2015.02.113     Document Type: Article

References (35)

1. Ahumada Forigua, D. A. (2010, April). Reducción del efecto matriz en el análisis de residuos de plaguicidas mediante cromatografía de gases. Universidad Nacional de Colombia. Retrieved from http://www.bdigital.unal.edu.co/3164/.
2. K. Banerjee, S. Mujawar, S.C. Utture, S. Dasgupta, and P.G. Adsule Optimization of gas chromatography-single quadrupole mass spectrometry conditions for multiresidue analysis of pesticides in grapes in compliance to EU-MRLs Food Chemistry 138 1 2013 600 607 10.1016/j.foodchem.2012.10.105
3. E. Boselli, K. Grob, and G. Lercker Solvent trapping during large volume injection with an early vapor exit, Part 3: The main cause of volatile component loss during partially concurrent evaporation Journal of High Resolution Chromatography I 6 1999 327 334
4. E. Boselli, B. Grolimund, K. Grob, G. Lercker, and R. Amadò Solvent trapping during large volume injection with an early vapor exit, Part 1: description of the flooding process Journal of High Resolution Chromatography 21 6 1998 355 362 10.1002/(SICI)1521-4168(19980601)21:6<355::AID-JHRC355>3.0.CO;2-B
5. T. Cajka, J. Hajslova, O. Lacina, K. Mastovska, and S.J. Lehotay Rapid analysis of multiple pesticide residues in fruit-based baby food using programmed temperature vaporiser injection-low-pressure gas chromatography-high-resolution time-of-flight mass spectrometry Journal of Chromatography A 1186 1-2 2008 281 294 10.1016/j.chroma.2007.12.009
6. CEN. (2008). EN 15662. Foods of plant origin - Determination of pesticide residues using GC-MS and/or LC-MS/MS following acetonitrile extraction/partitioning and clean-up by dispersive SPE - QuEChERS-method.
7. M.I. Cervera, T. Portolés, E. Pitarch, J. Beltrán, and F. Hernández Application of gas chromatography time-of-flight mass spectrometry for target and non-target analysis of pesticide residues in fruits and vegetables Journal of Chromatography A 1244 2012 168 177 10.1016/j.chroma.2012.04.063
8. Codex Committee on Pesticide Residues (CCPR). (2010). Analysis of Pesticide Residues: Portion of Commodities to which Codex MRLS Apply and which is Analyzed, 1-9.
9. De Koning, S.; Kurano, M.; Janssen, H.-G.; & Brinkman, U. A. T. (2004). AT-column, a novel concentrating technique for large-volume injections in gas chromatography. Journal of Chromatography A, 1023(2), 165-174. Retrieved from http://www.sciencedirect.com/science/article/B6TG8-4B0NY6R-2/2/e078a23de2a414b9f6dd728e44db7530.
10. Directorate General for Health & Consumers (DG SANCO). (2014). Document SANCO/12571/2013. "Method validation and quality control procedures for pesticide residues in food and feed".
11. Erney, D. R.; Gillespie, A. M.; Gilvydis, D. M.; & Poole, C. F. (1993). Explanation of the matrix-induced chromatographic response enhancement of organophosphorus pesticides during open tubular column gas chromatography with splitless or hot on-column injection and flame photometric detection. Journal Of Chromatography, 638(1), 57-63. Retrieved from http://www.sciencedirect.com/science/article/B6TG8-44CPVK5-B3/2/dd6a34b887a09b3d0bf21c9c7f8a469b.
12. D.R. Erney, T.M. Pawlowski, and C.F. Poole Matrix-induced peak enhancement of pesticides in gas chromatogrtaphy: Is there a solution? Journal of High Resolution Chromatography 20 7 1997 375 378 10.1002/jhrc.1240200706
13. J.C. España Amórtegui, and J.A. Guerrero Comparison of QuEChERS official methodologies for the analysis of pesticide residues on Colombian fruits by GC-MS Food Additives & Contaminants: Part A 31 4 2014 676 687 10.1080/19440049.2014.885660
14. EU Reference Laboratory for single residue methods CVUA Stuttgart. (2011). What to pay attention to when using Analyte Protectants (AP) (pp. 8-9). Retrieved from http://www.crl-pesticides.eu/library/docs/srm/AP-UsingAP-SRM.pdf.
15. A.R. Fernández-Alba, and J.F. García-Reyes Large-scale multi-residue methods for pesticides and their degradation products in food by advanced LC-MS TrAC Trends in Analytical Chemistry 27 11 2008 973 990 10.1016/j.trac.2008.09.009
16. Grob, K.; & Müller, E. (1988). Co solvent effects for preventing broadening or loss of early eluted peaks when using concurrent solvent evaporation in capillary GC. Part 1: Concept of the technique. Journal of High Resolution Chromatography, 11(1), 388-394. Retrieved from http://onlinelibrary.wiley.com/doi/10.1002/jhrc.1240110506/abstract.
17. Grob Jr, K.; Karrer, G.; & Riekkola, M.-L. (1985). On-column injection of large sample volumes using the retention gap technique in capillary gas-cromatography. Journal of Chromatography A, 334(0), 129-155. Retrieved from http://www.sciencedirect.com/science/article/pii/S0021967300802691.
18. Heide, M. Van Der, Bruns, S.; Lach, G.; & Parlar, H. (2012). Ascorbic acid as analyte protectant applied within the QuEChERS multi-method (GC-MS) for vegetable analysis (Vol. 21, p. 1). Vienna, Austria.
19. E. Hoh, and K. Mastovska Large volume injection techniques in capillary gas chromatography Journal of Chromatography A 1186 1-2 2008 2 15 10.1016/j.chroma.2007.12.001
20. S.J. Lehotay, U. Koesukwiwat, H. van der Kamp, H.G. Mol, and N. Leepipatpiboon Qualitative aspects in the analysis of pesticide residues in fruits and vegetables using fast low-pressure gas chromatography-time-of-flight mass spectrometry Journal of Agricultural and Food Chemistry 59 14 2011 7544 7556 10.1021/jf104606j
21. S.J. Lehotay, and R. Gates Blind analysis of fortified pesticide residues in carrot extracts using GC-MS to evaluate qualitative and quantitative performance Journal of Separation Science 32 21 2009 3706 3719 10.1002/jssc.200900387
22. P. Magni, and T. Porzano Concurrent solvent recondensation large sample volume splitless injection Journal of Separation Science 26 17 2003 1491 1498 10.1002/jssc.200301553
23. K. Mastovská, S.J. Lehotay, and M. Anastassiades Combination of analyte protectants to overcome matrix effects in routine GC analysis of pesticide residues in food matrixes Analytical Chemistry 77 24 2005 8129 8137 10.1021/ac0515576
24. K. Mastovska, and P.L. Wylie Evaluation of a new column backflushing set-up in the gas chromatographic-tandem mass spectrometric analysis of pesticide residues in dietary supplements Journal of Chromatography A 1265 2012 155 164 10.1016/j.chroma.2012.09.094
25. H.G.J. Mol, H. Janssen, and C.A. Cramers Large volume sample introduction using temperature programmable injectors: Implications of liner diameter Journal of High Resolution Chromatography 18 1995 19 27
26. H. Mol, H. Janssen, C. Cramers, J. Vreuls, and U. Brinkman Trace level analysis of micropollutants in aqueous samples using gas chromatography with on-line sample enrichment and large volume injection Journal of Chromatography A 703 1-2 1995 277 307 10.1016/0021-9673(95)00169-N
27. H.G.J. Mol, P. Plaza-bolan, P. Zomer, T.C. De Rijk, and A.A.M. Stolker Toward a generic extraction method for simultaneous determination of pesticides, mycotoxins, plant toxins, and veterinary drugs in feed and food matrixes Analitical Chemistry 80 24 2008 9450 9459
28. H.G.J. Mol, P. Zomer, and M. de Koning Qualitative aspects and validation of a screening method for pesticides in vegetables and fruits based on liquid chromatography coupled to full scan high resolution (Orbitrap) mass spectrometry Analytical and Bioanalytical Chemistry 403 10 2012 2891 2908 10.1007/s00216-012-6100-x
29. Official Journal of the European Communities. Regulation (EC) No 396/2005 of the European Parliament and the Council of 23 February 2005 on maximum residue levels of pesticides in or on food and feed of plant and animal origin and amending Council Directive 91/414/EEC (2005). Retrieved from ec.europa.eu/sanco-pesticides/public/index.cfm.
30. C.F. Poole Matrix-induced response enhancement in pesticide residue analysis by gas chromatography Journal of Chromatography A 1158 1-2 2007 241 250 10.1016/j.chroma.2007.01.018
31. Teske, J.; & Engewald, W. (2002). Methods for, and applications of, large-volume injection in capillary gas chromatography. TrAC Trends in Analytical Chemistry, 21(9-10), 584-593. Retrieved from http://www.sciencedirect.com/science/article/B6V5H-46WWC34-5/2/fe47fb5c00cdc5da21007bd7cd4f9155.
32. D.P. Venema, P. Zomer, T.C. De Rijk, and H.G.J. Mol Multi-residue analysis of pesticides in animal products by generic extraction and LC-MS/MS 31 2012 6700
33. Vogt, W.; Jacob, K.; Ohnesorge, A.-B.; & Werner Obwexer, H. (1979). Capillary gas chromatographic injection system for large sample volumes. Journal of Chromatography A, 186(0), 197-205. Retrieved from http://www.sciencedirect.com/science/article/pii/S0021967300952488.
34. F.H. Walters Sequential Simplex Optimization 1991 CRC Press LLC. Boca Raton, FL p. 403
35. X. Xu, L. Li, W. Zhong, and Y. He Rapid GC-MS Analysis of Pesticide Residues Using Analyte Protectants Analytical Letters 42 16 2009 2578 2591 10.1080/00032710903243646