Improved sample preparation for GC-MS-SIM analysis of ethyl carbamate in wine

Food Chemistry

Volumn 177, Issue , 2015, Pages 23-28

  Nóbrega, Ian C C ^a   Pereira, Giuliano E ^b   Silva, Marileide ^c   Pereira, Elainy V S ^a   Medeiros, Marcelo M ^c   Telles, Danuza L ^c   Albuquerque, Eden C ^c   Oliveira, Juliane B ^b   Lachenmeier, Dirk W ^d  

^a UNIVERSIDADE FEDERAL RURAL DE PERNAMBUCO   (Brazil)

^b EMBRAPA UVA E VINHO   (Brazil)

^c Instituto de Tecnologia de Pernambuco   (Brazil)

^d Chemisches und Veterinäruntersuchungsamt ^*  (Germany)

Author keywords

Automated parallel evaporation; Diethyl ether extraction; Ethyl carbamate; GC MS SIM; Validation; Wine

Indexed keywords

DICHLOROMETHANE; ETHERS; EVAPORATION; EXTRACTION; VACUUM EVAPORATION;

DIETHYL ETHERS; ETHYL CARBAMATE; GC-MS-SIM; LIMITS OF DETECTION; REGRESSION COEFFICIENT; SAMPLE PREPARATION; SAMPLE PREPARATION PROCEDURE; VALIDATION;

WINE;

DICHLOROMETHANE; ETHER; URETHAN;

ACCURACY; ACIDITY; ARTICLE; CONCENTRATION (PARAMETERS); DISTILLATION; EVAPORATION; FOOD ANALYSIS; FOOD STORAGE; ION MONITORING; LIMIT OF DETECTION; LIMIT OF QUANTITATION; MASS FRAGMENTOGRAPHY; MOLECULAR STABILITY; PH; PHYSICAL CHEMISTRY; RELATIVE DENSITY; RESIDUAL VOLUME; SOLVENT EXTRACTION; VALIDATION STUDY; WINE; ANALYSIS; PROCEDURES;

GAS CHROMATOGRAPHY-MASS SPECTROMETRY; URETHANE; WINE;

EID: 84920721169     PISSN: 03088146     EISSN: 18737072     Source Type: Journal    
DOI: 10.1016/j.foodchem.2014.12.031     Document Type: Article

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