Dispersive micro-solid-phase extraction of benzodiazepines from biological fluids based on polyaniline/magnetic nanoparticles composite

Analytica Chimica Acta

Volumn 844, Issue , 2014, Pages 80-89

  Asgharinezhad, Ali Akbar ^a   Ebrahimzadeh, Homeira ^a   Mirbabaei, Fatemeh ^a   Mollazadeh, Narges ^a   Shekari, Nafiseh ^a  

^a SHAHID BEHESHTI UNIVERSITY   (Iran)

Author keywords

Dispersive solid phase extraction; Lorazepam; Nitrazepam; Preconcentration

Indexed keywords

BODY FLUIDS; DOPING (ADDITIVES); HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; NANOCOMPOSITES; ORGANIC SOLVENTS; PHASE SEPARATION; POLYANILINE; POLYPYRROLES; SORBENTS; SORPTION;

LORAZEPAM; NITRAZEPAM; POLYANILINE NANOCOMPOSITES; PRE-CONCENTRATION; SOLID-PHASE EXTRACTION;

EXTRACTION;

ACETONITRILE; AMMONIUM DERIVATIVE; ANILINE PYRROLE COPOLYMER; CETHYLTRIMETHYL AMMONIUM BROMIDE; COPOLYMER; IRON OXIDE; LORAZEPAM; MAGNETIC NANOPARTICLE; NANOCOMPOSITE; NITRAZEPAM; ORGANIC SOLVENT; PARA TOLUENE SULFONIC ACID; POLYANILINE; POLYPYRROLE; SODIUM CHLORIDE; SORBENT; SULFONIC ACID DERIVATIVE; UNCLASSIFIED DRUG; BENZODIAZEPINE DERIVATIVE; NANOPARTICLE;

ARTICLE; CALIBRATION; CONTROLLED STUDY; DISPERSIVE MICRO SOLID PHASE EXTRACTION; DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG STRUCTURE; DRUG URINE LEVEL; ELUTION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; HUMAN; INTERMETHOD COMPARISON; LIMIT OF DETECTION; LINEAR SYSTEM; OXIDATION; PH; POLYMERIZATION; PRIORITY JOURNAL; PROCESS OPTIMIZATION; SOLID PHASE MICROEXTRACTION; ULTRAVIOLET SPECTROSCOPY; ISOLATION AND PURIFICATION; MAGNETISM; PROCEDURES; SCANNING ELECTRON MICROSCOPY; SOLID PHASE EXTRACTION; ULTRAVIOLET SPECTROPHOTOMETRY;

BENZODIAZEPINES; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MAGNETICS; MICROSCOPY, ELECTRON, SCANNING; NANOPARTICLES; SOLID PHASE EXTRACTION; SPECTROPHOTOMETRY, ULTRAVIOLET;

EID: 84906935642     PISSN: 00032670     EISSN: 18734324     Source Type: Journal    
DOI: 10.1016/j.aca.2014.06.007     Document Type: Article

References (41)

1. Bakavoli M., Kaykhai M. Quantitative determination of diazepam, nitrazepam and flunitrazepam in tablets using thin-layer chromatography-densitometry technique. J. Pharm. Biomed. Anal. 2003, 31:1185-1189.
2. Baselt R.C. Disposition of Toxic Drugs and Chemicals in Man 1995, Chemical Toxicology Institute, Foster City, CA. 4th edition.
3. Bugey A., Staub C. Rapid analysis of benzodiazepines in whole blood by high-performance liquid chromatography: use of a monolithic column. J. Pharm. Biomed. Anal. 2004, 35:555-562.
4. Pistos C., Stewart J.T. Direct injection HPLC method for the determination of selected benzodiazepines in plasma using a Hisep column. J. Pharm. Biomed. Anal. 2003, 33:1135-1142.
5. Borrey D., Meyer E., Lambert W., Van Peteghem S., Van Peteghem C., De Leenheer A.P. Sensitive gas chromatographic-mass spectrometric screening of acetylated benzodiazepines. J. Chromatogr. A 2001, 910:105-118.
6. Nakamura M. Analyses of benzodiazepines and their metabolites in various biological matrices by LC-MS (/MS). Biomed. Chromatogr. 2011, 25:1283-1307.
7. Wang K., Cheng M., Hsieh C., Hsu J., Wu J., Lee C. Determination of nimetazepam and 7-aminonimetazepam in human urine by using liquid chromatography-tandem mass spectrometry. Forensic Sci. Int. 2013, 224:84-89.
8. Lee H.H., Lee J.F., Lin S.Y., Lin Y.Y., Wu C.F., Wu M.T., Chen B.H. Simultaneous quantification of urine flunitrazepam, nimetazepam and nitrazepam by using liquid chromatography-tandem mass spectrometry. Clin. Chim. Acta 2013, 420:134-139.
9. Lee X.P., Kumazawa T., Sato J., Shoji Y., Hasegawa C., Karibe C., Arinobu T., Seno H., Sato K. Simple method for the determination of benzodiazepines in human body fluids by high-performance liquid chromatography-mass spectrometry. Anal. Chim. Acta 2003, 492:223-231.
10. Monzon L.M.A., Yudi L.M. Voltammetric analysis of lipophilicity of benzodiazepine derivatives at the water {divides} 1,2-dichloroethane interface. J. Electroanal. Chem. 2001, 495:146-151.
11. Li N., Lee H.K. Solid-phase extraction of polycyclic aromatic hydrocarbons in surface water: negative effect of humic acid. J. Chromatogr. A 2001, 921:255-263.
12. Basheer C., Chong H.G., Hii T.M., Lee H.K. Application of porous membrane-protected micro-solid-phase extraction combined with HPLC for the analysis of acidic drugs in wastewater. Anal. Chem. 2007, 79:6845-6850.
13. 4@C@PANI magnetic microspheres for the extraction and analysis of phenolic compounds in water samples by gas chromatography-mass spectrometry. J. Chromatogr. A 2011, 1218:2841-2847.
14. Basheer C., Alnedhary A.A., Madhava Rao B.S., Lee H.K. Determination of carbamate pesticides using micro-solid-phase extraction combined with high-performance liquid chromatography. J. Chromatogr. A 2009, 1216:211-216.
15. Meng J., Bu J., Deng C., Zhang X. Preparation of polypyrrole-coated magnetic particles for micro solid-phase extraction of phthalates in water by gas chromatography-mass spectrometry analysis. J. Chromatogr. A 2011, 1218:1585-1591.
16. Chen L., Wang T., Tong J. Application of derivatized magnetic materials to the separation and the preconcentration of pollutants in water samples. Trends Anal. Chem. 2011, 30(7):1095-1108.
17. Kim T.Y., Yamazaki Y., Hirano T. Magneto-optical properties of Bi-YIG nanoparticle with polymethacrylate matrix materials. Phys. Status Solidi B 2004, 241:1601-1604.
18. Sounderya N., Zhang Y. Use of core/shell structured nanoparticles for biomedical applications. Recent Pat. Biomed. Eng. 2008, 1:34-42.
19. 4@Ag core@shell nanoparticles: characterization and application. Anal. Chim. Acta 2012, 756:13-22.
20. Rossi L.M., Quach A.D., Rosenzweig Z. Glucose oxidase-magnetite nanoparticle bioconjugate for glucose sensing. Anal. Bioanal. Chem. 2004, 380:606-613.
21. Xu H., Tong N., Cui L., Lu Y., Gu H. Preparation of hydrophilic magnetic nanospheres with high saturation magnetization. J. Magn. Magn. Mater. 2007, 311:125-130.
22. Galán-Cano F., Alcudia-León M.C., Lucena R., Cárdenas S., Valcárcel M. Ionic liquid coated magnetic nanoparticles for the gas chromatography/mass spectrometric determination of polycyclic aromatic hydrocarbons in waters. J. Chromatogr. A 2013, 1300:134-140.
23. Bagheri H., Mohammadi A., Salemi A. On-line trace enrichment of phenolic compounds from water using a pyrrole-based polymer as the solid-phase extraction sorbent coupled with high-performance liquid chromatography. Anal. Chim. Acta 2004, 513:445-449.
24. Bagheri H., Ayazi Z., Naderi M. Conductive polymer-based microextraction methods: a review. Anal. Chim. Acta 2013, 767:1-13.
25. Bagheri H., Daliri R., Roostaie A. A novel magnetic poly(aniline-naphthylamine)-based nanocomposite for micro solid phase extraction of rhodamine B. Anal. Chim. Acta 2013, 794:38-46.
26. Zhao Q., Lu Q., Feng Y.-Q. Dispersive microextraction based on magnetic polypyrrole nanowires for the fast determination of pesticide residues in beverage and environmental water samples. Anal. Bioanal. Chem. 2013, 405:4765-4776.
27. Faraji M., Yamini Y., Tahmasebi E., Saleh A., Nourmohammadian F. Cetyltrimethylammonium bromide-coated magnetite nanoparticles as highly efficient adsorbent for rapid removal of reactive dyes from the textile companies' wastewaters. J. Iran Chem. Soc. 2010, 7:S130-S144.
28. Tahmasebi E., Yamini Y., Seidi S., Rezazadeh M. Extraction of three nitrophenols using polypyrrole-coated magnetic nanoparticles based on anion exchange process. J. Chromatogr. A 2013, 1314:15-23.
29. Asgharinezhad A.A., Mollazadeh N., Ebrahimzadeh H., Mirbabaei F., Shekari N. Magnetic nanoparticles based dispersive micro-solid-phase extraction as a novel technique for coextraction of acidic and basic drugs from biological fluids and waste water. J. Chromatogr. A 2014, 1338:1-8.
30. 4/polyaniline nanocomposites: effect of dopant on the properties. Colloids Surf. A 2008, 320:49-56.
31. Jang J., Ha J., Kim S. Fabrication of polyaniline nanoparticles using microemulsion polymerization. Macromol. Res. 2007, 15:154-159.
32. Bagheri H., Alipour N., Ayazi Z. Multiresidue determination of pesticides from aquatic media using polyaniline nanowires network as highly efficient sorbent for microextraction in packed syringe. Anal. Chim. Acta 2012, 740:43-49.
33. Ebrahimzadeh H., Molaei K., Asgharinezhad A.A., Shekari N., Dehghani Z. Molecularly imprinted nano particles combined with miniaturized homogenous liquid-liquid extraction for the selective extraction of loratadine in plasma and urine samples followed by high performance liquid chromatography-photo diode array detection. Anal. Chim. Acta 2013, 767:155-162.
34. Ebrahimzadeh H., Asgharinezhad A.A., Abedi H., Kamarei F. Optimization of carrier-mediated three-phase hollow fiber microextraction combined with HPLC-UV for determination of propylthiouracil in biological samples. Talanta 2011, 85:1043-1049.
35. Ebrahimzadeh H., Shekari N., Saharkhiz Z., Asgharinezhad A.A. Simultaneous determination of chloropheniramine maleate and dextromethorphan hydrobromide in plasma sample by hollow fiber liquid phase microextraction and high performance liquid chromatography with the aid of chemometrics. Talanta 2012, 94:77-83.
36. Verplaetse R., Cuypers E., Tytgat J. The evaluation of the applicability of a high pH mobile phase in ultrahigh performance liquid chromatography tandem mass spectrometry analysis of benzodiazepines and benzodiazepine-like hypnotics in urine and blood. J. Chromatogr. A 2012, 1249:147-154.
37. Salomone A., Gerace E., Brizio P., Gennaro M.C., Vincenti M. A fast liquid chromatography-tandem mass spectrometry method for determining benzodiazepines and analogues in urine. Validation and application to real cases of forensic interest. J. Pharm. Biomed. Anal. 2011, 56:582-591.
38. Papoutsis I.I., Athanaselis S.A., Nikolaou P.D., Pistos C.M., Spiliopoulou C.A., Maravelias C.P. Development and validation of an EI-GC-MS method for the determination of benzodiazepine drugs and their metabolites in blood: applications in clinical and forensic toxicology. J. Pharm. Biomed. Anal. 2010, 52:609-614.
39. Rezaei F., Yamini Y., Moradi M., Daraei B. Supramolecular solvent-based hollow fiber liquid phase microextraction of benzodiazepines. Anal. Chim. Acta 2013, 804:135-142.
40. Jinno K., Taniguchi M., Hayashida M. Solid phase micro extraction coupled with semi-microcolumn high performance liquid chromatography for the analysis of benzodiazepines in human urine. J. Pharm. Biomed. Anal. 1998, 17:1081-1091.
41. 4/polyaniline nanoparticles. J. Chromatogr. A 2011, 1218:4269-4274.