Expanding the separation capability of sequential injection chromatography: Determination of melamine in milk exploiting micellar medium and on-line sample preparation

Microchemical Journal

Volumn 117, Issue , 2014, Pages 106-110

  Batista, Alex D ^a   Nascimento, Carina F ^a   Melchert, Wanessa R ^a   Rocha, Fábio R P ^a  

^a UNIVERSITY OF SÃO PAULO   (Brazil)

Author keywords

Melamine; Micellar chromatography; Milk; Monolithic columns; Sequential injection chromatography

Indexed keywords

EID: 84903637174     PISSN: 0026265X     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.microc.2014.06.015     Document Type: Article

References (29)

1. Šatínský D., Solich P., Chocholouš P., Karlíček R. Monolithic columns-a new concept of separation in the sequential injection technique. Anal. Chim. Acta. 2003, 499:205-214.
2. Chocholouš P., Kosařová L., Šatínský D., Sklenářová H., Solich P. Enhanced capabilities of separation in sequential injection chromatography-fused-core particle column and its comparison with narrow-bore monolithic column. Talanta 2011, 85:1129-1134.
3. Chocholouš P., Vacková J., Šrámková I., Šatínský D., Solich P. Advantages of core-shell particle columns in sequential injection chromatography for determination of phenolic acids. Talanta 2013, 103:221-227.
4. Ángel M.J.R., Broch S.C., Coque M.C.G.A. Chromatographic efficiency in micellar liquid chromatography: should it be still a topic of concern?. Sep. Purif. Rev. 2012, 42:1-27.
5. Ángel M.J.R., Broch S.C., Lapasió J.R.T., Coque M.C.G.A. Retention mechanisms in micellar liquid chromatography. J. Chromatogr. A 2009, 1216:1798-1814.
6. Montgomery M.E., Wirth M.J. Spectroscopic study of the molecular basis of wetting of a C18 surface by long-chain n-alcohols. Anal. Chem. 1994, 66:680-684.
7. Vasimalai N., John S.A. Picomolar melamine enhanced the fluorescence of gold nanoparticles: spectrofluorimetric determination of melamine in milk and infant formulas using functionalized triazole capped goldnanoparticles. Biosens. Bioelectron. 2013, 42:267-272.
8. Yang H.H., Zhou W.H., Guo X.C., Chen F.R., Zhao H.Q., Lin L.M., Wang X.R. Molecularly imprinted polymer as SPE sorbent for selective extraction of melamine in dairy products. Talanta 2009, 80:821-825.
9. Cao X., Shen F., Zhang M., Guo J., Luo Y., Li X., Liu H., Sun C., Liu J. Efficient inner filter effect of gold nanoparticles on the fluorescence of CdS quantum dots for sensitive detection of melamine in raw milk. Food Control 2013, 34:221-229.
10. Pan X.D., Wu P.G., Yang D.J., Wang L.Y., Shen X.H., Zhu C.Y. Simultaneous determination of melamine and cyanuric acid in dairy products by mixed-mode solid phase extraction and GC-MS. Food Control 2013, 30:545-548.
11. Rambla-Alegre M., Peris-Vicente J., Marco-Peiró S., Beltrán-Martinavarro B., Esteve-Romero J. Development of an analytical methodology to quantify melamine in milk using micellar liquid chromatography and validation according to EU Regulation 2002/654/EC. Talanta 2010, 81:894-900.
12. W.H.Organization available at, (accessed October 10th, 2013). http://www.who.int.
13. U.S.F.D.A available at, (accessed October 10th, 2013). http://www.fda.gov.
14. Sun F., Ma W., Xu L., Zhu Y., Liu L., Peng C., Wang L., Kuang H., Xu C. Analytical methods and recent developments in the detection of melamine. Trends Anal. Chem. 2010, 29:1239-1249.
15. Saint-Denis T., Goupy J. Optimization of a nitrogen analyser based on the Dumas method. Anal. Chim. Acta. 2004, 515:191-198.
16. Wen Y., Liu H., Han P., Gao Y., Luan F., Li X. Determination of melamine in milk powder, milk and fish feed by capillary electrophoresis: a good alternative to HPLC. J. Sci. Food Agric. 2010, 90:2178-2182.
17. Filazi A., Sireli U.T., Ekici H., Can H.Y., Karagoz A. Determination of melamine in milk and dairy products by high performance liquid chromatography. J. Dairy Sci. 2012, 95:602-608.
18. 2 column. Food Control 2012, 23:245-250.
19. Chao Y.Y., Lee C.T., Wei Y.T., Kou H.S., Huang Y.L. Using an on-line microdialysis/HPLC system for the simultaneous determination of melamine and cyanuric acid in non-dairy creamer. Anal. Chim. Acta. 2011, 702:56-61.
20. Sun H., Wang L., Ai L., Liang S., Wu H. A sensitive and validated method for determination of melamine residue in liquid milk by reversed phase high-performance liquid chromatography with solid-phase extraction. Food Control 2010, 21:686-691.
21. Khedr A. Optimized extraction method for LC-MS determination of bisphenol A, melamine and di(2-ethylhexyl) phthalate in selected soft drinks, syringes, and milk powder. J. Chromatogr. B 2013, 930:98-103.
22. Guo C.Y., Wang H.Y., Liu X.P., Fan L.Y., Zhang L., Cao C.X. Fast and selective determination of total protein in milk powder via titration of moving reaction boundary electrophoresis. Electrophoresis 2013, 34:1343-1351.
23. Ono S., Funato T., Inoue Y., Munechika T., Yoshimura T., Morita H., Rengakuji S.-I., Shimasaki C. Determination of melamine derivatives, melame, meleme, ammeline and ammelide by high-performance cation-exchange chromatography. J. Chromatogr. A 1998, 815:197-204.
24. Su X., Zhou H.Y., Chen F.C., Gao B.X., Liu Z.W., Zhang Y.H., Liu F., Liu F., Li Z.R., Gao Z.X. Modified SBA-15 matrices for high-throughput screening of melamine in milk samples by MALDI-TOF MS. Int. J. Mass Spectrom. 2013, 338:39-44.
25. Zeng H.J., Yang R., Wang Q.W., Li J.J., Qu L.B. Determination of melamine by flow injection analysis based on chemiluminescence system. Food Chem. 2011, 127:842-846.
26. Zhang J., Wu M., Chen D., Song Z. Ultrasensitive determination of melamine in milk products and biological fluids by luminol-hydrogen peroxide chemiluminescence. J. Food Compos. Anal. 2011, 24:1038-1042.
27. Fodey T.L., Thompson C.S., Traynor I.M., Haughey S.A., Kennedy D.G., Crooks S.R.H. Development of an optical biosensor based immunoassay to screen infant formula milk samples for adulteration with melamine. Anal. Chem. 2011, 83:5012-5016.
28. Feng W., Lv C., Yang L., Cheng J., Yan C. Determination of melamine concentrations in dairy samples. LWT Food Sci. Technol. 2012, 47:147-153.
29. Chocholouš P., Solich P., Šatínský D. An overview of sequential injection chromatography. Anal. Chim. Acta. 2007, 600:129-135.