Determination of myo-inositol in infant formulae and milk powders using capillary gas chromatography with flame ionisation detection

International Dairy Journal

Volumn 37, Issue 2, 2014, Pages 74-81

  Woollard, David C ^a   Macfadzean, Craig ^b   Indyk, Harvey E ^c   McMahon, Adrienne ^d   Christiansen, Scott ^e  

^a R J Hill Laboratories Ltd   (New Zealand)

^b New Zealand MetService Ltd   (New Zealand)

^c FONTERRA RESEARCH CENTRE   (New Zealand)

^d Wyeth Nutrition   (Ireland)

^e Perrigo PBM Nutritionals   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ALCOHOLS; GAS CHROMATOGRAPHY; POWDERS; SUGARS;

CAPILLARY GAS CHROMATOGRAPHY; CURRENT REGULATIONS; DETECTION METHODS; INFANT FORMULAE; INOSITOL HEXAPHOSPHATE; LABORATORY METHODS; RELATIVE STANDARD DEVIATIONS; REPRODUCIBILITIES;

POLYOLS;

EID: 84899809650     PISSN: 09586946     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.idairyj.2014.03.004     Document Type: Article

References (31)

1. Baker H., DeAngelis B., Baker E.R., Khalil M., Reddi A.S., Frank O. Routine microbiological assay for myo inositol for clinical use. Journal of Micronutrient Analysis 1990, 8:223-232.
2. Beemster P., Groenen P., Steegers-Theunissen R. Involvement of inositol in reproduction. Nutrition Reviews 2002, 60:80-87.
3. Byun S.M., Jenness R. Estimation of free myo-inositol in milks of various species and its source in milk of rats (Rattus norvegicus). Journal of Dairy Science 1982, 65:531-536.
4. Campbell J.A., Goheen S.C., Donald P.A. Extraction and analysis of inositols and other carbohydrates from soybean plant tissues. Recent trends for enhancing the diversity and quality of soybean products 2011, 421-446. InTech, Rijeka, Croatia, Available from. http://www.intechopen.com/books, D. Krezhova (Ed.).
5. Chen Q. Determination of phytic acid and inositol pentakisphosphates in foods by high-performance ion chromatography. Journal of Agricultural and Food Chemistry 2004, 52:4604-4613.
6. Clements R.S., Darnell B. Myo-inositol content of common foods: development of a high-myo-inositol diet. American Journal of Clinical Nutrition 1980, 33:1954-1967.
7. Ellingson D., Pritchard T., Foy P., King K., Mitchell B., Austad J., et al. Analysis of free and total myo-inositol in foods, feeds, and infant formula by high-performance anion exchange chromatography with pulsed amperometric detection, including a novel total extraction using microwave-assisted acid hydrolysis and enzymatic treatment. Journal AOAC International 2012, 95:1469-1478.
8. Feth F., Wagner R., Baydoun H., Wagner K.G. Enzyme assay of l-myo-inositol 1-phosphate synthetase based on high performance liquid chromatography of benzoylated inositol. Analytical Biochemistry 1989, 178:135-136.
9. Fisher S.K., Novak J.E., Agranoff B.W. Inositol and higher inositol phosphates in neural tissues: homeostasis, metabolism and functional significance. Journal of Neurochemistry 2002, 82:736-754.
10. Flores M.I.A., Moreno J.L.F., Frenich A.G., Vidal J.L.M. Fast determination of myo-inositol in milk powder by ultra high performance liquid chromatography coupled to tandem mass spectrometry. Food Chemistry 2011, 129:1281-1286.
11. Frieler R.A., Mitteness D.J., Golovko M.Y., Giener H.M., Rosenberger T.A. Quantitative determination of free glycerol and myo-inositol from plasma and tissue by high performance liquid chromatography. Journal of Chromatography B 2009, 877:3667-3672.
12. Indyk H., Lawrence R., Broda D. The micronutrient content of bovine whole milk powder: influence of pasture feeding and season. Food Chemistry 1993, 46:389-396.
13. Indyk H.E., Woollard D.C. Determination of free myo-inositol in milk and infant formula by high-performance liquid chromatography. Analyst 1994, 119:397-402.
14. Kerovuo J., Rouvinen J., Hatzack F. Analysis of myo-inositol hexakisphosphate hydrolysis by Bacillus phytase: indication of a novel reaction mechanism. Journal of Biochemistry 2000, 352:623-628.
15. Kindt E., Shum Y., Badura L., Snyder P.J., Brant A., Fountain S., et al. Development and validation of an LC/MS/MS procedure for the quantification of endogenous myo-inositol concentrations in rat brain tissue homogenates. Analytical Chemistry 2004, 76:4901-4908.
16. de Koning A.J. Determination of myo-inositol and phytic acid by gas chromatography using scyllitol as internal standard. Analyst 1994, 119:1319-1322.
17. Lauro P.N., Craven P.A., DeRubertis F.R. Two-step high performance liquid chromatography method for the determination of myo-inositol and sorbitol. Analytical Biochemistry 1989, 178:331-335.
18. Lehrfeld J. High-performance liquid chromatography analysis of phytic acid on a pH-stable, macroporous polymer column. Cereal Chemistry 1989, 66:510-515.
19. March J.G., Forteza R., Grases F. Determination of inositol isomers and arabitol in human urine by gas chromatography-mass spectrometry. Chromatographica 1996, 42:329-331.
20. Michell R.H. Inositol derivatives: evolution and functions. Nature Reviews, Molecular Cell Biology 2008, 9:151-161.
21. Ogasa K., Kuboyama M., Kiyosawa I., Suzuki T., Itoh M. The content of free and bound inositol in human and cow's milk. Journal of Nutritional Science and Vitaminology (Tokyo) 1975, 21:129-135.
22. Pereira G.R., Baker L., Egler J., Corcoran L., Chiavacci R. Serum myo-inositol concentrations in premature infants fed human milk, formula for infants, and parenteral nutrition. American Journal of Clinical Nutrition 1990, 51:589-593.
23. Perello J., Isern B., Costa-Bauza A., Grases F. Determination of myo-inositol in biological samples by liquid chromatography-mass spectrometry. Journal of Chromatography B 2004, 802:367-370.
24. Poole C.F. Alkylsilyl derivatives for gas chromatography. Journal of Chromatography A 2013, 1296:2-14.
25. Sanders A.-S., Ahderine R. HPLC method for determination of inositol tri-, tetra-, penta- and hexaphosphates in foods and intestinal contents. Journal of Food Science 1986, 51:547-550.
26. Schimpf K., Thompson L., Baugh S. Determination of myo-inositol (free and bound as phosphatidylinositol) in infant formula and adult nutritionals by liquid chromatography/pulse amperometry with column switching. Journal AOAC International 2012, 95:1-6.
27. Shears S.B. How versatile are inositol phosphate kinases?. Journal of Biochemistry 2004, 377:265-280.
28. Tagliaferri E.G., Bonetti G., Blake C.J. Ion chromatographic determination of inositol in infant formulae and clinical products for enteral feeding. Journal of Chromatography A 2000, 879:129-135.
29. Troyano E., Villamiel M., Olano A., Sanz J., Martinez-Castro I. Monosaccharides and myo-inositol in commercial milks. Journal of Agricultural and Food Chemistry 1996, 44:815-817.
30. Wang W.-T., Safar J., Zopf D. Analysis of inositol by high performance liquid chromatography. Analytical Biochemistry 1990, 188:432-435.
31. Yang N., Ren G. Determination of d-chiro-inositol in tartary buckwheat using high performance liquid chromatography with an evaporative light scattering detector. Journal of Agricultural and Food Chemistry 2008, 56:757-760.