Rapid, high performance method for the determination of vitamin K1, menaquinone-4 and vitamin K1 2,3-epoxide in human serum and plasma using liquid chromatography-hybrid quadrupole linear ion trap mass spectrometry

Journal of Chromatography A

Volumn 1338, Issue , 2014, Pages 102-110

  Gentili, Alessandra ^a   Cafolla, Arturo ^a   Gasperi, Tecla ^b   Bellante, Simona ^a   Caretti, Fulvia ^a   Curini, Roberta ^a   Fernández, Virginia Pérez ^a  

^a SAPIENZA UNIVERSITY OF ROME   (Italy)

^b ROMA TRE UNIVERSITY   (Italy)

Author keywords

HPLC MS; Human serum and plasma; Menaquinone 4; Phylloquinone; Phylloquinone epoxide

Indexed keywords

ATMOSPHERIC IONIZATION; ATMOSPHERIC PRESSURE; DRUG PRODUCTS; HISTOLOGY; KETONES; LIPIDS; MAMMALS; MASS SPECTROMETRY; METABOLITES; PATIENT MONITORING; PATIENT TREATMENT; QUINONE; TISSUE;

ATMOSPHERIC PRESSURE CHEMICAL IONIZATION; HPLC-MS; HUMAN SERUM; LINEAR ION TRAP MASS SPECTROMETRIES; MENAQUINONE-4; MULTIPLE-REACTION MONITORING MODES; ORAL ANTICOAGULANT THERAPIES; PHYLLOQUINONE;

LIQUID CHROMATOGRAPHY;

MENATETRENONE; PHYTOMENADIONE; PHYTOMENADIONE OXIDE;

ANALYSIS; ANTICOAGULANT THERAPY; ARTICLE; CLINICAL ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; CORRELATION COEFFICIENT; FEMALE; HUMAN; HUMAN EXPERIMENT; INTERNATIONAL NORMALIZED RATIO; ION TRAP MASS SPECTROMETRY; LIMIT OF DETECTION; LIQUID CHROMATOGRAPHY; LIQUID CHROMATOGRAPHY HYBRID QUADRUPOLE LINEAR IONTRAP MASS SPECTROMETRY; LOWER LIMIT OF QUANTITATION; MALE; MULTIPLE REACTION MONITORING; NORMAL HUMAN; PLASMA; PRIORITY JOURNAL; SENSITIVITY AND SELECTIVITY; SERUM; VALIDATION PROCESS;

MAMMALIA;

HPLC-MS; HUMAN SERUM AND PLASMA; MENAQUINONE-4; PHYLLOQUINONE; PHYLLOQUINONE-EPOXIDE;

CHROMATOGRAPHY, HIGH PRESSURE LIQUID; EPOXY COMPOUNDS; HUMANS; TANDEM MASS SPECTROMETRY; TIME FACTORS; VITAMIN K; VITAMIN K 1; VITAMIN K 2; VITAMINS;

EID: 84897089002     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2014.02.065     Document Type: Article

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