Rapid determination of eight bioactive alkaloids in Portulaca oleracea L. by the optimal microwave extraction combined with positive-negative conversion multiple reaction monitor (+/-MRM) technology

Talanta

Volumn 120, Issue , 2014, Pages 167-172

  Liang, Xiao ^a   Tian, Jinlong ^a   Li, Lingzhi ^a   Gao, Jun ^b   Zhang, Qingyi ^b   Gao, Pinyi ^a   Song, Shaojiang ^a  

^a SHENYANG PHARMACEUTICAL UNIVERSITY   (China)

^b Liaoning Chengda Biotechnology Co Ltd   (China)

Author keywords

Alkaloids; Microwave extraction; Portulaca oleracea L.; Quantitative analysis

Indexed keywords

ALKALOIDS; CHEMICAL ANALYSIS; ELECTROSPRAY IONIZATION; EXTRACTION; MASS SPECTROMETRY; METABOLITES; MICROWAVES;

CALIBRATION CURVES; ELECTROSPRAY IONIZATION TANDEM MASS SPECTROMETRY; EXTRACTION RECOVERY; MICROWAVE EXTRACTION; OPTIMAL MICROWAVE; PORTULACA OLERACEA; REPRODUCIBILITIES; TRIPLE QUADRUPOLE LINEAR ION TRAP MASS SPECTROMETRIES;

ORGANIC SOLVENTS;

ALKALOID;

ARTICLE; CALIBRATION; CHEMISTRY; ELECTROSPRAY MASS SPECTROMETRY; EQUIPMENT; FRACTIONATION; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METHODOLOGY; MICROWAVE EXTRACTION; MICROWAVE RADIATION; PORTULACA; PORTULACA OLERACEA L.; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; TANDEM MASS SPECTROMETRY; UPLC-(+/-)MRM; VALIDATION STUDY;

ALKALOIDS; MICROWAVE EXTRACTION; PORTULACA OLERACEA L.; QUANTITATIVE ANALYSIS; UPLC-(+/-)MRM;

ALKALOIDS; CALIBRATION; CHEMICAL FRACTIONATION; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; MICROWAVES; PORTULACA; REPRODUCIBILITY OF RESULTS; SPECTROMETRY, MASS, ELECTROSPRAY IONIZATION; TANDEM MASS SPECTROMETRY;

EID: 84896524899     PISSN: 00399140     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.talanta.2013.11.067     Document Type: Article

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