A toolbox of HSQC experiments for small molecules at high 13C-enrichment. Artifact-free, fully 13C-homodecoupled and JCC-encoding pulse sequences

Magnetic Resonance in Chemistry

Volumn 51, Issue 12, 2013, Pages 808-814

  Foroozandeh, Mohammadali ^a   Giraudeau, Patrick ^b   Jeannerat, Damien ^a  

^a UNIVERSITY OF GENEVA   (Switzerland)

^b Centre National de la Recherche Scientifique   (France)

Author keywords

broadband homonuclear decoupling; carbon carbon coupling; HSQC; NMR; spatial encoding

Indexed keywords

CARBON; MOLECULES; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SIGNAL ENCODING;

BROADBAND HOMONUCLEAR DECOUPLING; CARBON-CARBON COUPLING; ENCODINGS; HIGH-ORDER; HOMONUCLEAR DECOUPLING; HSQC; PULSE SEQUENCE; SELECTIVE PULSE; SMALL MOLECULES; SPATIAL ENCODING;

ENCODING (SYMBOLS);

CARBON; CARBON 13; CHOLESTEROL;

13C-ENRICHMENT; 1H; ARTICLE; BROADBAND HOMONUCLEAR DECOUPLING; CARBON-CARBON COUPLING; CHEMICAL STRUCTURE; CHEMISTRY; HETERONUCLEAR SINGLE QUANTUM COHERENCE; NUCLEAR MAGNETIC RESONANCE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SPATIAL ENCODING; STANDARD;

13C; 13C-ENRICHMENT; 1H; BROADBAND HOMONUCLEAR DECOUPLING; CARBON-CARBON COUPLING; HSQC; NMR; SPATIAL ENCODING;

CARBON ISOTOPES; CHOLESTEROL; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR STRUCTURE; REFERENCE STANDARDS;

EID: 84887447310     PISSN: 07491581     EISSN: 1097458X     Source Type: Journal    
DOI: 10.1002/mrc.4019     Document Type: Article

References (48)

1. J. M. Hagel, P. J. Facchini,. Phytochem. Rev. 2008, 7, 479.
2. I. Werner, A. Bacher, W. Eisenreich,. J. Biol. Chem. 1997, 25474.
3. W. van Winden, D. Schipper, P. Verheijen, J. Heijnen,. Metab. Eng. 2001, 3, 322.
4. J.-P. Grivet, A.-M. Delort, J.-C. Portais,. Biochimie 2003, 85, 823.
5. U. Mocek, H. G. Floss, in Encyclopedia of Magnetic Resonance, (Eds:, R. K. Harris, R. E. Wasylishen,), John Wiley, Chichester, 2007.
6. M. A. McCoy, L. Mueller,. J. Am. Chem. Soc. 1992, 114, 2108.
7. J. Santoro, G. C. King,. J. Magn. Reson. 1992, 97, 202.
8. P. Jesson, P. Meakin, G. J. Kneissel,. J. Am. Chem. Soc. 1973, 95, 618.
9. A. P. D. M. Espindola, R. Crouch, J. R. DeBergh, J. M. Ready, J. B. MacMillan,. J. Am. Chem. Soc. 2009, 131, 15994.
10. T. Fujiwara, K. Nagayama,. J. Magn. Reson. 1988, 77, 53.
11. J. Huth, N. D. Kurur, G. Bodenhausen,. J. Magn. Reson. Ser. A 1996, 118, 286.
12. B. Baishya, T. F. Segawa, G. Bodenhausen,. J. Magn. Reson. 2011, 211, 240.
13. P. Mutzenhardt, F. Guenneau, D. Canet,. J. Magn. Reson. 1999, 141, 312.
14. M. Woodley, R. Freeman,. J. Magn. Reson. Ser. A 1994, 109, 103.
15. A. J. Pell, J. Keeler,. J. Magn. Reson. 2007, 189, 293.
16. A. J. Pell, R. A. E. Edden, J. Keeler,. Magn. Reson. Chem. 2007, 45, 296.
17. B. Haase, W. Bermel,. J. Magn. Reson. 2009, 199, 192.
18. K. Zangger, H. Sterk,. J. Magn. Reson. 1997, 124, 486.
19. P. Giraudeau, S. Akoka,. J. Magn. Reson. 2008, 195, 9.
20. B. Shapira, A. Lupulescu, Y. Shrot, L. Frydman,. J. Magn. Reson. 2004, 166, 152.
21. J. A. Aguilar, S. Faulkner, M. Nilsson, G. A. Morris,. Angew. Chem. Int. Ed. 2010, 49, 3901.
22. M. Nilsson, G. A. Morris,. Chem. Commun. 2007, 933.
23. J. A. Aguilar, A. A. Colbourne, J. Cassani, M. Nilsson, G. A. Morris,. Angew. Chem. Int. Ed. 2012, 51, 6460.
24. G. A. Morris, J. A. Aguilar, R. Evans, S. Haiber, M. Nilsson,. J. Am. Chem. Soc. 2010, 132, 12770.
25. N. Giraud, L. Béguin, J. Courtieu, D. Merlet,. Angew. Chem. Int. Ed. 2010, 49, 3481.
26. N. Giraud, M. Joos, J. Courtieu, D. Merlet,. Magn. Reson. Chem. 2009, 47, 300.
27. M. Foroozandeh, P. Giraudeau, D. Jeannerat,. ChemPhysChem 2011, 12, 2409.
28. L. Kay, P. Keifer, T. Saarinen,. J. Am. Chem. Soc. 1992, 114, 10663.
29. A. G. Palmer, J. Cavanagh, P. E. Wright, M. Rance,. J. Magn. Reson. 1991, 93, 151.
30. R. Shivapurkar, C. M. Souza, D. Jeannerat, H. Riezman,. J. Lipid Res. 2011, 52, 1062.
31. F. A. A. Mulder, R. Otten, U. M. Scheek,. J. Biomol. NMR 2011, 51, 199.
32. E. Kupče, J. Boyd, I. D. Campbell,. J. Magn. Reson. Ser. B 1995, 106, 300.
33. R. Burger, P. Bigler,. J. Magn. Reson. 1998, 135, 529.
34. J.-M. Nuzillard,. Molecular Physics 2007, 105, 2243.
35. S. Bourg, J.-M. Nuzillard,. J. Magn. Res 1998, 133, 173.
36. A. Bax, D. Max, D. Zax,. J. Am. Chem. Soc. 1992, 114, 6923.
37. V. Blechta, R. Freeman,. J. Magn. Reson. Ser. A 1993, 102, 253.
38. E. Fukushi, J. Kawabata,. Magn. Reson. Chem. 2006, 44, 475.
39. J.-S. Hu, A. Bax,. J. Am. Chem. Soc. 1996, 118, 8170.
40. L. Jin, K. E. Kövér, M. R. Lenoir, D. Uhrín,. J. Magn. Reson. 2008, 190, 171.
41. K. E. Kövér, P. Forgõ,. J. Magn. Reson. 2004, 166, 47.
42. H. Schwalbe, A. Rexroth, U. Eggenberger, T. Geppert, C. Griesinger,. J. Am. Chem. Soc. 1993, 115, 7878.
43. J. J. Titman, J. Keeler,. J. Magn. Reson. 1990, 89, 640.
44. G. W. Vuister, A. C. Wang, A. Bax,. J. Am. Chem. Soc. 1993, 115, 5334.
45. S. R. Walter, J. L. Marshall, C. R. McDaniel, E. D. Canada, M. Barfield,. J. Am. Chem. Soc. 1983, 105, 4185.
46. G. T. Montelione, S. D. Emerson, B. A. Lyons,. Biopolymers 1992, 32, 327.
47. G. T. Montelione, M. Winkler, E. Rinderknecht, G. Wagner,. J. Magn. Reson. 1989, 82, 198.
48. C. Griesinger, O. W. Sorensen, R. R. Ernst,. J. Magn. Reson. 1987, 75, 474.