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Volumn 131, Issue 44, 2009, Pages 15994-15995

Deconvolution of complex NMR spectra in small molecules by multi frequency homonuclear decoupling (MDEC)

Author keywords

[No Author keywords available]

Indexed keywords

CHOLESTERYL ACETATE; COMPLEX 1; COUPLING CONSTANTS; HOMONUCLEAR DECOUPLING; MULTI FREQUENCY; NMR SPECTRUM; SELECTIVE PULSE; SINGLE PULSE; SMALL MOLECULES; SPECIFIC PROBLEMS;

EID: 70450184415     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja907110e     Document Type: Article
Times cited : (28)

References (20)
  • 10
    • 70450210739 scopus 로고    scopus 로고
    • note
    • The resolution of the multiplet at δ 0.99 ppm is sufficient to measure the four coupling constants. We chose this signal as a clear example of how the MDEC experiment can reduce the complexity.
  • 13
    • 62649128998 scopus 로고    scopus 로고
    • For selective excitation experiments in natural products, see
    • For selective excitation experiments in natural products, see: (a) Morinaka, B. I.; Pawlik, J. R.; Molinski, T. F. J. Nat. Prod. 2009, 72, 259-264
    • (2009) J. Nat. Prod. , vol.72 , pp. 259-264
    • Morinaka, B.I.1    Pawlik, J.R.2    Molinski, T.F.3
  • 16
    • 70450215452 scopus 로고    scopus 로고
    • note
    • The synthetic and stereochemical analysis of the C16 fatty acids and their relationship to nigricanoside A will be published in due course.
  • 20
    • 70450219683 scopus 로고    scopus 로고
    • note
    • A stepwise procedure for acquiring the MDEC experiment and the 1D-TOCSY MDEC experiment is included in the Supporting Information.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.