Experimental access to HSQC spectra decoupled in all frequency dimensions

Journal of Magnetic Resonance

Volumn 199, Issue 2, 2009, Pages 192-198

  Sakhaii, Peyman ^a   Haase, Burkhard ^a   Bermel, Wolfgang ^b  

^a SANOFI AVENTIS DEUTSCHLAND GMBH   (Germany)

^b BRUKER BIOSPIN GMBH   (Germany)

Author keywords

Constant time acquisition; Frequency dependent folding; Homodecoupling; Pure shift spectra; SHARC

Indexed keywords

CONSTANT TIME ACQUISITION; FREQUENCY DEPENDENT FOLDING; HOMODECOUPLING; PURE SHIFT SPECTRA; SHARC;

CHEMICAL SHIFT; DATA PROCESSING; MERGERS AND ACQUISITIONS; SPIN DYNAMICS;

PROTONS;

PROTON;

ALGORITHM; ARTICLE; CHEMICAL MODEL; COMPUTER SIMULATION; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

ALGORITHMS; COMPUTER SIMULATION; MAGNETIC RESONANCE SPECTROSCOPY; MODELS, CHEMICAL; PROTONS;

EID: 67649670116     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2009.04.016     Document Type: Article

References (32)

1. Aue W.P., Karhan J., and Ernst R.R. Homonuclear broadband decoupling and two-dimensional J-resolved NMR spectroscopy. J. Chem. Phys. 64 (1976) 4226-4227
2. Shaka A.J., Keeler J., Frenkiel T., and Freeman R. An improved sequence for broadband decoupling: WALTZ-16. J. Magn. Reson. 52 (1983) 335-338
3. Shaka A.J., Barker P.B., and Freeman R. Computer-optimized decoupling scheme for wideband applications and low-level operations. J. Magn. Reson. 64 (1985) 547-552
4. Jesson P., Meakin P., and Kneissel G.J. Homonuclear decoupling and peak elimination in Fourier transform nuclear magnetic resonance. J. Am. Chem. Soc. 95 (1973) 618-620
5. 1H NMR spectroscopy by homonuclear semiselective shaped pulse decoupling during acquisition. J. Am. Chem. Soc. 116 (1994) 8847-8848
6. Weigelt J., Hammarstroem A., Bermel W., and Otting G. Removal of Zero-Quantum coherence in protein NMR spectra using SESAM decoupling and suppression of decoupling sidebands. J. Magn. Reson. B110 (1996) 219-224
7. E. Kupce, H. Matsuo, G. Wagner, in: Biological Magnetic Resonance, vol. 16, Modern Techniques in protein NMR (Chapter 5), Homonuclear Decoupling in Proteins, 1999, pp. 149-193.
8. Morris G.A., and Freeman R. Selective excitation in Fourier transform nuclear magnetic resonance. J. Magn. Reson. 29 (1978) 433-462
9. Nagayama K., Bachmann P., Wuethrich K., and Ernst R.R. The use of cross-sections and of projections in two-dimensional NMR spectroscopy. J. Magn. Reson. 31 (1978) 133-148
10. Nuzillard J.-M. Time-reversal of NMR signals by linear prediction. Application to phase-sensitive homonuclear J-resolved spectroscopy. J. Magn. Reson. A 118 (1996) 132-135
11. Simova S., Sengstschmid H., and Freeman R. Proton chemical-shift spectra. J. Magn. Reson. 124 (1997) 104-121
12. Naganagowda G.N. Spectral simplification and "pseudo decoupling" in one-dimensional proton NMR spectra using pulsed-field gradients. J. Magn. Reson. A 118 (1996) 113-116
13. Pell A.J., Edden R.A.E., and Keeler J. Broad band proton-decoupled proton spectra. Magn. Reson. Chem. 45 (2007) 296-316
14. Harris G.J., Lowe S.R., and Norwood T.J. In-phase selective excitation of overlapping multiplets. J. Magn. Reson. 142 (2000) 389-392
15. Hall L.D., and Norwood T.J. A chemical-shift selective filter. J. Magn. Reson. 76 (1988) 548-554
16. Hall L.D., and Norwood T.J. An improved chemical-shift selective filter. J. Magn. Reson. 78 (1988) 582-587
17. Robinson P.T., Pham T.N., and Uhrin D. In phase selective excitation of overlapping multiplets by gradient-enhanced chemical shift selective filters. J. Magn. Reson. 170 (2004) 97-103
18. 1H decoupling in two-dimensional NMR spectroscopy. J. Magn. Reson. 78 (1988) 178-185
19. Zangger K., and Sterk H. Homonuclear broadband-decoupled NMR spectra. J. Magn. Reson. 124 (1997) 486-489
20. Giraudeau P., and Akoka S. Sources of sensitivity losses in ultra fast 2D NMR. J. Magn. Reson. 192 (2008) 151-158
21. Pell A.J., and Keeler J. Two-dimensional J-spectra with absorption-mode lineshapes. J. Magn. Reson. 189 (2007) 293-299
22. 1H spectra without multiplet structure. Chem. Commun. (2007) 933-935
23. Santoro J., and King G.C. A constant-time 2D overbodenhausen experiment for inverse correlation of isotopically enriched species. J. Magn. Reson. 97 (1992) 202-207
24. Bax A., Mehlkopf A.F., and Smidt J. Homonuclear broadband-decoupled absorption spectra, with line widths which are independent of the transverse relaxation rate. J. Magn. Reson. 35 (1979) 167-169
25. Garbow J.R., Weitekamp D.P., and Pines A. Bilinear rotation decoupling of homonuclear scalar interactions. Chem. Phys. Lett. 93 (1982) 504-509
26. Uhrin D., Liptaj T., and Koever K. Modified BIRD pulses and design of heteronuclear pulse sequences. J. Magn. Reson. A 101 (1993) 41-46
27. Uhrin D. 3D HSQC-HSQMBC - increasing the resolution of long-range proton-carbon correlation experiments. J. Magn. Reson. 159 (2002) 145-150
28. Bax A. Broadband homonuclear decoupling in heteronuclear shift correlation NMR spectroscopy. J. Magn. Reson. 53 (1983) 517-520
29. Sakhaii P., Haase B., and Bermel W. An alternative approach for recording of multidimensional NMR data based on frequency dependent folding. J. Magn. Reson. 191 (2008) 291-303
30. Boehlen J.M., and Bodenhausen G. Experimental aspects of chirp NMR spectroscopy. J. Magn. Reson. A 102 (1993) 293-301
31. Hwang T.L., van Zijl P.C.M., and Garwood M. Broadband adiabatic refocusing without phase distortion. J. Magn. Reson. 124 (1997) 250-254
32. Fu R., and Bodenhausen G. Broadband decoupling in NMR with frequency-modulated chirp pulses. Chem. Phys. Lett. 245 (1995) 415-420