A validated analytical method to study the long-term stability of natural and synthetic glucocorticoids in livestock urine using ultra-high performance liquid chromatography coupled to orbitrap-high resolution mass spectrometry

Journal of Chromatography A

Volumn 1301, Issue , 2013, Pages 111-121

  De Clercq, Nathalie ^a   Julie, Vanden Bussche ^a   Croubels, Siska ^a   Delahaut, Philippe ^b   Vanhaecke, Lynn ^a  

^a GHENT UNIVERSITY   (Belgium)

^b CER Groupe   (Belgium)

Author keywords

Glucocorticoids; Plackett Burman; Stability study; Ultra high performance liquid chromatography Orbitrap high resolution mass spectrometry; Urine

Indexed keywords

GLUCOCORTICOIDS; PLACKETT-BURMAN; STABILITY STUDY; ULTRA-HIGH PERFORMANCE; URINE;

AGRICULTURE; BODY FLUIDS; CHROMATOGRAPHY; EXTRACTION; FOOD PRODUCTS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MAMMALS; MASS SPECTROMETRY; OPTIMIZATION; STABILITY;

HORMONES;

CORTISONE; DIHYDROCORTISONE; GLUCOCORTICOID; HYDROCORTISONE; METHYLPREDNISOLONE; PREDNISOLONE; PREDNISONE; UNCLASSIFIED DRUG;

ANALYTICAL PARAMETERS; ARTICLE; CONCENTRATION (PARAMETERS); CONTROLLED STUDY; COW; DEGRADATION; LIMIT OF DETECTION; LIMIT OF QUANTITATION; LIVESTOCK; MASS SPECTROMETRY; NONHUMAN; PH; PRIORITY JOURNAL; STORAGE TEMPERATURE; ULTRA PERFORMANCE LIQUID CHROMATOGRAPHY; URINALYSIS; VALIDATION PROCESS;

GLUCOCORTICOIDS; PLACKETT-BURMAN; STABILITY STUDY; ULTRA-HIGH PERFORMANCE LIQUID CHROMATOGRAPHY-ORBITRAP-HIGH RESOLUTION MASS SPECTROMETRY; URINE;

ANIMALS; CATTLE; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; DRUG STABILITY; FECES; GLUCOCORTICOIDS; HYDROGEN-ION CONCENTRATION; LIMIT OF DETECTION; LINEAR MODELS; MASS SPECTROMETRY; REPRODUCIBILITY OF RESULTS; TEMPERATURE;

ANIMALIA; BOVINAE;

EID: 84879884714     PISSN: 00219673     EISSN: 18733778     Source Type: Journal    
DOI: 10.1016/j.chroma.2013.05.066     Document Type: Article

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