Optimization of solid phase extraction clean up and validation of quantitative determination of corticosteroids in urine by liquid chromatography-tandem mass spectrometry

Analytica Chimica Acta

Volumn 617, Issue 1-2, 2008, Pages 216-224

  Andersen, Jens Hinge ^a   Hansen, Lene Gram ^a   Pedersen, Mikael ^a  

^a TECHNICAL UNIVERSITY OF DENMARK   (Denmark)

Author keywords

Corticosteroids; Ion suppression; Liquid chromatography tandem mass spectrometry; Urine; Validation

Indexed keywords

DRUG PRODUCTS; ELECTROSPRAY IONIZATION; LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY;

CORTICOSTEROIDS; ION SUPPRESSION; SOLID PHASE EXTRACTION;

HORMONES;

ARYLSULFATASE; BECLOMETASONE; BETA GLUCURONIDASE; BETAMETHASONE; CORTICOSTEROID; DEXAMETHASONE; FLUMETASONE; FLUOCINOLONE ACETONIDE; METHYLPREDNISOLONE; PREDNISOLONE; PREDNISONE; TRIAMCINOLONE ACETONIDE;

ANIMAL EXPERIMENT; ANION EXCHANGE; ARTICLE; CONJUGATION; COW; ELECTROSPRAY MASS SPECTROMETRY; HELIX POMATIA; LIQUID CHROMATOGRAPHY; NONHUMAN; PRIORITY JOURNAL; QUANTITATIVE ANALYSIS; REPRODUCIBILITY; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; SOLID PHASE EXTRACTION; STANDARD; SWINE; TANDEM MASS SPECTROMETRY; URINE; VALIDATION PROCESS;

ADRENAL CORTEX HORMONES; ALKALIES; ANIMALS; BIOLOGICAL PRODUCTS; CALIBRATION; CHROMATOGRAPHY, LIQUID; HYDROGEN-ION CONCENTRATION; IONS; MOLECULAR STRUCTURE; MOLECULAR WEIGHT; SENSITIVITY AND SPECIFICITY; SOLID PHASE EXTRACTION; TANDEM MASS SPECTROMETRY;

ANIMALIA; BOVINAE; HELIX POMATIA; SUS;

EID: 43849090377     PISSN: 00032670     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.aca.2008.02.070     Document Type: Article

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