Lactide cyclopolymerization kinetics, X-ray structure, and solution dynamics of (tBu-SalAmEE)Al and a cautionary tale of polymetalate formation

Macromolecules

Volumn 46, Issue 9, 2013, Pages 3273-3279

  Reisberg, Solomon H ^a   Hurley, Harry J ^a   Mathers, Robert T ^b   Tanski, Joseph M ^c   Getzler, Yutan D Y L ^a  

^a KENYON COLLEGE   (United States)

^b PENNSYLVANIA STATE UNIVERSITY   (United States)

^c VASSAR COLLEGE   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BRIDGING LIGANDS; CAUTIONARY TALES; COORDINATION INSERTION MECHANISM; CYCLOPOLYMERIZATION; POLYMERIZATION KINETICS; POLYMERIZATION OF LACTIDE; RATE DETERMINING STEP; SOLUTION DYNAMICS;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POLYMERIZATION; THERMOGRAVIMETRIC ANALYSIS;

X RAYS;

EID: 84877743579     PISSN: 00249297     EISSN: None     Source Type: Journal    
DOI: 10.1021/ma400046x     Document Type: Article

References (69)

1. Greenwood, N. N.; Earnshaw, A. Chemistry of the Elements, 2 nd ed.; Butterworth-Heinemann: Oxford, U.K., 1997.
2. Church, T. L.; Getzler, Y. D. Y. L.; Coates, G. W. J. Am. Chem. Soc. 2006, 128, 10125-10133
3. Rowley, J. M.; Lobkovsky, E. B.; Coates, G. W. J. Am. Chem. Soc. 2007, 129, 4948-4960
4. Church, T. L.; Byrne, C. M.; Lobkovsky, E. B.; Coates, G. W. J. Am. Chem. Soc. 2007, 129, 8156-8162
5. Mahadevan, V.; Getzler, Y. D. Y. L.; Coates, G. W. Angew. Chem., Int. Ed. 2002, 41, 2781-2784
6. Cao, J.; Zhou, F.; Zhou, J. Angew. Chem., Int. Ed. 2010, 49, 4976-4980
7. Clegg, W.; Harrington, R.; North, M.; Pasquale, R. Chem.-Eur. J. 2010, 16, 6828-6843
8. Darensbourg, D. J. Chem. Rev. 2007, 107, 2388-2410
9. Graves, C. R.; Zhou, H.; Stern, C. L.; Nguyen, S. T. J. Org. Chem. 2007, 72, 9121-9133
10. Ko, B.; Wu, C.; Lin, C. Organometallics 2000, 19, 1864-1869
11. Lee, P.; Liang, L. Inorg. Chem. 2009, 48, 5480-5487
12. Muñoz-Hernández, M.; Sannigrahi, B.; Atwood, D. A. J. Am. Chem. Soc. 1999, 121, 6747-6748
13. Ahmed, S. A.; Hill, M. S.; Hitchcock, P. B.; Mansell, S. M.; St John, O. Organometallics 2007, 26, 538-549
14. Raders, S. M.; Verkade, J. G. J. Org. Chem. 2009, 74, 5417-5428
15. Hamashima, Y.; Sawada, D.; Kanai, M.; Shibasaki, M. J. Am. Chem. Soc. 1999, 121, 2641-2642
16. Raders, S. M.; Verkade, J. G. Tetrahedron Lett. 2009, 50, 5317-5321
17. Li, W.; Qin, S.; Su, Z.; Yang, H.; Hu, C. Organometallics 2011, 30, 2095-2104
18. Dagorne, S.; Le Bideau, F.; Welter, R.; Bellemin-Laponnaz, S.; Maisse-Francois, A. Chem.-Eur. J. 2007, 13, 3202-3217
19. Johnson, A. L.; Davidson, M. G.; Perez, Y.; Jones, M. D.; Merle, N.; Raithby, P. R.; Richards, S. P. Dalton Trans. 2009, 5551-5558
20. Dechy-Cabaret, O.; Martin-Vaca, B.; Bourissou, D. Chem. Rev. 2004, 104, 6147-6176
21. Chisholm, M. H. Pure Appl. Chem. 2010, 82, 1647-1662
22. Stanford, M. J.; Dove, A. P. Chem. Soc. Rev. 2010, 39, 486-494
23. Thomas, C. M. Chem. Soc. Rev. 2010, 39, 165-173
24. Dijkstra, P. J.; Du, H.; Feijen, J. Polym. Chem. 2011, 2, 520-527
25. Nomura, N.; Ishii, R.; Akakura, M.; Aoi, K. J. Am. Chem. Soc. 2002, 124, 5938-5939
26. Doherty, S.; Errington, R. J.; Housley, N.; Clegg, W. Organometallics 2004, 23, 2382-2388
27. Tang, Z.; Yang, Y.; Pang, X.; Hu, J.; Chen, X.; Hu, N.; Jing, X. J. Appl. Polym. Sci. 2005, 98, 102-108
28. Pang, X.; Du, H.; Chen, X.; Zhuang, X.; Cui, D.; Jing, X. J. Polym. Sci., Part A: Polym. Chem. 2005, 43, 6605-6612
29. Ma, H.; Melillo, G.; Oliva, L.; Spaniol, T. P.; Englert, U.; Okuda, J. Dalton Trans. 2005, 721-727
30. Lee, W.; Liang, L. Dalton Trans 2005, 1952-6
31. Hormnirun, P.; Marshall, E. L.; Gibson, V. C.; Pugh, R. I.; White, A. J. P. Proc. Natl. Acad. Sci. U.S.A. 2006, 103, 15343-15348
32. Du, H.; Pang, X.; Yu, H.; Zhuang, X.; Chen, X.; Cui, D.; Wang, X.; Jing, X. Macromolecules 2007, 40, 1904-1913
33. Bouyahyi, M.; Grunova, E.; Marquet, N.; Kirillov, E.; Thomas, C. M.; Roisnel, T.; Carpentier, J. Organometallics 2008, 27, 5815-5825
34. Du, H.; Velders, A. H.; Dijkstra, P. J.; Zhong, Z.; Chen, X.; Feijen, J. Macromolecules 2009, 42, 1058-1066
35. Darensbourg, D. J.; Karroonnirun, O. Organometallics 2010, 29, 5627-5634
36. Darensbourg, D. J.; Karroonnirun, O.; Wilson, S. J. Inorg. Chem. 2011, 50, 6775-6787
37. Ma, W.; Wang, Z. Organometallics 2011, 30, 4364-4373
38. Chen, H.; Dutta, S.; Huang, P.; Lin, C. Organometallics 2012, 31, 2016-2025
39. Tang, Z.; Chen, X.; Pang, X.; Yang, Y.; Zhang, X.; Jing, X. Biomacromolecules 2004, 5, 965-970
40. Ovitt, T. M.; Coates, G. W. J. Am. Chem. Soc. 2002, 124, 1316-1326
41. Wade, C. R.; Lamprecht, B. J.; Day, V. W.; Belot, J. A. Polyhedron 2007, 26, 3286-3290
42. Emig, N.; Nguyen, H.; Krautscheid, H.; Réau, R.; Cazaux, J.; Bertrand, G. Organometallics 1998, 17, 3599-3608
43. Liu, Z.; Gao, W.; Zhang, J.; Cui, D.; Wu, Q.; Mu, Y. Organometallics 2010, 29, 5783-5790
44. Whitelaw, E. L.; Loraine, G.; Mahon, M. F.; Jones, M. D. Dalton Trans. 2011, 40, 11469-11473
45. Wang, Y.; Ma, H. Chem. Commun. 2012, 48, 6729-6731
46. Allan, L. E. N.; Bélanger, J. A.; Callaghan, L. M.; Cameron, D. J. A.; Decken, A.; Shaver, M. P. J. Organomet. Chem. 2012, 706-707, 106-112
47. Alaaeddine, A.; Roisnel, T.; Thomas, C.; Carpentier, J. Adv. Synth. Catal. 2008, 350, 731-740
48. Atwood, D. A.; Harvey, M. J. Chem. Rev. 2001, 101, 37-52
49. Weil, J.; Mathers, R. T.; Getzler, Y. D. Y. L. Macromolecules 2012, 45, 1118-1121
50. Culkin, D. A.; Jeong, W.; Csihony, S.; Gomez, E. D.; Balsara, N. P.; Hedrick, J. L.; Waymouth, R. M. Angew. Chem., Int. Ed. 2007, 46, 2627-2630
51. Jeong, W.; Shin, E. J.; Culkin, D. A.; Hedrick, J. L.; Waymouth, R. M. J. Am. Chem. Soc. 2009, 131, 4884-4891
52. Kricheldorf, H. R. J. Polym. Sci., Part A: Polym. Chem. 2004, 42, 4723-4742
53. Kricheldorf, H. R.; Lomadze, N.; Schwarz, G. Macromolecules 2008, 41, 7812-7816
54. Bielawski, C. W.; Benitez, D.; Grubbs, R. H. Science 2002, 297, 2041-2044
55. Kim, Y.; Verkade, J. Inorg. Chem. 2003, 42, 4804-4806
56. Hemmingson, S. L.; Stevens, A. J.; Tanski, J. M.; Getzler, Y. D. Y. L. Acta Crystallogr., Sect. E: Struct. Rep. Online 2010, E66, m937
57. Hu, C.; Wang, Y.; Xiang, H.; Fu, Y.; Fu, C.; Sun, J.; Xiang, Y.; Ruan, C.; Li, X. Polym. Int. 2012, 61, 1564-1574
58. Atwood, D. A.; Hutchison, A. R.; Zhang, Y. Struct. Bonding (Berlin) 2003, 105, 167-201
59. Addison, A. W.; Rao, T. N.; Reedijk, J.; van Rijn, J.; Verschoor, G. C. J. Chem. Soc., Dalton Trans. 1984, 1349-1356
60. Su, W.; Kim, Y.; Ellern, A.; Guzei, I. A.; Verkade, J. G. J. Am. Chem. Soc. 2006, 128, 13727-13735
61. Su, W.; Kobayashi, J.; Ellern, A.; Kawashima, T.; Verkade, J. G. Inorg. Chem. 2007, 46, 7953-7959
62. Badiei, Y. M.; Jiang, Y.; Widger, L. R.; Siegler, M. A.; Goldberg, D. P. Inorg. Chim. Acta 2012, 382, 19-26
63. Tiempos-Flores, N.; Metta-Magana, A.; Montiel-Palma, V.; Cortes-Llamas, S.; Munoz-Hernandez, M. Dalton Trans. 2010, 39, 4312-4320
64. Wasserman, E. P.; Annis, I.; Chopin, L. J., III; Price, P. C.; Petersen, J. L.; Abboud, K. A. Macromolecules 2005, 38, 322-333
65. Szigethy, G.; Heyduk, A. F. Dalton Trans. 2012, 41, 8144-8152
66. Nishida, H.; Mori, T.; Hoshihara, S.; Fan, Y.; Shirai, Y.; Endo, T. Polym. Degrad. Stab. 2003, 81, 515-523
67. Williams, D. B.; Lawton, M. J. Org. Chem. 2010, 75, 8351-8354
68. Sheldrick, G. M. Acta Crystallogr., Sect. A: Found. Crystallogr. 2008, A64, 112-122
69. Macrae, C. F.; Bruno, I. J.; Chisholm, J. A.; Edgington, P. R.; McCabe, P.; Pidcock, E.; Rodriguez-Monge, L.; Taylor, R.; van de Streek, J.; Wood, P. A. J. Appl. Crystallogr. 2008, 41, 466-470